• Title/Summary/Keyword: Physical property test

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A comparative study of electroplating and electroless plating for diameter increase of orthodontic wire (교정용 선재의 직경 증가를 위한 전기도금법과 무전해도금법의 비교연구)

  • Kim, Jae-Nam;Cho, Jin-Hyoung;Sung, Young-Eun;Lee, Ki-Heon;Hwang, Hyeon-Shik
    • The korean journal of orthodontics
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    • v.36 no.2 s.115
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    • pp.145-152
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    • 2006
  • The purpose of this study was to evaluate electroless plating as a method of increasing the diameter of an orthodontic wire in comparison with eletroplating. After pretreatment plating of the 0.016 inch stainless steel orthodontic wire, electroless plating was performed at $90^{\circ}C$ until the diameter of the wire was increased to 0.018 inch. During the process of electroless plating, the diameter of the wire was measured every 5 minutes to examine the increasing ratio of the wire's diameter per time unit. And to examine the uniformity, the diameter at 3 points on the electroless-plated orthodontic wire was measured. An X-ray diffraction test for analyzing the nature of the plated metal and a 3-point bending test for analyzing the physical property were performed. The electroless-plated wire group showed a increased tendency for stiffness, yield strength, and ultimate strength than the electroplated wire group. And there was a statistically significant difference between the two groups for stiffness and ultimate strength. In the electroless-plated wire group, the increasing ratio of the diameter was $0.00461{\pm}0.00003mm/5min$ (0.00092 mm/min). In the electroplated wire group, it was $0.00821{\pm}0.00015mm/min$. The results of the uniformity test showed a tendency for uniformity in both the plating methods. The results of this study suggest that electroless plating of the wire is closer to the ready-made wire than electroplating wire in terms of the physical property. However, the length of plating time needs further consideration for the clinical application of electroless plating.

Physical Property of W-C-N Diffusion Barrier through Stress-Strain curve (Stress-Strain curve를 이용한 W-C-N 확산방지막 물성 특성 연구)

  • Lee, Kyu-Young;Kim, Soo-In;Park, Sang-Jae;Lee, Dong-Kwan;Jeong, Yong-Rok;Jung, Jun;Lee, Jong-Rim;Lee, Chang-Woo
    • Journal of the Korean Vacuum Society
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    • v.20 no.4
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    • pp.266-270
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    • 2011
  • This paper suggest tungsten (W)-carbon (C)-nitrogen (N) thin films for diffusion barrier that W is main material and C and N are additives. W-C-N thin films are deposited with fixed rates of W and C but with a variation of $N_2$ gas flow and W-C-N thin films are heated at $600^{\circ}C$. From the experimental results, the variation of elastoplastic region for W-C-N thin film measured by tribological property is larger than that of elastic region with a variation of $N_2$ gas flow. These results show that the $N_2$ gas flow is more directly related with the elastoplastic region of W-C-N thin film. Nanoindenting test executed 16 times consecutively and we got the stress-strain curve graphs and hardness datas at each sample. Through the stress-strain curve graphs, the standard diviation of stress-strain curve for $N_2$ gas flow rate of 2.0 sccm is smaller than that of 0, 0.5, 1.5 sccm. Consequently, the physical stability of W-C-N thin film depends on the flow rate of $N_2$ gas.

A Study on the Calculation of Consolidation Constants using Moisture Content of Sedimentary Clay in Busan and Gyeongnam Regions (부산·경남지역 퇴적 점토의 함수비를 이용한 압밀정수 산정 연구)

  • Sung-Uk Kang;Dae-Hwan Kim;Tae-hyung Kim;Chin-Gyo Chung;In-Gon Joo
    • Journal of the Korean Geosynthetics Society
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    • v.23 no.1
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    • pp.39-47
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    • 2024
  • In this study, physical property tests and standard consolidation tests were conducted on the marine clay of Busan New Port and North Port, the middle and lower reaches of the Nakdong River including Gimhae and Yangsan, and Ulsan regions. The moisture content, a property unrelated to sample disturbance with small individual test errors, was used for regression analysis with the compression index, virgin compression index, consolidation coefficient, expansion index, and secondary compression index, among others. Subsequently, the correlation and accuracy were evaluated. Upon analyzing the correlation between the moisture content, void ratio, and liquid limit commonly used physical properties for calculating compression indexes, it was confirmed that the liquid limit had the lowest correlation. Through a linear regression analysis of the consolidation constants using the current moisture content in the natural state, a high correlation was demonstrated. Relationship equations were then presented to determine settlement and settlement time. This study suggests that moisture content can be utilized as an alternative for evaluating and calculating consolidation constants when examining ground settlement in sedimentary clays distributed in the Busan and Gyeongnam regions.

