• Title/Summary/Keyword: Post-heat-treatment

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Microstructure and Hardness of Titanium Aluminide/Carbide Composite Coatings Prepared by Reactive Spray Method (반응성 스프레이방법으로 제작한 티타늄 알루미나이드/탄화물 복합박막의 미세조직과 경도)

  • Han, Chang-Suk;Jin, Sung-Yooun
    • Korean Journal of Materials Research
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    • v.30 no.7
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    • pp.350-358
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    • 2020
  • A variety of composite powders having different aluminum and carbon contents are prepared using various organic solvents having different amounts of carbon atoms in unit volume as ball milling agents for titanium and aluminum ball milling. The effects of substrate temperature and post-heat treatment on the texture and hardness of the coating are investigated by spraying with this reduced pressure plasma spray. The aluminum part of the composite powder evaporates during spraying, so that the film aluminum content is 30.9 mass%~37.4 mass% and the carbon content is 0.64 mass%~1.69 mass%. The main constituent phase of the coating formed on the water-cooled substrate is a non-planar α2 phase, obtained by supersaturated carbon regardless of the alloy composition. When these films are heat-treated at 1123 K, the main constituent phase becomes γ phase, and fine Ti2AlC precipitates to increase the film hardness. However, when heat treatment is performed at a higher temperature, the hardness is lowered. The main constitutional phase of the coating formed on the preheated substrate is an equilibrium gamma phase, and fine Ti2AlC precipitates. The hardness of this coating is much higher than the hardness of the coating in the sprayed state formed on the water-cooled substrate. When hot pressing is applied to the coating, the porosity decreases but hardness also decreases because Ti2AlC grows. The amount of Ti2AlC in the hot-pressed film is 4.9 vol% to 15.3 vol%, depending on the carbon content of the film.

Effect of Electrical Resistance Welding on Microstructure and Mechanical Properties of API X70 Linepipe Steel (ERW 용접 전후 API X70 라인파이프강의 미세조직과 기계적 특성 변화)

  • Oh, Dong-Kyu;Choi, Ye-Won;Shin, Seung-Hyeok;Jeong, Han-Gil;Kwack, Jin-Sub;Hwang, Byoungchul
    • Journal of the Korean Society for Heat Treatment
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    • v.35 no.4
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    • pp.185-192
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    • 2022
  • Variations in the microstructure and mechanical properties of API X70 steel processed by piping, electrical resistance welding (ERW), and post seam annealing (PSA) are investigated in this study. In the welding zone, some elongated pearlites are formed and grains coarsening occurs due to extra heat caused by the ERW and PSA processes. After the piping, the base metal shows continuous yielding behavior and a decrease in yield and impact strengths because mobile dislocation and back stress are introduced during the piping process. On the other hand, the ERW and PSA processes additionally decreased the impact strength of welding zone at room and low temperatures because some elongated pearlites easily act as crack initiation site and coarse ferrite grains facilitate crack propagation. As a result, the fracture surface of the welding zone specimen tested at low temperature revealed mostly cleavage fracture unlike the base metal specimen.

Occurrence of Ovario-uterine Disease and Hormonal Therapeutic Effect in Dairy Cows (젖소에서 난소.자궁 질병 발생과 호르몬 치료 효과)

  • Ryu, Jae-Sun;Park, Chul-Ho;Kim, Sang-Il;Bae, Jae-Han;Suh, Guk-Hyun;Kim, Jae-Pung;Park, Sang-Guk;Lee, Suk-Kyung;Son, Chang-Ho;Oh, Ki-Seok
    • Journal of Embryo Transfer
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    • v.26 no.1
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    • pp.37-43
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    • 2011
  • A total 5,946 cows from 24 dairy farms were carried out for the improvement of reproductive performance. Dairy cows in post-parturition 30 day were performed periodic reproductive examination to check for recovery of post-parturition ovary and uterus and for the early diagnosis of reproductive disease. The results obtained from this studies were as follow. The result of 1,126 cows with ovario-uterine disease were 579 slient heat and error of estrus detection (51.4%), 296 ovarian disease (26.3%), 248 uterine disease (22%), mummification and freematin were each 1 head (0.1%), respectively. Hormonal therapeutic effects were follicular cyst 81.5%, luteal cyst 90.7%, endometritis 86.9%, mucometra 90.1%, pyometra 60.9%, respectively. In cows, even if the 1st treatment fails, 2nd, 3rd treatment were performed. Therapeutic effect of 2nd, 3rd were reduced, but the number of cured cows were gradually increased. The cured cows after hormonal treatment were performed service repeatedly and the cumulative conception rate were increased. The cows treated with hormones at first service, the conception rate were follicular cyst 26%, luteal cyst 64.1%, endometritis 38.7%, mucometra 40%, pyometra 20.5%, respectively. The cumulative conception rates were increased by repeated service follicular cyst 57.3%, luteal cyst 84.6%, endometritis 67%, mucometra 75%, pyometra 64.1%, respectively.

