• Title/Summary/Keyword: Powder based 3D printing

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Enhancing Electrical Properties of N-type Bismuth Telluride Alloys through Graphene Oxide Incorporation in Extrusion 3D Printing

  • Jinhee Bae;Seungki Jo ;Kyung Tae Kim
    • Journal of Powder Materials
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    • v.30 no.4
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    • pp.318-323
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    • 2023
  • The thermoelectric effect, which converts waste heat into electricity, holds promise as a renewable energy technology. Recently, bismuth telluride (Bi2Te3)-based alloys are being recognized as important materials for practical applications in the temperature range from room temperature to 500 K. However, conventional sintering processes impose limitations on shape-changeable and tailorable Bi2Te3 materials. To overcome these issues, three-dimensional (3D) printing (additive manufacturing) is being adopted. Although some research results have been reported, relatively few studies on 3D printed thermoelectric materials are being carried out. In this study, we utilize extrusion 3D printing to manufacture n-type Bi1.7Sb0.3Te3 (N-BST). The ink is produced without using organic binders, which could negatively influence its thermoelectric properties. Furthermore, we introduce graphene oxide (GO) at the crystal interface to enhance the electrical properties. The formed N-BST composites exhibit significantly improved electrical conductivity and a higher Seebeck coefficient as the GO content increases. Therefore, we propose that the combination of the extrusion 3D printing process (Direct Ink Writing, DIW) and the incorporation of GO into N-BST offers a convenient and effective approach for achieving higher thermoelectric efficiency.

Influence of Powder Size on Properties of Selectively Laser-Melted- AlSi10Mg Alloys (AlSi10Mg 합금분말 크기가 선택적 레이저 용융된 3차원 조형체 특성에 미치는 영향)

  • Eom, Yeong Seong;Kim, Dong Won;Kim, Kyung Tae;Yang, Sang Sun;Choe, Jungho;Son, Injoon;Yu, Ji Hun
    • Journal of Powder Materials
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    • v.27 no.2
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    • pp.103-110
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    • 2020
  • Aluminum (Al) - based powders have attracted attention as key materials for 3D printing because of their excellent specific mechanical strength, formability, and durability. Although many studies on the fabrication of 3D-printed Al-based alloys have been reported, the influence of the size of raw powder materials on the bulk samples processed by selective laser melting (SLM) has not been fully investigated. In this study, AlSi10Mg powders of 65 ㎛ in average particle size, prepared by a gas atomizing process, are additively manufactured by using an SLM process. AlSi10Mg powders of 45 ㎛ average size are also fabricated into bulk samples in order to compare their properties. The processing parameters of laser power and scan speed are optimized to achieve densified AlSi10Mg alloys. The Vickers hardness value of the bulk sample prepared from 45 ㎛-sized powders is somewhat higher than that of the 65 ㎛m-sized powder. Such differences in hardness are analyzed because the reduction in melt pool size stems from the rapid melting and solidification of small powders, compared to those of coarse powders, during the SLM process. These results show that the size of the powder should be considered in order to achieve optimization of the SLM process.

Evaluation and Development of Multi Thermal Bubble Ink Jet 3D Printing System (다중써멀버블 잉크젯방식의 3D 프린팅 시스템 개발 및 성능평가)

  • Shin, Mun Gwan;Bae, Sung Woo;Kim, Jung Su
    • Journal of the Korean Society for Precision Engineering
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    • v.32 no.9
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    • pp.787-792
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    • 2015
  • Recently, 3D printing technology is a hot issue in various industrial fields. According to the user's application, it allows for the free form fabrication method to be utilized in a wide range. The powder based fusion technique is one of the 3D printing methods. When using this method it is possible to apply the various binder jetting techniques such as piezo, thermal bubble jet, dispenser and so on. In this paper, a multi thermal bubble ink jet was integrated for jetting of powder binding material and developing a power fused 3D printing system. For high quality 3D printing parts, it needs an analysis and evaluation of the behavior of the thermal bubble ink jet head. In the experiment, a correlation between jetting binder quantity and layer thickness of powder was investigated, and a 3D part model was fabricated, which was used by measuring the scale factor.

