• 제목/요약/키워드: Porosity distribution

검색결과 502건 처리시간 0.023초

크롬탄화물 용사피막의 접착력 및 잔류응력측정에 관한 연구 (A Study on the Adhesion Strength and Residual Stress Measurement of Plasma Sprayed Cr$_3$C$_2$-NiCr Coating)

  • 김의현;김종영
    • Journal of Welding and Joining
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    • 제14권4호
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    • pp.43-52
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    • 1996
  • The plasma sprayed Cr$_{2}$C$_{2}$-NiCr coatings are widely used as wear-resistant and corrosion-resistant materials. The mechanical properties of the plasma sprayed Cr$_{2}$C$_{2}$-NiCr coatings were examined in this study. The distribution of the residual stress with the coating thickness was also examined by X-ray diffraction method. The pore in the coatings could be classified into two types ; one is the intrinsic pore originated from the spraying powder, the other is the extrinsic pore formed during spraying. During the tensile adhesion test, the fracture occurred at the interface of top coat and substrate or top coat and bond coat depending on the existence of bond coat. It was found that the compressive residual stress near the interface decreased with the increase of the top coat thickness. The tensile adhesion strength of the coating without bond coat was higher than that with bond coat, because the coating with bond coat has higher horizontal crack density near the interface between bond coat and top coat.

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미시역학적 유한요소 모델을 이용한 다공성 복합재료의 기공 탄성 인자 산출 (Calculation of Poroelastic Parameters of Porous Composites by Using Micromechanical Finite Element Models)

  • 김성준;한수연;신의섭
    • Composites Research
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    • 제25권1호
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    • pp.1-8
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    • 2012
  • 본 논문에서는 다공성 복합재료의 열탄성 거동 예측을 위하여 미시역학적 유한요소 해석을 통해 기공 탄성 인자를 측정하였다. 먼저 기공 압력에 의한 복합재료의 응력 및 변형 상태를 기술하기 위해서 구성 방정식에 기공 탄성 인자를 도입하였다. 기공 탄성 인자의 산출에 필요한 기공 압력에 의한 팽창 변형도와 기공 형성에 따른 균질화 탄성 계수의 저하를 측정하였다. 기공의 형상, 크기, 배열 형태에 따른 이차원 대표 체적 요소의 모델링과 유한요소 해석을 수행하였다. 기공도, 재료 이 방성이 기공 탄성 인자에 미치는 영향과 기공 압력에 따른 변형 에너지 밀도 분포를 살펴보았다. 또한, 측정된 기공 탄성 인자의 유용성을 검토하기 위하여 탄소/페놀릭 복합재료의 열탄성 거동을 예측하였다.

Wave dispersion properties in imperfect sigmoid plates using various HSDTs

  • Batou, Belaid;Nebab, Mokhtar;Bennai, Riadh;Atmane, Hassen Ait;Tounsi, Abdeldjebbar;Bouremana, Mohammed
    • Steel and Composite Structures
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    • 제33권5호
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    • pp.699-716
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    • 2019
  • In this paper, wave propagations in sigmoid functionally graded (S-FG) plates are studied using new Higher Shear Deformation Theory (HSDT) based on two-dimensional (2D) elasticity theory. The current higher order theory has only four unknowns, which mean that few numbers of unknowns, compared with first shear deformations and others higher shear deformations theories and without needing shear corrector. The material properties of sigmoid functionally graded are assumed to vary through thickness according sigmoid model. The S-FG plates are supposed to be imperfect, which means that they have a porous distribution (even and uneven) through the thickness of these plates. The governing equations of S-FG plates are derived employed Hamilton's principle. Using technique of Navier, differential equations of S-FG in terms displacements are solved. Extensive results are presented to check the efficient of present methods to predict wave dispersion and velocity wave in S-FG plates.

COMPARATIVE ANALYSIS OF STRUCTURAL CHANGES IN U-MO DISPERSED FUEL OF FULL-SIZE FUEL ELEMENTS AND MINI-RODS IRRADIATED IN THE MIR REACTOR

