Browse > Article

Study on the Effect of Sputtering Process on the Adhesion Strength of CrZrN Films Synthesized by a Duplex Surface Treatment Process  

Kim, M.K. (Center for Advanced Plasma Surface Technology)
Kim, E.Y. (Center for Advanced Plasma Surface Technology)
Lee, S.Y. (Center for Advanced Plasma Surface Technology)
Publication Information
Journal of the Korean institute of surface engineering / v.39, no.6, 2006 , pp. 268-275 More about this Journal
Abstract
In this study, effect of sputtering on the plasma-nitriding substrate and before PVD coating on the microstucture, microhardness, surface roughness and the adhesion strength of CrZrN thin films were investigated. Experimental results showed that this sputtering process not only removed surface compound layer which formed during a plasma nitriding process but also induced an alteration of the surface of plasma nitrided substrate in terms of microhardness distribution, surface roughness. This in turn affected the adhesion strength of PVD coatings. After sputtering, microhardness distribution showed general decrease and the surface roughness became increased slightly. The critical shear stress measured from the scratch test on the CrZrN coatings showed an approximately 1.4 times increase in the adhesion strength through the sputtering prior to the coating and this could be attributed to a complete removal of compound layer from the plasma nitrided surface and to an increase in the surface roughness after sputtering.
Keywords
Duplex surface treatment; Plasma nitriding; PVD coating; Adhesion strength; CrZrN thin film;
Citations & Related Records
연도 인용수 순위
  • Reference
1 배규호, Plasma/Ion Nitride treatment, Dangoon (1996) 92
2 S. J. Won, B. S. Lim, J. Y. Ha, K. S. Nam, KASE, (2000)
3 B. Edenhofer, Heat. Treat. Met., 2 (1974) 59-67
4 T. Arai, H. Fujita, M. Watanabe, Thin Solid Films, 154 (1987) 387-401   DOI
5 S. Y. Lee, S. D. Kim, Y. S. Hong, Surf. Coat. Technol., 193 (2005) 266-271   DOI
6 S. Ma, Y. Li, K. Xu, Surf. Coat. Technol., 137 (2001) 116-121   DOI
7 M. T. Laugier, Thin Solid Films, 117 (1984) 243-249   DOI   ScienceOn
8 Y. Sun, T. Bell, Trans. Inst. Met. Finish., 70(1) (1992) 38-44   DOI
9 S. J. Bull, Failure Modes in Scratch Adhesion Testing, Surf. Coat. Technol., 50 (1991) 25-32   DOI   ScienceOn
10 K.- T. Rie, E. Broszeit, Surf. Coat. Technol., 76-77 (1995) 425-436