• Title/Summary/Keyword: Powder removal

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Removal Characteristics of Copper from Anthraquinone Dyes by Iron Cementation (안트라퀴논계 염료에서 철 교착반응에 의한 구리의 제거 특성)

  • 천재기;이석희;주창식
    • Journal of the Korean Graphic Arts Communication Society
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    • v.20 no.1
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    • pp.45-53
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    • 2002
  • The removal of chelated copper from anthraquinone dyes by cementation on powdered iron was studied. The removal of chelated copper was found to be a function of solution pH, amount of NTA and iron, and reaction temperature. In the presence of NTA, reaction rate of cementation was found to be strongly dependent on reaction temperature, solution pH, amount of NTA and amount of iron powder. These experimental results can be explained successfully by the distribution of complexed copper iron in solutions.

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Evaluation of the adsorptive capacity of spent coffee powder for the removal of aqueous organic pollutants (액상 유기오염물질에 대한 폐커피가루의 흡착능력 평가)

  • Kim, Seulgi;Na, Seungmin;Son, Younggyu
    • Journal of Wetlands Research
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    • v.18 no.1
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    • pp.39-44
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    • 2016
  • The reuse of spent coffee powder has been researched for environmental engineering applications such as adsorbents of organic/inorganic pollutants. In this study adsorption equilibrium tests and adsorption kinetics tests for the removal of aqueous organic pollutant (methylene blue) were conducted using spent coffee powder, granular activated carbon, and powdered activated carbon. It was found that the maximum adsorption capacity of three adsorbents followed the order of powdered activated carbon (178.6 mg/g) > spent coffee powder (60.6 mg/g) > granular activated carbon (15.6 mg/g). The results of adsorption kinetics tests also indicated that spent coffee powder had higher kinetic parameters than granular activated carbon for pseudo 1st and 2nd order kinetics. The high performance of spent coffee powder might be due to its porous surface like those of granular and powdered activated carbons and smaller particle size comparing with granular activated carbon.

A Study on Rinsing Effects of Sn Sensitization and Pd Activation Processes for Uniform Electroless Plating (무전해 도금에서 Sn 민감화와 Pd 활성화 공정의 세척 효과에 대한 연구)

  • Seong-Jae, Jeong;Mi-Se, Chang;Jae-Won, Jeong;Sang-Sun, Yang;Young-Tae, Kwon
    • Journal of Powder Materials
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    • v.29 no.6
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    • pp.511-516
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    • 2022
  • Electroless plating is widely utilized in engineering for the metallization of insulator substrates, including polymers, glass, and ceramics, without the need for the application of external potential. Homogeneous nucleation of metals requires the presence of Sn-Pd catalysts, which significantly reduce the activation energy of deposition. Therefore, rinsing conducted during Sn sensitization and Pd activation is a key variable for the formation of a uniform seed layer without the lack or excess of catalysts. Herein, we report the optimized rinsing process for the functionalization of Sn-Pd catalysts, which enables the uniform FeCo metallization of the glass fibers. Rinsing enables good deposition of the FeCo alloy because of the removal of excess catalysts from the glass fiber. Concurrently, excessive rinsing results in a complete removal of the Sn-Pd nucleus. Collectively, the comprehensive study of the proposed nanomaterial preparation and surface science show that the metallization of insulators is a promising technology for electronics, solar cells, catalysts, and mechanical parts.

Odor Removal with Powdered Adsorbent using Bag-filter System (분말 흡착제를 이용한 악취 저감 여과 집진장치 개발연구)