Friction Weldability of Grey Cast Iron - by the Concept of Friction Weld Heat Input Parameter - (회주철의 마찰용접 특성에 관한 연구 - 입열량 이론식을 중심으로 -)

  • Jeong, Ho-Shin;Bang, Kook-Soo
    • Journal of Welding and Joining
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    • v.32 no.3
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    • pp.95-101
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    • 2014
  • Joining of grey cast iron by fusion welding has much difficulties for its extremely low ductility and low toughness because of the flake form of the graphite. And the brittle microstructure, i.e. ledeburite may be formed during fusion welding by its rapid cooling rates. By these kinds of welding problem, preheat and post heat treatment temperature must be increased to avoid weld crack or welding problems. In order to avoid these fusion welding problem, friction welding of cast iron was carried out for improving joint soundness, establishing friction welding variables. There is no factor for evaluating friction weldability in continuous drive type friction welding. In this point of view, this study proposed the parameters for calculating friction weld heat input. The results obtained are as follows ; 1. There was a close relationship between tensile strength and flash appearance of friction welded joint. 2. Tensile strength was decreased and flash was severely oxidized as increasing frictional heating time. 3. As increased forging pressure $P_2$, flash had a large crack and tensile strength was decreased. 4. As powdered graphite by rotational frictional force induced flat surface and hindered plastic flow of metal, tensile strength of welded joint was decreased. 5. Heat input for continuous drive type friction welding could be calculated by the factors of $P_1$, $P_2$ and upset distance(${\delta}$).

A Study on the Corrosion Properties and Microstructure of the Nitrocarburized and Oxidized Low Carbon Steel according to the Treatment Atmospheres (저탄소강의 질화침탄과 산화처리시 분위기 변화에 따른 조직 및 부식특성에 관한 연구)

  • Shin, P.W.;Lee, K.H.;Nam, K.S.;Park, Y.M.;Jo, H.J.
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.2
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    • pp.87-93
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    • 2004
  • Nitrocarburizing was carried out with various $CH_4$ gas composition with 4 torr gas pressure at $570^{\circ}C$ for 3 hours and post oxidation was carried out with 100% $O_2$ gas atmosphere with 4 torr at different temperatures for various time. In the case of plasma nitrocarburizing, It is that the ratio of ${\varepsilon}-Fe_{2-3}$(N, C) and ${\gamma}^{\prime}-Fe_4$(C, N), which comprise the compound layer phase, depend on concentrations of $N_2$ gas and $CH_4$ such that when the concentration of $N_2$ and $CH_4$ increased, the ratio of ${\gamma}^{\prime}-Fe_4$(C, N) decreased, but the ratio of ${\varepsilon}-Fe_{2-3}$(N, C) increased. The thickness of compound layer consistently increased as gas concentration increased regardless of $N_2$ and $CH_4$ expect when the concentration of $CH_4$ was 3.5 volume%, it decreased insignificantly. When oxidizing for 15min in the temperature range of $460{\sim}570{^\circ}C$, the study found small amount of $Fe_3O_4$ at the temperature of $460{^\circ}C$ and also found that amounts of $Fe_2O_3$. and $Fe_3O_4$ on the surface and amount of ${\gamma}^{\prime}-Fe_4$(C, N) in the compound layer increased as the increased over $460^{\circ}C$, but the thickness of the compound layer decreased. Corrosion resistance was influenced by oxidation times and temperature.

