• Title/Summary/Keyword: Plasma test

Search Result 1,363, Processing Time 0.029 seconds

Study on the Effect of Sputtering Process on the Adhesion Strength of CrZrN Films Synthesized by a Duplex Surface Treatment Process (복합표면처리된 CrZrN 박막의 밀착력에 미치는 스퍼터링 효과에 관한 연구)

  • Kim, M.K.;Kim, E.Y.;Lee, S.Y.
    • Journal of the Korean institute of surface engineering
    • /
    • v.39 no.6
    • /
    • pp.268-275
    • /
    • 2006
  • In this study, effect of sputtering on the plasma-nitriding substrate and before PVD coating on the microstucture, microhardness, surface roughness and the adhesion strength of CrZrN thin films were investigated. Experimental results showed that this sputtering process not only removed surface compound layer which formed during a plasma nitriding process but also induced an alteration of the surface of plasma nitrided substrate in terms of microhardness distribution, surface roughness. This in turn affected the adhesion strength of PVD coatings. After sputtering, microhardness distribution showed general decrease and the surface roughness became increased slightly. The critical shear stress measured from the scratch test on the CrZrN coatings showed an approximately 1.4 times increase in the adhesion strength through the sputtering prior to the coating and this could be attributed to a complete removal of compound layer from the plasma nitrided surface and to an increase in the surface roughness after sputtering.

The Study of Corrosion Behavior of Active Screen Plasma Nitrided Stainless Steels

  • Chiu, L.H.;Chang, C.A.;Yeh, S.H.;Chen, F.S.;Chang, Heng
    • Corrosion Science and Technology
    • /
    • v.6 no.5
    • /
    • pp.251-256
    • /
    • 2007
  • Plasma nitriding is a surface treatment process which is increasingly used to improve wear, fatigue and corrosion resistance of industrial parts. Active screen plasma nitriding (ASPN) has both the advantages of the classic cold wall and the hot wall conventional dc plasma nitriding (DCPN) method and the parts to be nitrided are no longer directly exposed to the plasma. In this study, AS plasma nitriding has been used to nitride the UNS S31803 duplex stainless steel, AISI 304 and AISI 316 austenitic stainless steel, and AISI 420 martensitic stainless steel. Treated specimenswere characterized by means of microstructural analysis, microhardness measurements and electrochemical tests in NaCl aerated solutions. Hardness of the nitride cases of AISI 420 stainless steel by Knoop test can get up to 1300 HK0.1. From polarization tests, the corrosion current densities of AISI 420 and UNS S31803specimens ASPN at $420^{\circ}C$ were generally lower than those of their untreated substrates. The corrosion resistance of UNS S31803 duplex stainless steel can be enhanced by plasma nitriding at $420^{\circ}C$ Cowing to the formation of the S-phase.

Test Results of Pulsed Power Supply for Nonthermal Plasma Process (저온 플라즈마 공정용 펄스발생 전원장치의 성능시험)

  • Jang, S.D.;Byun, Y.C.;Cho, M.H.;Shin, D.N.
    • Proceedings of the KIEE Conference
    • /
    • 2011.07a
    • /
    • pp.1574-1575
    • /
    • 2011
  • The application of a pulsed power system is being extended to an environmental and industrial field. The non-destructive gaseous pollutants from industrial plants such as power generation plants and incinerators can be processed by applying high voltage pulses with a fast rising time (a few nanoseconds) and short duration (nano to microseconds) in a pulsed corona discharge reactor. The pulsed plasma generator with a triggered switch has been developed. Its corona current in load can be adjusted by applied voltage and repetition rate. We investigated the performance of the pulsed plasma generator by analyzing the concentration of ozone in small reactor. This paper describes the electrical characteristics of the pulse generator with a voltage of 30 kV at repetition rate of 50 PPS. In addition, we briefly discuss a configuration of the system and initial test results.

  • PDF

Acoustic Emission Characteristics of Ceramic Coated Steel by Plasma Spraying (플래즈머용사에 의한 세라믹 코팅 강재의 음향방출 특성)

  • Kim, G.S.
    • Journal of Power System Engineering
    • /
    • v.2 no.3
    • /
    • pp.49-54
    • /
    • 1998
  • This paper is investigated of hardness and adhesiveness of plasma sprayed coating steels by AE(Acoustic Emission) testing when loading a tensile. AE Parameters used are Event, Count, Energy and Amplitude. Test specimens are carbon steel(S45C) with sprayed coating layers of Ni-4.5wt.%Al(bond coating) and $TiO_2$(top coating), and carry out heat treatment at $800^{\circ}C\;and\;1000^{\circ}C$, respectively. The micro-hardness of the heat treatment specimen have been improved more than that of non-heat treatment. On the tensile test, the process and occurence of the exfoliation of the sprayed coating layer can be estimated by AE Characteristics of AE parameters, such as event, count, amplitude and energy, on the layer exfoliation are shown the similar aspects. The exfoliation of bond coating occure at about 20% of strain and top coating is about 5% of strain.

