• Title/Summary/Keyword: Powder characteristic

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AN ELECTROCHEMICAL STUDY ON SURFACE FINISH OF DENTAL AMALGAM (아말감의 표면연마에 관한 전기화학적 연구)

  • Suk, Chang-In;Um, Chung-Moon
    • Restorative Dentistry and Endodontics
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    • v.16 no.2
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    • pp.18-32
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    • 1991
  • The purpose of this study was to observe characteristic properties of amalgam through the polarization curves and SEM images from 4 type amalgams (Amalcap, Shofu spherical. Dispersalloy and Tytin) with 3 different surface finish procedures (polishing, burnishing and carving) by using the potentiostats (EG & GPARC) and SEM (Jeol JSM-35). After each amalgam alloy and Hg was triturated as the direction of the manufacturer by means of mechanical amalgamator (Samki), the triturated mass was inserted into the cylndrical metal mold which was 12 mm in diameter and 10 mm in height and was pressed with $100kg/cm^2$. 4 specimens of each type amalgam were burnished with egg burnisher and another 4 specimens of each type amalgam were carved with Hollenback carver. Above 8 specimens and remaining untreated 4 specimens were stored at room temperature for about 7 days. Untreated 4 specimens of each type amalgam were polished with abrasive papers (Deer) from #400 to #1200 and finally on the polishing cloth with $0.5{\mu}m$ and $0.06{\mu}m$ $Al_2O_3 $ powder suspended water. Anodic polarization measurements was employed to compare the corrosion behaviours of the amalgams in 0.9% saline solution at $37^{\circ}C$. The open circuit potential was determined after 30 minutes immersion of specimen in electrolyte. The scan rate was 1 mV/sec and the surface area of amalgam exposed to the solution was $0.64cm^2$ for each specimen. All the potentials reported are with respect to a saturated calomel electrode (SCE). SEM images of each specimen were taken after + 800 mV (SCE) polarization. The results were as follows: 1. The corrosion potential of high copper amalgam was more anodic than that of low copper amalgam. 2. The polished amalgam were more resistant to corrosion than any other burnished and carved amalgam. 3. In the case of polishing, current density of high copper amalgam was lower than that of low copper amalgam.

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Effects of Adsorption Condition on Fat-binding Characteristics of Chitosan (흡착조건이 키토산의 지방질 흡착 특성에 미치는 영향)

  • LEE Keun-Tai;SONG Ho-Su;PARK Seong-Min;KANG Ok-Ju;CHEONG Hyo-Sook
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.37 no.5
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    • pp.359-365
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    • 2004
  • To study the lipid adsorption characteristic of chitosans with different molecular weights and the degrees of deacetylation, in vitro test and near-infrared (NIR) spectroscopic analysis have been performed for the measurement of lipid adsorption characteristics of chitosan. The degrees of deacetylation in chitosans were $70{\%},\;85{\%}\;and\;92{\%}$ at different deacetylation times (1 hr, 2 hrs, 3 hrs), respectively. The molecular weight of each chitosan was controlled by enzymatic hydrolysis, and then the molecular weight of the chitosan was 4 kDa. The bulk density, water holding capacity and fat binding capacity of each chitosan powder were $96.2-504.0{\%},\;374.4-1217.9{\%},\;and\;307.0-659.3{\%}$, respectively. The higher molecular weight of chitosan was exhibited the lower bulk density and the higher water and fat binding capacities. Bindinf capacities of chitosan powders to bile salts, cholesterol and linoleic acid were $41.2-63.3{\%},\;40.8-67.4{\%},\;42.6-72.6{\%}$, respectively. In NIR spectrum of lipid adsorbed chitosan the occurrence static eletronical binding between chitosan and lipid was identified by NIR spectrum peak induced from combination of carboxylic group in lipid and amino group in chitosan. In conclusion, the higher degree of deacetylation and molecular weight of chitosan showed the higher lipid binding capacity and the lipid adsorption of chitosan were occurred by combination of carboxylic group in lipids and amino group in chitosan.

A Study on the Beauty Culture of Chosun Period Appearing in Korean Genre Painting (조선후기 풍속화에 나타난 미용문화의 특성)