Mechanical Properties of Friction Welded SM 45C-SF 45 Joints for Automobile Reverse Idle Gear Shaft Applications (자동차 후진기어용 축재(SM 45C-SF 45)의 이종마찰용접 특성)

  • Kong, Yu-Sik;Yun, Seong-Pil;Kim, Seon-Jin
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.1
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    • pp.85-90
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    • 2010
  • Friction welding is a common practice to join axially symmetrical parts for automobile industry applications. The shaft for automobile reverse idle gear is generally produced by forging steel, SF 45. This method is not so good because of high cost of material and production. In this study, in order to investigate the possibility of application of SM 45C to SF 45 dissimilar friction welding, the dissimilar friction welded joints were performed using 20 mm diameter solid bar in forging steel(SF 45) to carbon steel(SM 45C). The optimal friction welding parameters were selected to ensure reliable quality welds on the basis of visual examination, tensile test, micro-Virkers hardness surveys of the bond of area and optical microstructure investigations for welded joint parts. Finally, post weld heat treatment(PWHT) of the high-frequency induction hardening was performed for the friction welded specimens under the optimal welding conditions. And then, the mechanical properties were compared for as-welded and PWHT in SM 45C to SF 45.

The Effect of Student-Centered Storytelling on Students' Learning Motivation and Attitude in Elementary Science Class (학생 중심 스토리텔링을 활용한 과학 수업이 초등학생의 학습 동기 및 태도에 미치는 영향)

  • Kang, Bu-Mi;Jeon, Kyungmoon
    • Journal of Science Education
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    • v.38 no.3
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    • pp.657-669
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    • 2014
  • The purpose of this research is to investigate the effect of students' storytelling on the science learning motivation and science related attitude in elementary science class. We had developed storytelling materials for 11 class hours on the 'Heat transfer and our life' unit based on the analysis of the 4th grade-science curriculum. The research sample was 22 4th graders who were belonged to one of the classes at an elementary school in Gwangju. The test of students' science learning motivation and science related attitude were administered before and after the storytelling treatment, and the difference was checked by the paired t-test using SPSS program. Students' perceptions on the storytelling were also investigated. The conclusions of this research are as follows. First, the students' storytelling tend to have somewhat positive influence on learning motivation. The each mean of post-test in the domain of attention, confidence and satisfaction was significantly higher than that of pre-test. Second, students' storytelling have a positive influence on scientific attitude. Although the means of post-test were higher than those of pre-test in both science subject attitude and scientific attitude domain, a statistically significant difference was found only in the scientific attitude domain. For future researches, the development of more story-materials or strategies for effective storytelling is needed.

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Reproductive Monitoring and Estrus Induction using Ultrasonography and Hormone Assay in Dairy Cows I. Periodical Examination of Reproductive Status and Treatment of Reproductive Dysfunctions (초음파검사 및 호르몬검사에 의한 젖소 번식검진과 발정유도 I. 정기적인 번식검진 및 번식장애 치료)

  • 오기석;박상국;김방실;고진성;신종봉;백종환;홍기강;문광식;임원호
    • Journal of Veterinary Clinics
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    • v.20 no.3
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    • pp.369-375
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    • 2003
  • The ultrasonography was performed in 77,924 subestrous dairy cows from 680 dairy farms at 57 districts. The cows were examined for confirmation of resumption of ovaries and uterus after 30 days postpartum, for early pregnancy diagnosis after 30 days post-insemination, confirmation of pregnancy at 8 month post-insemination, and for diagnosis of reproductive dysfunctions, respectively. The results of reproductive examination by ultrasonography in 77,924 dairy cows were ovarian disorders 35,452 (46.8%), uterine disorders 10,721 (13.8%), pregnancy and pregnant failure 24,044 (30.8%), adhesion of reproductive tracts 167 (0.2%), freematins 13 (0.01%) and others 6,527 (8.4%) cows, respectively. The 13,732 (49.6%) cows out of 27,694 cows were treated for silent heat or error of estrus detection, 3,473 (12.5%) cows for follicular cysts, 815 (3.0%) cows for luteal cysts, 606 (2.2%) cows for inactive ovaries, 4 (0.01%) cows for granulosa cell tumors, and 6,455 (23.3%) cows for endometritis, respectively. The indices of reproductive efficiencies before (2001-08-10) and after (2003-07-20) periodical examination of reproductive status were as follows; the mean intercalving interval were shortened from 471 days to 383 days, the mean interval calving to conception were shortened from 187 days to 99 days, the mean interval calving to first service were shortened from 105 days to 67 days, the mean cows showing heat by 60 days postpartum were increased from 33% to 89%, the mean conception rate to first service were increased from 43% to 68%, and the mean service per conception were shortened from 2.6 times to 1.8 times, respectively. These results suggest that periodical examination of reproductive status would be useful for the improvement of the reproductive performance in dairy cows.