  • PDF

Improvement of Oxidation Resistance and Erosion Resistance Properties of the C/C Composite with the Multilayer Coating (다층코팅을 이용한 C/C 복합재료의 내산화성 및 내마모성 증진)

  • 김옥희;이승윤;윤병일;박종욱
    • Journal of the Korean Ceramic Society
    • /
    • v.32 no.9
    • /
    • pp.1003-1008
    • /
    • 1995
  • CVD-Si3N4/CVD-SiC/pack-SiC/pyro-carbon/(3-D C/C composite) multilayer coating was performed to improve the oxdiation resistance and erosion resistance properteis of the 3-D carbon/carbon composite, and the plasma test was performed to measure the oxidation resistance and erosion resistance properties. The thicknesses of each film layer were about 10${\mu}{\textrm}{m}$ for pack-SiC, 5${\mu}{\textrm}{m}$ for CVD-SiC and 40${\mu}{\textrm}{m}$ for CVD-Si3N4. When the multilayer coated specimen was exposed to the plasma flame with temperature of 500$0^{\circ}C$ for 20 seconds, it showed the weight loss five times less than that of the only pyro-carbon coated specimen.

  • PDF

Evaluation of the Electrical Resistance between ITO/black interlayer/Bus electrodes in a Plasma Display Panel (플라스마 디스플레이 패널에서 ITO/black interlayer/Bus 전극 간의 전기저항 평가)

  • Moon, Cheol Hee
    • Korean Journal of Metals and Materials
    • /
    • v.46 no.2
    • /
    • pp.97-104
    • /
    • 2008
  • Black interlayer was introduced into between ITO and Bus electrodes to enhance a bright room contrast ratio of a plasma display panel. To measure the electrical resistance of the black interlayer, we designed two test patterns, type I and type II, of which type II pattern was successful. Using type II test pattern, the electrical resistance of the black interlayer was measured to be $300{\Omega}$ for $2{\mu}m$ thickness case and infinitely high for 4, $6{\mu}m$ thickness. This result shows that electrical resistance of the black interlayer in the ITO/black interlayer/Bus electrodes structure is a critical parameter which determines the electrical characteristics of the PDP.

HIP Effects on Mechanical Properties of Oxide Plasma-sprayed Coatings

  • Korobova, N.;Soh, Dea-Wha
    • Journal of the Speleological Society of Korea
    • /
    • no.76
    • /
    • pp.61-66
    • /
    • 2006
  • The present report is the investigation of the effects of the HIP treatment on plasma-sprayed ceramic coating of $Al_2O_3$, $Al_2O_3-SiO_2$ on the metal substrate. These effects were characterized by phase identification, Vickers hardness measurement, and tensile test before and after HIPing.

Effect of Vitamin C Supplementation on Blood Sugar and Serum Lipid in NIDDM Patients (비타민 C 보충이 인슐린 비의존형 당뇨병 환자의 혈당 및 혈청지질에 미치는 영향)

  • Lee, Yun-Mi;Park, Hyoung-Sook
    • The Korean Journal of Rehabilitation Nursing
    • /
    • v.5 no.2
    • /
    • pp.99-112
    • /
    • 2002
  • The purpose of this study is to determine the effect of oral vitamin C supplements on blood sugar and serum lipid level(total cholesterol, triglyceride, high density lipoprotein, low density lipoprotein) in non-insulin independent diabetes mellitus. The study design was a non equivalent control group pre-test post-test design. Data for the study were collected from June 24 to August 31, 2001. The ninty-five research subject were assigned to experimental group(51) and control group(44). Vitamin C(3g/day) was given to 51 subjects for 4 weeks. Following a 12h overnight fasting, blood sample was obstaind at baseline and at the end of 4week - supplementation. Blood samples were taken for plasma vitamin C concentration, fasting blood sugar, HbA1c and serum lipid level. The pre-equivalent test was used by Chi-squre, t-test and two group's pre and post experimental differences were analyzed by t-tset to compare with each other. The results of this study were as follows ; 1. The difference between the two groups in plasma vitamin C concentration was significant(t=-12.950, p=.000). 2. The difference between the two groups in fasting blood sugar was significant(t=5.293, p=.000). 3. The difference between the two groups in HbA1c was not significant(t=1.758, p=.082). 4. The difference between the two groups in total cholesterol, HDL, LDL was significant(t=3.786, p=.000 ; t=-5.515, p=.000 ; t= 4.169, p = .000). These results suggest that megadose vitamin C supplementation be effective in lowering fasting blood sugar, serum lipids and increasing plasma vitamin C. Thus dietary measures to increase plasma vitamin C may be on important health strategy for reducing the compliance of diabetic patients.