  • An, Jong-Suk;Lee, Sang-Eun
    • Journal of the Korea Fashion and Costume Design Association
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    • v.8 no.3
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    • pp.73-85
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    • 2006
  • The purpose of this study is to consider the characteristics of beauty culture in the latter period of Chosun Dynasty from the viewpoint of public morals and find out how characteristic beauty culture was developed along with traditional culture. Therefore, the clothes, the make-up, the style of beard and hair were examined and the beauty culture of women in the latter period Chosun Dynasty was considered. The changes of the beauty culture on the genre painting and the characteristics of the latter period Chosun Dynasty were analyzed. Conclusions are as follows ;First, in case of woman dress, the Korean Jergori was short and the Chima was too long. Due to the diversification of wearing, the underpants play as a decorations. Second, the hair which focus on the cleanness and the sanitation and the skin maintenance method were important. The make-up focus on make-up with powder which emphasis on the slim and round eyebrow, the small and thick lips for the beauty look of the latter period Chosun Dynasty. Third, a unmarried woman did the braids('Taun Muri') and a feme covert did 'Unseen Muri'. As people cling to the big and head of hairs gradually, the chignon('Terae Muri') was in fashion. The beauty culture in the latter period of Chosun Dynasty clothes and cosmetic treatment style were generalized through nobility, common people, lowly people. The imitation mentality which follow after Gisaeng style that led the fashion of that period was shown up. With understanding the beauty culture of the latter period of Chosun Dynasty, the study on the traditional beauty culture should be revitalized. This study help to uplift the pride on Korea traditional culture and to promote the globalization of Korean culture.

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Development and Performance Evaluation of a Two-component Thin Spray-on Liner to Guarantee Its Homogeneous Qualities and to Reduce Dust (균질한 품질 확보와 분진 저감을 위한 2성분 박층 뿜칠 라이너의 개발과 성능평가)

  • Chang, Soo-Ho;Choi, Soon-Wook;Lee, Chulho;Kang, Tae-Ho;Hwang, Gwi-Sung;Kim, Jintae;Choi, Myung-Sik
    • Tunnel and Underground Space
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    • v.26 no.5
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    • pp.441-453
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    • 2016
  • This study aimed to develop a two-component TSL suitable for reducing dust and guaranteeing homogeneous qualities during its spraying. Its performance was evaluated by a series of laboratory and field tests. High ductility of two-component TSL prototypes resulted in increasing their elongation at break even though their tensile strengths were slightly lower than those of one-component powder TSLs. One prototype of the two-component TSLs developed in this study was verified to satisfy every criterion specified by EFNARC (2008). Especially, it increased the average compressive strength of mortar specimens by 50% even when it coated them only with the thickness of 3 mm. From a preliminary spraying test, a spraying machine suitable for the developed TSL prototype was derived and modified. After its field application, dust and rebound generated during its spraying works were found to be very minimal. Its spraying rate was recorded to be approximately $60m^2/hr$. In addition, it showed a very rapid hardening characteristic compared with general sprayable waterproofing membranes.

Study on characteristic of mycelial culture in ear mushroom (목이의 균사생육 특성에 관한 연구)

  • Yu, Young-Jin;Choi, Kyu-Hwan;Jeong, Jong-Seong;Lee, Gi-Kwon;Choi, So-Ra
    • Journal of Mushroom
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    • v.11 no.1
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    • pp.15-20
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    • 2013
  • This study was performed to obtain the scientific data an artificial culture of ear mushroom(Auricularia auricula). Liquid cultural of Auricularia auricula. mycelium was characterized with respect to temperature, pH, compositions of inorganic, carbon and nitrogen. The its optimum temperature and media pH were at $25^{\circ}C$ and pH 5.0~6.0 on the mycelial growth, respectively. The optimum inorganic compositions and concentration for mycelial growth were $MgSO_4$ 0.05%(w/v) and $KH_2PO_4$ 0.1%(w/v), respectively. The optimum carbon sources and nitrogen sources were black-sugar 2%(w/v) and soybean powder at 0.3~0.5%(w/v) with7 days optimum culture time.

Phase Analysis of Mechanically Alloyed $\sigma$-VFe Alloy Powders by Neutron and X-ray Diffraction (기계적 합금화한 $\sigma$-VFe합금의 중성자 및 X선 회절에 의한 상분석)

  • 이충효;조재문;이상진;심해섭;이창희
    • Korean Journal of Materials Research
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    • v.11 no.8
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    • pp.664-664
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    • 2001
  • The mechanical alloying (MA) effect in $\sigma$-VFe intermetallic compound was studied by neutron and X-ray diffraction. The structure of MA $\sigma$-VFe powders were characterized by the X- ray diffraction with Cu- $K\alpha$ radiation and neutron diffraction with monochromatic neutrons of $1.835\AA$ using a high resolution powder diffractometer (HRPD). Mechanical alloying of $\sigma$-VFe compound gives rise to a dramatic structural change. After 60 hours of MA, the Fe-Fe distribution of the $\sigma$- phase VFe tetragonal structure with 30 atoms in a unit cell is found to change into that of the $\sigma$-(V,Fe) solid solution with bcc structure, which is a stable phase at elevated temperature above $1200^{\circ}C$. A comparison of X-ray diffraction data for the $\alpha$-phase has been also made with the corresponding neutron diffraction data. The (101) and (111) diffraction peaks of the $\sigma$-phase was clearly observed only in neutron diffraction pattern, which is believed to be a characteristic feature due to the chemical atomic ordering of $\sigma$- VFe phase.