Numerical Study of the Post Combustion Chamber of Grate Type Incinerator in Daejon 4th Industrial Complex (대전 4공단 소각로 후연소로 모델 연구)

  • Kim Hey-Suk;Shin Mi-Soo;Jang Dong-Soon;Park Byung-Soo;Um Tae-In
    • 한국전산유체공학회:학술대회논문집
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    • 2002.10a
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    • pp.133-138
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    • 2002
  • A 3-D axisymmetric computer program is developed to predict the NO behavior in SNCR system for the stoker incinerator with the waste treatment capacity, 200ton/day. To this end a turbulent reacting flow field calculation is made using proper assumption and empiricism. The stoker bed is assumed to be a homogeneous waste-volatilized gaseous state. The initial composition or reactants are assumed based on the data of the ultimate analysis. Turbulent is resolved by k-e model and turbulent reaction is handled by eddy-breakup model harmonized with empirical chemistry data for gaseous combustion, NO and urea reaction. The liquid droplet is traced by Lagrangian method incorporated by aerodynamic drag, Coriolis and crntrifugal forces. Radiation is treated by sensible heat loss model. Calculation results are in good agreement with experimental data at the outlet of post combustion chamber in Daejon 4th industrial complex. The flue gas shows the temperature range of $900\sim1000^{\circ}C$, velocity of 5m/s and NO concentration of 140ppm at the exit while the measured temperature, flue gas velocity and NO concentration are $967^{\circ}C$, $3\sim4m/s$ and $100\sim200ppm$respectively. Using the developed computer program a parametric study has been made with the variation of heat content of waste, castable length and SNCR variables for the determination of proper injector location. In general, the calculated results are consistent and physically acceptable.

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The Arabidopsis Phytocystatin AtCYS5 Enhances Seed Germination and Seedling Growth under Heat Stress Conditions

  • Song, Chieun;Kim, Taeyoon;Chung, Woo Sik;Lim, Chae Oh
    • Molecules and Cells
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    • v.40 no.8
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    • pp.577-586
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    • 2017
  • Phytocystatins (PhyCYSs) are plant-specific proteinaceous inhibitors that are implicated in protein turnover and stress responses. Here, we characterized a PhyCYS from Arabidopsis thaliana, which was designated AtCYS5. RT-qPCR analysis showed that the expression of AtCYS5 in germinating seeds was induced by heat stress (HS) and exogenous abscisic acid (ABA) treatment. Analysis of the expression of the ${\beta}-glucuronidase$ reporter gene under the control of the AtCYS5 promoter showed that AtCYS5 expression during seed germination was induced by HS and ABA. Constitutive overexpression of AtCYS5 driven by the cauliflower mosaic virus 35S promoter led to enhanced HS tolerance in transgenic Arabidopsis, which was characterized by higher fresh weight and root length compared to wild-type (WT) and knockout (cys5) plants grown under HS conditions. The HS tolerance of AtCYS5-overexpressing transgenic plants was associated with increased insensitivity to exogenous ABA during both seed germination and post-germination compared to WT and cys5. Although no HS elements were identified in the 5'-flanking region of AtCYS5, canonical ABA-responsive elements (ABREs) were detected. AtCYS5 was upregulated in ABAtreated protoplasts transiently co-expressing this gene and genes encoding bZIP ABRE-binding factors (ABFs and AREB3). In the absence of ABA, ABF1 and ABF3 directly bound to the ABREs in the AtCYS5 promoter, which activated the transcription of this gene in the presence of ABA. These results suggest that an ABA-dependent pathway plays a positive role in the HS-responsive expression of AtCYS5 during seed germination and post-germination growth.