• 한국분말재료학회지
• /
• 제21권6호
• /
• pp.454-459
• /
• 2014

In this study, the porous ceramic filter was developed to be able to remove both dust and hazardous gas contained in fuel gas at high temperature. The porous ceramic filters were fabricated and used as a catalyst support. And the effects have been investigated such as the mean particle size, organic content and addition of foaming agent on the porosity, compressive strength and pressure drop of ceramic filters. With the increase of mean powder size and the organic content for the cordierite filter, the porosity was increased, but the compressive strength and pressure drop were decreased. From the results of the research, the optimum condition for the fabrication of ceramic filters could be acquired and they had the porosity of 58%, the compressive strength of 13.4 MPa and the pressure drop of 250 Pa. It was expected that this ceramic filter was able to be applied to the glass melting furnace, combustor, and dust/toxic gas removal filter.

• 설비공학논문집
• /
• 제25권12호
• /
• pp.668-673
• /
• 2013

In this study, specimens with nano-sized porous thin films were manufactured by injecting fluorescence solution into the pores. We intended to find out the difference of the fluorescence intensity in each region of the specimen through an experimental apparatus that makes a temperature field. Before conducting experiments, the optimized manufacturing conditions were determined by analysis of all parameters that influence the emission intensity, and the experiments were carried out with the specimens produced in the optimized conditions. Then, the calibration curves of the fluorescence intensity versus temperature were performed by taking the intensity distributions from the specimen in various temperature fields. The surfaces of specimens were coated with Rhodamine-B (Rh-B) fluorescent dye and measured based on the fluorescence intensity. Silica (SiO2) nanoporous structure with 1-um thickness was constructed on a cover glass, and fluorescence dye was absorbed into these porous thin films.

• 설비공학논문집
• /
• 제25권12호
• /
• pp.674-678
• /
• 2013

We present a non-invasive technique to the measure temperature distribution in nano-sized porous thin films by means of the two-color laser-induced fluorescence (2-LIF) of rhodamine B. The fluorescence induced by the green line of a mercury lamp with the makeup of optical filters was measured on two separate color bands. They can be selected for their strong difference in the temperature sensitivity of the fluorescence quantum yield. This technique allows for absolute temperature measurements by determining the relative intensities on two adequate spectral bands of the same dye. To measure temperature fields, Silica (SiO2) nanoporous structure with 1-um thickness was constructed on a cover glass, and fluorescent dye was absorbed into these porous thin films. The calibration curves of the fluorescence intensity versus temperature were measured in a temperature range of $10-60^{\circ}C$, and visualization and measurement of the temperature field were performed by taking the intensity distributions from the specimen for the temperature field.

• 대한기계학회논문집
• /
• 제12권5호
• /
• pp.1130-1137
• /
• 1988

본 연구에서는 증발분출냉각장치의 설계 및 이의 응용을 위하여 두께가 비교 적 두꺼운(120mm) 다공물질층을 모델로 사용하여 증발분출냉각에 관한 열전달특성을 실험적으로 조사하였다. 실험은 열과 유체의 흐름이 1차원 정상상태에 대하여 증발 영역의 발생과 그 길이 및 상변화위치, 그리고 다공물질층의 표면온도등에 영향을 미 치는 인자들을 조사하며, 아울러 냉각수의 상변화시 다공층내 냉각수 유동의 안정성 여부를 관찰하였다.

• Journal of Applied Biological Chemistry
• /
• 제62권1호
• /
• pp.51-56
• /
• 2019

Biofilms facilitate communication among microorganisms for nutrients and protect them from predators and harmful chemicals such as antibiotics and detergents. Biofilms can also act as cores for the development of clogs in many agricultural irrigation systems and in porous media. In this study, we deployed glass units at a depth of 20 m below the ground surface in the groundwater-surface water mixing zone, and retrieved them after 4 months to investigate the potential colonization of indigenous microbial community and possible mineral-microbe assemblages. We observed the periodic formation of microbial colonies by fluorescence dye staining and microscopy, and analyzed the composition of the microbial community in both the mineral-microbe aggregates and groundwater, by next generation sequencing of the 16S rRNA gene amplicons using MiSeq platform. During the course of incubation, we observed an increase in both the mineral-microbe aggregates and content of extracellular polymeric substances. Interestingly, the microbial community from the aggregates featured a high abundance of iron redox-related microorganisms such as Geobacter sp., Comamonadaceae sp., and Burkholderiales incertae sedis. Therefore, these microorganisms can potentially produce iron-minerals within the sediment-microbe-associated aggregates, and induce biofilm formation within the groundwater borehole and porous media.