A STUDY ON THE PHYSICAL PROPERTIES AND BIOLOGICAL CHARACTERISTICS OF DENTAL MAGNETIC ATTACHMENTS (치과용 자석부착장치의 물리적, 생물학적 특성에 관한 연구)

  • Lim, Yong-Sik;Kim, Yung-Soo;Kim, Chang-Whe;Kim, Yong-Ho
    • The Journal of Korean Academy of Prosthodontics
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    • v.37 no.1
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    • pp.1-22
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    • 1999
  • In order to investigate various physical and biological properties of dental magnetic attachments studies on retentive characteristics, corrosion properties, cytotoxicity of different magnetic systems for dental applications were done. For the study of retentive characteristics changes of retentive force by increasing air gap, wear properties of various attachment systems and loss of magnetic force by heat treatment were measured. Forte study of corrosion property of magnet covering metal electrochemical corrosion was done in artificial saliva and 0.9% NaCl solution between $-1,000mV_{SCE}\;and\;+1,000mV_{SCE}$. Anodic polarization curves are obtained about 6 types of samples and 2 types of solution. Corroded surfaces were examined with metallurgical microscope, scanning electron microscope and surface profilometer. For the study of cytotoxicity of magnetic attachment and its field cell growth and agar overlay test were done. The results of this study were as follows. 1. In Magnetic attachments using closed circuit retentive force at zero air gap was greater than magnets using open circuit, but decrease of retentive force by increasing air gap was also greater than open systems. 2. After 40,000 cycles of wear test all mechanical attachment resulted in varing degree of retention loss but in magnetic attachments no loss of retentive force was observed. 3. The magnetic attachment using Neodymium magnet showed early loss of retentive force about $200^{\circ}C$ but attachment using Samarium magnet showed some resistance to heat treatment and complete retention loss was observed about $500^{\circ}C$. The keeper was not influenced by heat treatment in retention. 4. In electrochemical corrosion test Dyna magnetic attachment covering metal showed the highiest corrosion resistance and Shiner magnet covering metal showed the least corrosion resistance and examination of corroded surface with metallurgical microscope, scanning electron micro-scope and surface profilometer also showed same results with anodic polarization corves. 5. The result of cell culture tests on the magnet covered with metal showed least recognizable cytotoxicity.

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Estimation of Soft Ground Piezocone Factors at Gwangyang, Jeonnam (전남 광양지역 연약지반의 피에조콘계수 산정)

  • Oh, Dongchoon;Kim, Kibeom;Baek, Seungcheol
    • Journal of the Korean GEO-environmental Society
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    • v.20 no.2
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    • pp.59-67
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    • 2019
  • Using the results from laboratory soil test, field vane test and piezocone penetration test, the engineering characteristics of the soft ground at east side of Gwangyang Port, which is located at south coast of Jeollanam-do, were investigated and optimal piezocone penetration test depth was derived to calculate piezocone factor. In this paper, the results of 61 laboratory soil tests, 226 times of field vane tests and 26 piezocone penetration tests were used. The result of laboratory soil test suggested that some physical properties such as specific gravity, moisture content, liquid limit and plastic index and others are higher than other south coast regions, meanwhile uniaxial compression strength, undrained shear strength, defined as mechanical property, appeared to be relatively small, distributed widely. According to the plastic chart, the ground was classified as high compressibility clay and low compressibility clay, mostly represent to Type 3 clay by Robertson (1990)'s classification chart. Piezocone factor was calculated by empirical method, based on the undrained shear strength which was obtained by the field vane test. According to the analysis with 3 different depth range, to set the appropriate measured depth range of piezocone penetration for comparation, using average value of the range of 5 times the vane length showed the highest correlation.