Development of Multi Piezo Ink-Jet Printing System Using Arbitrarily Waveform Generator (임의 전압파형발생기를 이용한 다중 피에조 잉크젯 3D 프린팅 장비 개발)

  • Kim, Jung Su;Kim, Dong Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.32 no.9
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    • pp.781-786
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    • 2015
  • Recently, studies of 3D printing methods have been working in various applications. For example, the powder base method laminates the prints by using a binding or laser sintering method. However, the draw back of this method is that the post process is time consuming and does not allow for parts to be rapidly manufactured. The binding method requires the post process while the time required for the post process is longer than the manufacturing time. This paper proposes a UV curing binding method with an integrated piezo printing head system. The optimization of an arbitrary waveform generation for the control of a UV curable resin droplet was researched, in addition to developed optimized UV curing processes in multi nozzle ink jet heads.

Trend of Metal 3D Printing by Welding (용접에 의한 Metal 3D Printing의 동향)

  • Byun, Jae-Gyu;Cho, Sang-Myung
    • Journal of Welding and Joining
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    • v.34 no.4
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    • pp.1-8
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    • 2016
  • Metal AM(Additive Manufacturing) has been steadily developed and that is classified into two method. PBF(Powder Bed Fusion) deposited in the bed by the laser or electron beam as a heat source of the powder material and DED(Directed Energy Deposition) deposited by varied heat source of powder and solid filler material. In the developed countries has been applying high productivity process of solid filler metal based DED method to the aerospace and defense sectors. The price of the powder material is quite expensive compared to the solid filler metal. A study on DED method that is based on a solid filler metal is increasing significantly although was low accuracy and degree of freedom.

Cryogenic Tensile Behavior of Ferrous Medium-entropy Alloy Additively Manufactured by Laser Powder Bed Fusion

  • Seungyeon Lee;Kyung Tae Kim;Ji-Hun Yu;Hyoung Seop Kim;Jae Wung Bae;Jeong Min Park
    • Journal of Powder Materials
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    • v.31 no.1
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    • pp.8-15
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    • 2024
  • The emergence of ferrous-medium entropy alloys (FeMEAs) with excellent tensile properties represents a potential direction for designing alloys based on metastable engineering. In this study, an FeMEA is successfully fabricated using laser powder bed fusion (LPBF), a metal additive manufacturing technology. Tensile tests are conducted on the LPBF-processed FeMEA at room temperature and cryogenic temperatures (77 K). At 77 K, the LPBF-processed FeMEA exhibits high yield strength and excellent ultimate tensile strength through active deformation-induced martensitic transformation. Furthermore, due to the low stability of the face-centered cubic (FCC) phase of the LPBF-processed FeMEA based on nano-scale solute heterogeneity, stress-induced martensitic transformation occurs, accompanied by the appearance of a yield point phenomenon during cryogenic tensile deformation. This study elucidates the origin of the yield point phenomenon and deformation behavior of the FeMEA at 77 K.

Characterization and Classification of Pores in Metal 3D Printing Materials with X-ray Tomography and Machine Learning (X-ray tomography 분석과 기계 학습을 활용한 금속 3D 프린팅 소재 내의 기공 형태 분류)

  • Kim, Eun-Ah;Kwon, Se-Hun;Yang, Dong-Yeol;Yu, Ji-Hun;Kim, Kwon-Ill;Lee, Hak-Sung
    • Journal of Powder Materials
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    • v.28 no.3
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    • pp.208-215
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    • 2021
  • Metal three-dimensional (3D) printing is an important emerging processing method in powder metallurgy. There are many successful applications of additive manufacturing. However, processing parameters such as laser power and scan speed must be manually optimized despite the development of artificial intelligence. Automatic calibration using information in an additive manufacturing database is desirable. In this study, 15 commercial pure titanium samples are processed under different conditions, and the 3D pore structures are characterized by X-ray tomography. These samples are easily classified into three categories, unmelted, well melted, or overmelted, depending on the laser energy density. Using more than 10,000 projected images for each category, convolutional neural networks are applied, and almost perfect classification of these samples is obtained. This result demonstrates that machine learning methods based on X-ray tomography can be helpful to automatically identify more suitable processing parameters.