  • PDF

The Regeneration Effect of Platelet-Rich Plasma on the Treatment of Grade II Furcation Involvement Using Synthetic Bone in Human (2급 치근이개부 병변의 합성골 이식 시 혈소판 농축 혈장의 재생에 관한 효과)

  • Kim, Jun-Hee;Lim, Sung-Bin;Chung, Chin-Hyung
    • Journal of Periodontal and Implant Science
    • /
    • v.31 no.2
    • /
    • pp.477-488
    • /
    • 2001
  • The present study evaluated of regeneration effect of platelet rich plasma on the treatment of grade II furcation involvement, with coralline calcium phosphate bone in humans. 30 teeth with grade II furcation defect were selected and 15 teeth(control) were treated with coralline calcium phosphate bone, the others(test) were treated with coralline calcium phosphate bone and platelet rich plasma. Pocket depth, clinical attachment level, width of keratinized gingiva width were measured at baseline, postoperative 3, 6months. from cementoenamel junction to alveolar crest and fundus were measured at baseline, 6months(re-entry). Both groups were statistically analyzed by Wilcoxon signed Ranks Test & Mann-whitney Test using SPSS program(5% significance level). The results were as follows: 1. Pocket depth, clinical attachment level, keratinized gingva width, cementoenamel junction - alveolar crest, cementoenamel junction - fundus were not differ significantly in both groups at baseline 2. The change of pocket depth, clinical attachment level, keratinized gingva width, cementoenamel junction - alveolar crest, cementoenamel junction - fundus in both groups were decreased significantly at 3, 6months(p<0.05). 3. The change of pocket depth, clinical attachment level in test group decreased significantly than control at 3, 6months(p<0.05). 4. The change of keratinized gingiva width, cementoenamel junctional - alveolar crest, cementoenamel junction - fundus were not differ significantly in both groups at 3, 6months. 5. The pocket depth, clinical attachment level, keratinized gingiva width exhibited marked changes at 3 months in both groups. In conclusion, the results of this study suggest that platelet rich plasma have adjunctive clinical treatment effect to periodontal regeneration in grade II furcation defects.

  • PDF

Analysis of Trace Level and Correlation of Lead in the Plasma of Field Workers and General Public by ICP-MS (유도결합플라즈마 질량분석법에 의한 납 취급 근로자와 일반인의 혈장 중 납 분석 및 상관성 분석)

  • Lee, Sung-Bae;Yang, Jeong-Sun;Choi, Sung-Bong;Kim, Nam-Soo;Lee, Byung-Kook;Shin, Ho-Sang
    • Journal of Korean Society of Occupational and Environmental Hygiene
    • /
    • v.23 no.2
    • /
    • pp.65-74
    • /
    • 2013
  • Objectives: This study attempted to develop a method to measure ultra-trace lead concentrations in plasma using Inductively Coupled Plasma Mass Spectrometry(ICP-MS) and to test whether plasma lead can be used as a biomarker for the biological monitoring of exposure to lead. Methods: Lead concentrations in 160 plasma samples of field workers and 42 plasma samples from the control group were measured by ICP-MS. Blood zinc protophorphyrin(ZPP) concentrations and urinary ${\delta}$-aminolevulinic acid${\delta}-ALA$) were measured for correlation analysis with plasma lead. Results: The mean lead level in the plasma of the workers exposed to lead at work were 786.1 ng/L. Plasma lead levels were not correlated with blood ZPP or urinary ${\delta}-ALA$ concentrations. Otherwise, plasma lead levels showed a good correlation coefficient of 0.400 with blood lead levels, and their correlation coefficient had a better value of 0.552 for the non-smoking and drinking group. In the general population group which was not exposed to lead in the workplace and was considered the control group, the mean concentration of plasma lead was 123.1 ng/L. The plasma lead levels for the general population group showed a good correlation coefficient of 0.520 with blood ZPP and urinary ${\delta}-ALA$ concentrations.