• 대한전자공학회논문지
• /
• 제23권5호
• /
• pp.699-705
• /
• 1986

Sb2S3 thin films were fabricated by vacuum evaporation of compound Sb2S3 at a pressure of 10**-5 torr. and in argon ambient. Then, their electrical and photoconductive properties were investigated. The Sb2S3 glass-layer showed maximum photosensitivity at the deposition rate of 250\ulcornersec, and Sb2S3 porous layer had mininum dielectric constant of 1.5 at the deposition rate of 0.3 um/sec and argon partial pressure of 0.2torr. Sb2S3 multi-layers were prepared at the different thickness ratio (B/A) to find the proper structural property suited for camera pick-up tube. Here, A is the sum of the thickness of Sb2S3 porous layer and Sb2S3 fine grain layer, and B is the thickness of Sb2S3 fine grain layer. As a result, photosensitivity had a peak value at the thickness ratio (B/A) of 60%.

• 한국세라믹학회지
• /
• 제30권7호
• /
• pp.535-542
• /
• 1993

It was investigated in this study that a preparation method, activation energy, surface area, pore volume, pore size distribution and DTA analysis of the dry gel in process of producing monolithic porous gel in Li2O-Al2O3-TiO2-SiO2 system by the sol-gel technique using metal alkoxides. Activation energy for gellation according to the variation of water concentration and the kind of catalysts ranged from 10 to 20kcal/mole. Monolithic dry gels were prepared after drying at 9$0^{\circ}C$ when the amount of water for gellation was 4~8 times more than the stoichiometric amount, that was necessary for the full hydrolysis of the mixed metal alkoxide. The specific surface area, the pore volume, the average pore radius of the dried gel at 18$0^{\circ}C$ according to the various kinds of catalyst were about 348~734$m^2$/g, 0.35~0.70ml/g and 10~35$\AA$, respectively. It showed that the dry gels were porous body. As a result ofthe analysis of DTA, it was confirmed that the exothermaic peaks at 715$^{\circ}C$ and 77$0^{\circ}C$ was clue to the crystallization of dried gel.

• Journal of Electrochemical Science and Technology
• /
• 제11권2호
• /
• pp.148-154
• /
• 2020

Highly ordered mesoporous manganese oxide films were electrodeposited onto indium tin oxide coated (ITO) glass using sodium dodecyl sulfate (SDS) and ethylene glycol (EG) which were used as a templating agent and stabilizer for the formation of micelle, respectively. The manganese oxide films synthesized with surfactant templating exhibited a highly mesoporous structure with a long-range order, which was confirmed by SAXRD and TEM analysis. The unique porous structure offers a more favorable diffusion pathway for electrolyte transportation and excellent ionic conductivity. Among the synthesized samples, Mn₂O₃-SDS+EG exhibited the best electrochemical performance for a supercapacitor in the wide range of scan rate, which was attributed to the well-developed mesoporous structure. The Mn₂O₃ prepared with SDS and EG displayed an outstanding capacitance of 72.04 F g^-1, which outperform non-porous Mn₂O₃ (32.13 F g^-1) at a scan rate of 10 mV s^-1.

• 한국세라믹학회지
• /
• 제40권3호
• /
• pp.273-278
• /
• 2003

다공질 세라믹스 흡음재료의 흡음특성과 물리.기계적 특성에 미치는 하수슬러지 슬래그 첨가량과 입경 효과에 대하여 조사하였다. 시편의 물리.기계적 특성은 슬래그 입경과 관계 없이 소성온도가 증가하고 슬래그 함량이 감소함에 따라 증가하였으며, 슬래그의 함량이 일정한 시편은 물유리 첨가량이 증가하고 슬래그 입경이 감소함에 따라 증가하였다. 1~3mm 크기의 슬래그를 약 77~89 wt% 함유하고 1,05$0^{\circ}C$에서 2시간 소성한 시편의 부피비중은 1.48~1.71, 압축강도 85~163 kgf/$\textrm{cm}^2$을 나타내었으며, 1~3mm의 슬래그를 이용한 시편은 저주파영역, 슬래그 입경이 1 mm이하인 시편은 고주파영역의 흡음특성이 향상되었으며, 시편의 두께가 증가함에 따라 저주파영역의 흡음특성이 향상되었다.

• 한국분말재료학회지
• /
• 제26권1호
• /
• pp.40-44
• /
• 2019

Tungsten trioxide ($WO_3$) is a promising candidate as a photocatalyst because of its outstanding electrical and optical properties. In this study, we prepare $WO_3$ thin films by electrodeposition and characterize the photocatalytic degradation of methylene blue using these films. Depending on the voltage conditions (static and pulse), compact and porous $WO_3$ films are fabricated on a transparent ITO/glass substrate. The morphology and crystal structure of electrodeposited $WO_3$ thin films are investigated by scanning electron microscopy, atomic force microscopy, and X-ray diffraction. An application of static voltage during electrodeposition yields a compact layer of $WO_3$, whereas a highly porous morphology with nanoflakes is produced by a pulse voltage process. Compared to the compact film, the porous $WO_3$ thin film shows better photocatalytic activities. Furthermore, a much higher reaction rate of degradation of methylene blue can be achieved after post-annealing of $WO_3$ thin films.