A Study on the Mechanical Properties of Al2O3 Cutting Tools by DLP-based 3D Printing (DLP 기반 3D 프린팅으로 제조된 Al2O3 절삭공구의 기계적 물성 연구)

  • Lee, Hyun-Been;Lee, Hye-Ji;Kim, Kyung-Ho;Kim, Kyung-Min;Ryu, Sung-Soo;Han, Yoonsoo
    • Journal of Powder Materials
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    • v.26 no.6
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    • pp.508-514
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    • 2019
  • In the development of advanced ceramic tools, material improvements and design freedom are critical in improving tool performance. However, in the die press molding method, many factors limit tool design and make it difficult to develop innovative advanced tools. Ceramic 3D printing facilitates the production of prototype samples for advanced tool development and the creation of complex tooling products. Furthermore, it is possible to respond to mass production requirements by reflecting the needs of the tool industry, which can be characterized by small quantities of various products. However, many problems remain in ensuring the reliability of ceramic tools for industrial use. In this study, alumina inserts, a representative ceramic tool, was manufactured using the digital light process (DLP), a 3D printing method. Alumina inserts prepared by 3D printing are pressurelessly sintered under the same conditions as coupon-type specimens prepared by press molding. After sintering, a hot isostatic pressing (HIP) treatment is performed to investigate the effects of relative density and microstructure changes on hardness and fracture toughness. Alumina inserts prepared by 3D printing show lower relative densities than coupon specimens prepared by powder molding but indicate similar hardness and higher fracture toughness values.

Fabrication and Characterization of PZT Suspensions for Stereolithography based on 3D Printing

  • Cha, JaeMin;Lee, Jeong Woo;Bae, Byeonghoon;Lee, Seong-Eui;Yoon, Chang-Bun
    • Journal of the Korean Ceramic Society
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    • v.56 no.4
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    • pp.360-364
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    • 2019
  • PZT suspensions for photo-curable 3D printing were fabricated and their characteristics were evaluated. After mixing the PZT, photopolymer, photo-initiator, and dispersant for 10 min by using a high-shear mixer, the viscosity characteristics were investigated based on the powder content. To determine an appropriate dispersant content, the dispersant was mixed at 1, 3, and 5 wt% of the powder and a precipitation test was conducted for two hours. Consequently, it was confirmed that the dispersibility was excellent at 3 wt%. Through thermogravimetric analysis, it was confirmed that weight reduction occurred in the photopolymer between 120? and 500?, thereby providing a debinding heat treatment profile. The fabricated suspensions were cured using UV light, and the polymer was removed through debinding. Subsequently, the density and surface characteristics were analyzed by using the Archimedes method and field-emission scanning electron microscopy. Consequently, compared with the theoretical density, an excellent characteristic of 97% was shown at a powder content of 87 wt%. Through X-ray diffraction analysis, it was confirmed that the crystallizability improved as the solid content increased. At the mixing ratio of 87 wt% powder and 13 wt% photo-curable resin, the viscosity was 3,100 cps, confirming an appropriate viscosity characteristic as a stereolithography suspension for 3D printing.

Investigation to Metal 3D Printing Additive Manufacturing (AM) Process Simulation Technology (I) (금속 3D 프린팅 적층제조(AM) 공정 시뮬레이션 기술에 관한 고찰(I))

  • Kim, Yong Seok;Choi, Seong Woong;Yang, Soon Yong
    • Journal of Drive and Control
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    • v.16 no.3
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    • pp.42-50
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    • 2019
  • 3D printing AM processes have advantages in complex shapes, customized fabrication and prototype development stage. However, due to various parameters based on both the machine and the material, the AM process can produce finished output after several trials and errors in the initial stage. As such, minimizing or optimizing negative factors for various parameters of the 3D printing AM process could be a solution to reduce the trial-and-error failures in the early stages of such an AM process. In addition, this can be largely solved through software simulation in the preprocessing process of 3D printing AM process. Therefore, the objective of this study was to investigate a simulation technology for the AM software, especially Ansys Inc. The metal 3D printing AM process, the AM process simulation software, and the AM process simulation processor were examined. Through this study, it will be helpful to understand 3D printing AM process and AM process simulation processor.