  • Izhutov, Aleksey.L.;Iakovlev, Valeriy.V.;Novoselov, Andrey.E.;Starkov, Vladimir.A.;Sheldyakov, Aleksey.A.;Shishin, Valeriy.Yu.;Kosenkov, Vladimir.M.;Vatulin, Aleksandr.V.;Dobrikova, Irina.V.;Suprun, Vladimir.B.;Kulakov, Gennadiy.V.
    • Nuclear Engineering and Technology
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    • 제45권7호
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    • pp.859-870
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    • 2013
  • The paper summarizes the irradiation test and post-irradiation examination (PIE) data for the U-Mo low-enriched fuel that was irradiated in the MIR reactor under the RERTR Program. The PIE data were analyzed for both full-size fuel rods and mini-rods with atomized powder dispersed in Al matrix as well as with additions of 2%, 5% and 13% of silicon in the matrix and ZrN protective coating on the fuel particles. The full-size fuel rods were irradiated up to an average burnup of ${\sim}60%^{235}U$; the mini-rods were irradiated to an average burnup of ${\sim}85%^{235}U$. The presented data show a significant increase of the void fraction in the U-Mo alloy as the U-235 burnup rises from ~ 40% up to ~ 85%. The effect of irradiation test conditions and U-235 burnup were analyzed with regard to the formation of an interaction layer between the matrix and fuel particles as well as generation of porosity in the U-Mo alloy. Shown here are changes in distribution of U fission products as the U-235 burnup increases from ~ 40% up to ~ 85%.

Sol-Gel 법으로 제조한 알루미나 담체의 $TiO_2$ 복합 한외여과막의 특성 (Characteristics of Alumina-Supported TiO2 Composite Ultrafiltration Membranes Prepared by the Sol-Gel Method)

  • 현상훈;최영민
    • 한국세라믹학회지
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    • 제29권2호
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    • pp.107-118
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    • 1992
  • Alumina supports for TiO2 ultrafiltration membrane coating were prepared by presintering disk-type preforms at 140$0^{\circ}C$. These supports showed uniform microstructures which had the apparent porosity of 40%, the pore size distribution in the range of 0.1~0.5${\mu}{\textrm}{m}$, and the water flux of 1400ι/$m^2$.h at the pressure difference of 10 atm. The optimum pH and concentration of the TiO2 sol for coating were 0.8 and 1.0 wt%, respectively, and sol particles were identified as rutile forms of 20 nm size. Crack-free alumina-supported rutile TiO2 membranes could be prepared through well controlled drying and heating the gel layer coated by the sol-gel dipping. The pore size of the TiO2 membranes heat-treated at 50$0^{\circ}C$ for 2 hrs was 30~80$\AA$, and their thickness varied from 1.1 to 3.8 ${\mu}{\textrm}{m}$ in accordence with the dipping time (4~40 min). The flux of water through this composite membrane at 10 atm was found to be in the range from 800 to 1100ι/$m^2$.hr depending on the dipping time (10~40 min). The membrane thickness increased linearly with the square root of the dipping time and the slope was 0.62 ${\mu}{\textrm}{m}$/{{{{ SQRT { min} }}.

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Polymer Nanofibers for Biomedical Engineering

  • Shin, Min-Kyoon;Kim, Seon-Jeong;Kim, In-Young;Kim, Sun-I.
    • 대한의용생체공학회:의공학회지
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    • 제29권3호
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    • pp.173-178
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    • 2008
  • Recent advancements in the electrospinning method enable the production of ultrafine solid and continuous fibers with diameters ranging from a few nanometers to a few hundred nanometers with controlled surface and morphological features. A wide range of biopolymers can be electrospun into mats with a specific fiber arrangement and structural integrity. These features of nanofiber mats are morphologically similar to the extracellular matrix of natural tissues, which are characterized by a wide pore diameter distribution, a high porosity, effective mechanical properties, and specific biochemical properties. This has resulted in various kinds of applications for polymer nanofibers in the field of biomedicine and biotechnology. The current emphasis of research is on exploiting these properties and focusing on determining the appropriate conditions for electrospinning various biopolymers for biomedical applications, including scaffolds used in tissue engineering, wound dressing, drug delivery, artificial organs, and vascular grafts, and for protective shields in specialty fabrics. This paper reviews the research on biomedical applications of electrospun nanofibers.