  • Xu, Rong-bin;Kim, Tae-Hyeung;Ha, Hyun-Chul;Piao, Cheng-Xu
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.27 no.4
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    • pp.291-301
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    • 2017
  • Objectives: In order to improve the working environment and solve the complaints, many efforts have been made to remove the odor from the industrial process. There are many disposal methods to remove odor, but there are many disadvantages and inadequate applications. The Purpose of this study was to develop a bag-filer system for odor removal using powder adsorbent. Methods: The bag-filter system is composed of a shear bag filter, an absorbent spraying system and an absorbent circulation system. The spraying absorbent system was connected with the inlet duct of the shear bag filter for inputting adsorbent. And the absorbent circulation system can transport the collecting adsorbent from hoper to the inlet duct of the system. As a result, the adsorbent can remove odor with recycling in the system. Also affective factors like the powdered absorbent combination and injection method was researched for maximization of system efficiency. The study was conducted in two stages. The first step was testing equipment made and the second is to evaluate the efficiency of the odor control by connecting to the actual odor generation process. Results: Both experiment stages showed efficient odor control ability. The adsorption efficiency of the system is demonstrated and the odor was adsorbed well by the powder adsorbent. It is essential to accurately understand the characteristics of the odorous and use the appropriate adsorbent. Although the powder adsorbent was used in the experiment, the problem of scattering did not occur due to the high degree of system sealing. Also the system manufactured in this study was designed to recycle the adsorbent, so adsorbent reuse or batch processing is convenient. Conclusions: The applicability of the system has been proven through this research. Customized systems for industrial process and the appropriate adsorbent base on the characteristics of pollutant generation will show efficient odor collection ability.

Removal of Ammonia in Water using Acid-impregnated Activated Carbon and Dynamic Membrane System (산 첨착활성탄과 동적막 공정을 이용한 수중 암모니아 제거)

  • Choi, Won Kyung;Shin, Dong-Ho;Lee, Yong Taek
    • Applied Chemistry for Engineering
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    • v.17 no.3
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    • pp.310-316
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    • 2006
  • In this study, activated carbon in a powder form was used to remove dissolved ammonia which causes a fouling smell in water. Since the adsorption capacity of common powder activated carbon is not high enough, we prepared powder activated carbon deposited on an acid solution to enhance the adsorption capacity. The acid-impregnated activated carbon was applied on the surface of porous fibril support ($10{\sim}50{\mu}m$) by which adsorption and separation processes take place simultaneously by varying effective pressure. As the result, the ammonia removal efficiency is above 60% in the mixing process which is 10~15% higher than general powder activated carbon. From the result of an experiment on the pure permeable test of a dynamic membrane, its transmittance is 400~700 LMH (liter per hour), indicating that the prepared membrane works as a microfiltration membrane. Therefore, it is expected that the membrane prepared in this way would improve the efficiency of water treatment than conventional membranes.

Synthesis and Characteristics of W-l5wt%Cu Nanocomposite Powder by Oxide Reduction (산화물환원에 의한 W-15wt%Cu 나노복합분말의 합성과 특성)

  • 윤의식
    • Journal of Powder Materials
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    • v.4 no.4
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    • pp.304-309
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    • 1997
  • The synthesis of W-l5wt%Cu nanocomposite powder by hydrogen reduction of ball milled W-Cu oxide mixture was investigated in terms of powder characteristics such as particle size, mixing homogeneity and micropore structure. It is found that the micropores in the ball milled oxide (2-50 nm in size) act as an effective removal path of water vapor, followed by the formation of dry atmosphere at reaction zone. Such thermodynamic condition enhances the nucleation of W phase but suppresses the growth process, being in favor of the formation of W nanoparticles (about 21 nm in size). In addition, the superior mixing homogeneity of starting oxide mixture turned out to Play a significant role for forming extraordinary chemical homogeneity of W-l5wt%Cu nanocomposite powder.

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Pretreatment Condition of Cu by Ammonium-Based Mixed Solvent and Its Effects on the Fabrication of Ag-Coated Cu Particles (Ag 도금 Cu 입자의 제조에서 암모늄 기반 혼합 용매를 사용한 Cu 입자의 전처리 조건과 이의 영향)