Aggregate Utilization Estimation of River Sand according to Typical Location of Main Stream of Nakdong-River (낙동강 본류의 대표위치별 하천모래의 골재 활용성 평가)

  • Park, Jae-Im;Bae, Su-Ho;Kwon, Soon-Oh;Kim, Chang-Duk;Lee, Seung-Han
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.8
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    • pp.3719-3725
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    • 2012
  • Due to the recent shortage of well-graded river sand resulting from a rapid growth of concrete construction, sea sand, crushed sand, and etc. are increasingly used instead. It is, however, well noted that non-washed sea sand leads to corrosion of the reinforcing steel in concrete, and thus eventually results in damage to concrete. Also, the crushed sand is not being widely used, since it is difficult to maintain the allowable amount of passing 0.08mm sieve and to adjust grading. On the other hand, because the fine sand of Nakdong-River has a poor grading but good quality as a fine aggregate for concrete, it is strongly needed to investigate the fine sand as an alternative fine aggregate. Thus, the purpose of this research is to evaluate the physical properties of the fine sand of Nakdong-River to utilize it actively as a fine aggregate. For this purpose, after the sand samples were collected according to typical location of main stream of Nakdong-River, the physical properties such as density in oven-dry condition, grading, unit volume mass, and etc. of them were estimated. It was observed from the test results that physical properties of the fine sand of Nakdong-River except grading were found to be excellent.

Experimental Study on the Thermal Characteristics According to the Content Change of Biodiesel Mixture (바이오디젤 혼합물의 함량변화에 따른 열적 특성에 대한 실험적인 연구)

  • Ju Suk Kim;Jae Sun Ko
    • Journal of the Society of Disaster Information
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    • v.19 no.3
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    • pp.532-544
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    • 2023
  • Purpose: To identify and evaluate the risk of chemical fire causative substances by using thermal analysis methods (DSC, TGA) for the hazards and physical property changes that occur when newly used biofuels are mixed with existing fuels It is to use it for identification and evaluation of the cause of fire by securing data related to the method and the hazards of the material according to it. Method: The research method used in this experiment is the differential scanning calorimeter (DSC: Difference in heat flux) through quantitative information on the caloric change from the location, shape, number, and area of peaks. flux) was measured, and the weight change caused by decomposition heat at a specific temperature was continuously measured by performing thermogravimetric analyzer (TGA: Thermo- gravimetric Analyzer). Result: First, in the heat flux graph, the boiling point of the material and the intrinsic characteristic value of the material or the energy required for decomposition can be checked. Second, as the content of biodiesel increased, many peaks were identified. Third, it was confirmed through analysis that substances with low expected boiling points were contained. Conclusion: It was shown that the physical risk of the material can be evaluated by using the risk of biodiesel, which is currently used as a new energy source, through various physical and chemical analysis techniques (DSC + TGA).In addition, it is expected that the comparison of differences between test methods and the accumulation and utilization of know-how on experiments in this study will be helpful in future studies on physical properties of hazardous materials and risk assessment of materials.

Drying Characteristics and Drying Model of Red Pepper (고추의 건조특성(乾燥特性)과 건조모델에 관(關)한 연구(硏究))

  • Cho, Y.J.;Koh, H.K.
    • Journal of Biosystems Engineering
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    • v.11 no.1
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    • pp.52-63
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    • 1986
  • This study was performed to find out drying characteristics and develop drying model for the design of an efficient dryer or drying system of red peper. The basic model which describes drying phenomenon of red pepper was firstly established, and drying tests were conducted at 14-different drying conditions. In this test, the effects of drying air temperature and relative humidity on the rate of drying were undertaken. Finally, a new drying model based on these experimental results was developed to describe the drying characteristics of red pepper. The results from this study may be summarized as follows. 1. Drying constant of the basic model established from Lewis' experimental model and diffusion equation was theoretically deduced as a function of moisture content and inner-temperature of red pepper. 2. From the results of drying tests, drying air temperature was found to have the greatest effect on the rate of drying. However, the effect of temperature was small for the condition of high relative humidity, and for low temperature, the effect of relative humidity was found to be large even though the range of relative humidity was low. 3. Modified Henderson equation was found to be better than Chung equation as the EMC model for the estimation of the equilibrium moisture content of red Pepper. 4. Constant-rate drying period did not exist in the red pepper drying test. And falling-rate drying period was divided into three distinct phases. Drying rate was dependent on the moisture content, the inner-temperature of red pepper and the change of physical property due to drying. 5. Drying constant increased with decrease of free moisture content, but it decreased at the end of the drying period. Also, drying constant was dependent on the drying air temperature and relative humidity. 6. The new drying model developed in this study was found to be most suitable in describing the drying characteristics of red pepper. Therefore, it may be concluded that drying time could be accurately estimated by the new drying model.