Optimization of powder compaction parameters for the pressureless sintered ZTA (상압소결 ZTA의 분말 성형 공정 최적화)

  • 신동우;김경도;박삼식;임창성;이수완
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.2
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    • pp.356-364
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    • 1998
  • The dependence of green and sintered densities of Zirconia-Toughened Alumina ($ZTA:\;Al_2O_3/\;15\;vol{%}\;ZrO_2$) on the properties of spray-dried granules was studied thoroughly to establish the optimum compaction condition leading to high reproducibility in the light of sintered density. The sphericity, mean size, degree of hollow occurrence and moisture content of spray-dried granules were largely different in between the granule containing binder and the ones with no binder. The effect of these differences in the characteristic of granules on the compaction behavior was examined in terms of the compaction pressure from 80 MPa to 120 MPa 10 MPa increment and the compaction method, i.e., uniaxial and cold isostatic pressing. This work confirmed that the reproducibility of sintered density caused by the variation of granule property could be improved by the optimization of compaction process. The variation of sintered density was controlled within 1 % deviation by compacting the granules under a relatively low pressure of 80 MPa in an uniaxial forming and subsequent cold isostatic pressing at high pressure of 500 MPa.

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Basic and Creepy Characteristics of High Performance Concrete Complexly Using Blast Furnace Slag Powder and Fly ash (고로슬래그 미분말 및 플라이애시를 복합사용한 고성능 콘크리트의 기초 및 크리프 특성)

  • Park, Byung-Kwan;Pei, Chang-Chun;Kim, Soo-Yung;Kim, Bok-Kyu;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.11a
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    • pp.717-720
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    • 2008
  • This study analyzed the basic characteristics and the characteristic of drying shrinkage and creep of high performance concrete complexly metathesized by BS and FA and the results are summarized as the followings. Regarding to the compressive strengths according to the passage of aging, OPC was appeared to be larger than B2F1 at the initial aging but B2F1 was appeared to be higher than OPC at aging 28days. Regarding to the changing rate of drying shrinkage according to the passage of aging, both OPC and B2F1 were appeared to be increased and, at aging 60days, B2F1 was appeared to be largely increased by about 42% as -21${\times}$10-6 및 -51${\times}$10-6 as compared to OPC. The transforming rate of creep was appeared to have been largely increased at the initial aging and then be smoothly increased somewhat as the aging was passed. And regardign to the transforming rate of creep after 60 days had been passed, B2F1 was appeared to be largely increased by about 13% as compared to OPC.

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Optimal Strategy for Ethanol Production in Repeated Fed-batch Operation Using Flocculent Sacchromyces cerevisiae (응집성 Sacchromyces cerevisiae 를 이용한 반복 유가식 ethanol 생산에서의 최적 운전전략)

  • Lee, Sang-Eun;Yeon, Ji-Hyeon;Seo, Yong-Chang;Kang, Do-Hyung;Lee, Hyeon-Yong;Jung, Kyung-Hwan
    • KSBB Journal
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    • v.25 no.2
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    • pp.179-186
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    • 2010
  • We investigated the optimal strategy for ethanol production using flocculent Sacchromyces cerevisiae ATCC 96581. Considering the characteristic of flocculent yeast, a repeated fed-batch ethanol fermentation was designed, in which non-sterile glucose powder was fed every 12 hours and, after cell flocculation, new feeding medium was exchanged every 24 or 36 hours. We particularly compared this fermentation process with those when cell flocculation was not carried out. Finally, the maximal total ethanol production was 825 g-ethanol during 120 hours, in which the time interval of withdrawal-fill of feeding medium was 24 hours and cell flocculation was carried out.

Identification of Characteristic Aroma-active Compounds from Burnt Beef Reaction Flavor Manufactured by Extrusion (압출성형에 의해 제조된 구운 쇠고기 반응향의 특징적인 향기성분 동정)

  • Kim, Ki-Won;Seo, Won-Ho;Baek, Hyung-Hee
    • Korean Journal of Food Science and Technology
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    • v.38 no.5
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    • pp.621-627
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    • 2006
  • To characterize aroma properties of burnt beef reaction flavor manufactured by extrusion, volatile flavor compounds and aroma-active compounds were analyzed by simultaneous steam distillation and solvent extraction (SDE)-gas chromatography-mass spectrometry-olfactometry (GC-MS-O). Hydrolyzed vegetable protein (HVP) was successfully extruded with precursors (glucose, cystine, furaneol, thiamin, methionine, garlic powder, and lecithin) at $160^{\circ}C$, screw speed of 45 rpm, and feed rate of 38 kg/hr. Sixty eight volatile flavor compounds were found in burnt beef reaction flavor. The number of volatile flavor compounds decreased significantly when HVP was extruded either with furaneol-free precursors or without precursors. Twenty seven aroma-active compounds were detected in burnt beef reaction flavor. Of these, methional and 2-methyl-3-furanthiol were the most intense aroma-active compounds. It was suggested that furaneol played an important role in the formation of burnt beef reaction flavor.