시트르산의 양과 소결온도에 따른 (La,Sr)$MnO_3/Gd_{0.2}Ce_{0.8}O_{1.9}$ 계면특성 (Characterization of (La,Sr))$MnO_3/Gd_{0.2}Ce_{0.8}O_{1.9}$ Interface with Citric Acid Contents and Sintering Temperature)

  • 윤일영;윤희성;김병호
    • 한국전기전자재료학회논문지
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    • 제11권1호
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    • pp.18-25
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    • 1998
  • G $d_{0.2}$C $e_{0.8}$ $O_{1.9}$(CGO) for electrolyte and L $a_{0.5}$S $r_{0.5}$Mn $O_3$(LSM50) for cathode in Solid Oxide Fuel Cells(SOFC) were synthesized by citrate process. Specimens were prepared with sintering temperatures at 110$0^{\circ}C$, 120$0^{\circ}C$ and 130$0^{\circ}C$, which were fabricated by slurry coating with citric acid contents. Interfacial resistance was measured between cathode and electrolyte using AC-impedance analyzer. With various citric acid content, the degree of agglomeration for the initial particles changed. Also sintering temperature changed the particle size and the degree of densification of cathode. Factors affecting the interfacial resistance were adherent degree of the electrolyte and cathode, distribution of TPB(three phase boundaries, TPB i.e., electrolyte/electrode/gas phase area) and porosity of cathode. By increasing the sintering temperature, particle size and densification of the cathode were increased. And then, TPB area which occurs catalytic reaction was reduced and so interfacial resistance was increased.sed.sed.d.

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Use of Waste Woods for Developing Environment-friendly Shock-absorbing Materials

  • Kim, Chul-Hwan;Song, Dae-Bin;Lee, Young-Min;Kim, Jae-Ok;Kim, Gyeong-Yun;Shin, Tae-Gi;Park, Chong-Yawl
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 2006년도 PAN PACIFIC CONFERENCE vol.2
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    • pp.475-478
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    • 2006
  • Environment-friendly shock-absorbing materials were made using a vacuum forming method from waste wood collected from local mountains in Korea. The waste wood was pulped by thermomechanical pulping. The TMP cushions showed superior shock-absorbing properties with lower elastic moduli compared to EPS and pulp mold. Even though the TMP cushions made using different suction times had many free voids in their inner fiber structure, their apparent densities were a little higher than EPS and much lower than pulp mold. The addition of cationic starch improved the elastic modulus of the TMP cushions without increasing the apparent density, which was different from surface sizing with starch. The porosity of the TMP cushions was a little greater than EPS and much less than pulp mold. Finally, the TMP cushions have great potential to endure external impacts occurring during goods distribution.

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3차원적층조형법으로 제조된 타이타늄 금속 다공체의 기공구조 및 기계적 특성에 관한 연구 (A Study on Pore Structure and Mechanical Properties of Porous Titanium Fabricated by Three-dimensional Layer Manufacturing Process)

  • 손병휘;홍재근;현용택;배석천;김승언
    • 대한금속재료학회지
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    • 제50권2호
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    • pp.100-106
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    • 2012
  • This study was performed to fabricate porous titanium foam by three-dimensional layer manufacturing process, and to evaluate the porosities, compressive stress, Young's modulus and fracture pattern. Porous titanium foam was made of CP(Commercial Pure) titanium powder (${\leq}5{\mu}m$). Total porosities of titanium foam were in the range of 55-68%. Pore size distribution was $200-440{\mu}m$ for coarse pores, $50-100{\mu}m$ for intermediate pores and $5-10{\mu}m$ for fine pores. Compression elastic modulus and compression stress were decreased with increasing porosity. Young's modulus ranged from 1.04-5.62 GPa and maximum stress ranged from 20-241 MPa. Regarding the mechanical properties, 3D(Three Demensional) porous titanium fabricated layer manufacturing is a promising material for human bone replacement.

Application of the full factorial design to modelling of Al2O3/SiC particle reinforced al-matrix composites

  • Altinkok, Necat
    • Steel and Composite Structures
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    • 제21권6호
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    • pp.1327-1345
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    • 2016
  • $Al_2O_3$/SiC particulate reinforced (Metal Matrix Composites) MMCs which were produced by using stir casting process, bending strength and hardening behaviour were obtained using an analysis of variance (ANOVA) technique that uses full factorial design. Factor variables and their ranges were: particle size $2-60{\mu}m$; the stirring speed 450 rpm, 500 rpm and the stirring temperature $620^{\circ}C$, $650^{\circ}C$. An empirical equation was derived from test results to describe the relationship between the test parameters. This model for the tensile strength of the hybrid composite materials with $R^2$ adj = 80% for the bending strength $R^2$ adj = 89% were generated from the data. The regression coefficients of this model quantify the tensile strength and bending strengths of the effects of each of the factors. The interactions of all three factors do not present significant percentage contributions on the tensile strength and bending strengths of hybrid composite materials. Analysis of the residuals versus was predicted the tensile strength and bending strengths show a normalized distribution and thereby confirms the suitability of this model. Particle size was found to have the strongest influence on the tensile strength and bending strength.