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A Study on the Indoor Climate Characteristics and Thermal Sensation Vote of the Earthen House in Summer Season (흙집의 하절기 실내 물리적 환경 특성과 온열감에 관한 연구)

  • Chan, Kook;Jeon, Ji-Hyeon;Shin, Yong-Gyu
    • Journal of the Korean housing association
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    • v.17 no.5
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    • pp.9-16
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    • 2006
  • The researches on the environmental friendly buildings have carried out on the materials, environmental property, technical elements and etc., and various buildings with these green materials have built and under construction nowadays and became a new trend of the green building. And recently, new building technique which builds the wall with the soil and wood and very easy to construct (called M Earthen House) was introduced as the green building and rapidly propagated. But the research on the indoor climatic characteristics, the ability to control the environmental comfort and the influence to the human beings of these buildings are not sufficiently identified yet. In this paper, the indoor environmental characteristics and the temperature controlling ability of these buildings in summer season were measured and analysed by the Portable Indoor Air Quality Monitor(BABUC/A, LSI) measuring equipments, ana the subjective test on the thermal environment of the subjects were carried out to evaluate the thermal comfort. The results can be summarized as follows; 1) Compared to the outdoor dry bulb temp.($15.4{\sim}28.7^{\circ}C$), the indoor temp. was $19.5{\sim}26.8^{\circ}C$. It showed the temperature controlling ability of the M earthen house was outstanding. And the indoor relative humidity, compared to the outdoor($45.4{\sim}100%$), was $58.1{\sim}76.4%$, it showed the humidity controlling ability of the M earthen house was also outstanding. 2) The thermal environment was evaluated as 'comfort'(neutral-slightly warm) and the humidity was also evaluated as 'comfort'(neutral-slightly humid). So, the results of the physical and subjective evaluation on the indoor thermal comfort in summer season were 'neutral' and 'comfort' coincidently, it was confirmed that the controlling ability of the indoor temperature and humidity of the M earthen house was very excellent.

Enhancement of antimicrobial properties of shoe lining leather using chitosan in leather finishing

  • Mahmud, Yead;Uddin, Nizam;Acter, Thamina;Uddin, Md. Minhaz;Chowdhury, A.M. Sarwaruddin;Bari, Md. Latiful;Mustafa, Ahmad Ismail;Shamsuddin, Sayed Md.
    • Advances in materials Research
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    • v.9 no.3
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    • pp.233-250
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    • 2020
  • In this study, a chitosan based coating method was developed and applied on the shoe lining leather surface for evaluating its inhibition to bacterial and fungal attacks. At first, chitosan was prepared from raw prawn shells and then the prepared chitosan solution was applied onto the leather surface. Secondly, the characterization of the prepared chitosan and chitosan treated leather was performed by solubility test, ATR-FTIR, XRD pattern, SEM and TGA. Evaluation of antimicrobial efficacy of chitosan was assessed against two gram positive, two gram negative bacteria and a reputed fungi by agar diffusion test. The results of this study demonstrated that chitosan took place in both the surface of collagen fibres and inside the collagen matrix of crust leather. The chitosan showed strong antimicrobial activities against all the tested microorganisms and the inhibition increased with increasing percentage of chitosan. Therefore, the prepared chitosan in this study can be an environment friendly biocide, which functions simultaneously against different spoilage bacteria and fungi on the finished leather surface. Thus by using the prepared chitosan in shoe lining leather, the possibility of microbial attack during shoe wearing can be minimized which is one of the important hygienic requirements of footwear.