  • Lee, Hee Bum;Lee, Jong-Hyun
    • Korean Journal of Materials Research
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    • v.26 no.3
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    • pp.109-116
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    • 2016
  • To achieve the fabrication of high-quality Ag-coated Cu particles through a wet chemical process, we reported herein pretreatment conditions using an ammonium-based mixed solvent for the removal of a $Cu_2O$ layer on Cu particles that were oxidized in air for 1 hr at $200^{\circ}C$ or for 3 days at room temperature. Furthermore, we discussed the results of post-Ag plating with respect to removal level of the oxide layer. X-ray diffraction results revealed that the removal rate of the oxide layer is directly proportional to the concentration of the pretreatment solvent. With the results of Auger electron spectroscopy using oxidized Cu plates, the concentrations required to completely remove 50-nm-thick and 2-nm-thick oxides within 5 min were determined to be X2.5 and X0.13. However, the optimal concentrations in an actual Ag plating process using Cu powder increased to X0.4 and X0.5, respectively, because the oxidation in powder may be accelerated and the complete removal of oxide should be tuned to the thickest oxide layer among all the particles. Back-scattered electron images showed the formation of pure fine Ag particles instead of a uniform and smooth Ag coating in the Ag plating performed after incomplete removal of the oxide layer, indicating that the remaining oxide layer obstructs heterogeneous nucleation and plating by reduced Ag atoms.

Air Pollutant Removal Rates of Concrete Permeable Blocks Produced with Coated Zeolite Beads (코팅된 제올라이트 비드를 이용한 콘크리트 투수블록의 대기전구물질 제거율 평가)

  • Park, Jun-Seo;Yang, Keun-Hyeok
    • Journal of the Korea Institute of Building Construction
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    • v.23 no.2
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    • pp.153-164
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    • 2023
  • The objective of this study is to examine the removal rate of air pollutants, specifically sulfur oxides (SOx) and nitrogen oxides(NOx), using concrete permeable blocks containing zeolite beads coated with materials capable of eliminating these pollutants. Titanium dioxide(TiO2) powder and coconut shell powder were utilized for the removal of SOx and NOx and were applied as coatings on the zeolite beads. Concrete permeable block specimens embedded with the coated zeolite beads were produced using an actual factory production line. Test results demonstrated that the concrete permeable block containing zeolite beads coated with coconut shell powder in the surface layer achieved SOx and NOx removal rates of 12.5% and 99%, respectively, exhibiting superior performance compared to other blocks. Additionally, the flexural strength and slip resistance were 5.3MPa and 65BPN or higher, respectively, satisfying the requirements specified in KS F 4419 and KS F 4561. Conversely, the permeability coefficient exhibited low permeability, with grades 2 and 3 before and after contaminant pollution, according to the standard for 'design, construction, and maintenance of pavement using permeable block'. In conclusion, incorporating zeolite beads coated with coconut shell powder in the surface layer enables simultaneous removal of SOx and NOx, irrespective of ultraviolet rays, while maintaining adequate flexural strength and slip resistance. However, the permeability is significantly reduced, necessitating further improvements.

Wear Patterns and Mechanisms of Cutting Tool in Cutting of Machinable Ceramics (가공성 세라믹 절삭에서 공구의 마멸 패턴과 메카니즘)

  • Jang, Sung-Min;Baek, Seung-Yub
    • Journal of the Korean Society of Safety
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    • v.25 no.5
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    • pp.1-6
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    • 2010
  • When the ceramic material is being machined, micro crack and brittle fracture dominate the process of material removal. Generally, ceramics are very difficult-to-cut materials and machined using conventional method such as grinding and polishing. However, such processes are generally cost-expensive and have low material removal rate. Machinable ceramics used in this study contain BN powder to overcome these problem and for productivity elevation. This paper focuses on machinability evaluation during end mill process with CNC machining center in this study. Experiment for this purpose is performed for tool wear patterns and mechanism.

A Study on Mirror-like Polishing of Brittle Material by Elastic Emission Machining (탄성방출가공법에 의한 경취재료의 경면 폴리싱에 관한 연구)

  • 남성호;김정두
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.04a
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    • pp.1009-1014
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    • 1997
  • The small material removal rate of elastic emission machinong (EEM) becomes a serious problem due to using fine powder particles for obtaining finished of high quality. If a cylindrical polyurethane-wheel is used as a tool for accelerating powder particles, the efficiency of machining may be increased through enlarging the machining regionand increasing the surface velocity of the wheel. If these analyicl results are compared with experimental ones, characteristics of EEM using polyurethan-wheel can be clarified. In this study, effects of EEM using cylindrical polyurethane-wheel on the surface roughness and the material removal rate were verified through polishing of the brittle material under various conditions. The high-efficient polishing of silicon wafer has been also carried out using this method.

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