• Journal of the Korean Applied Science and Technology
• /
• v.20 no.2
• /
• pp.118-124
• /
• 2003

Silver nanoparticles was synthesized by the method of W/O microemulsions with AOT (bis(2-ethylhexyl) sodium sulfosuccinate). The nucleation particle growth and aggregation was controlled by the droplet exchange process. The intermicellar exchange reaction is varied by changing the AOT and the $H_2O$ concentration. The synthesized W/O microemulsions was found to give the nanoparticles, which was confirmed by SEM, TEM, particle-size-analyzer, and UV-spectrometer. The most stable particles was obtained at 0.056 mole AOT solution, and the particle size distribution was found in the range from 27 to 31 nm. The mean particle size was reduced by adding Tween 20 significantly, and distribution was found from 14 to 16 nm. And, It's size was reduced by cosurfactants as toluene and benzyl alcohol. In case of toluene and benzyl alcohol, the range of particle size was found 7${\sim}$11 nm and 8${\sim}$12 nm.

• Korean Chemical Engineering Research
• /
• v.54 no.2
• /
• pp.278-283
• /
• 2016

In this study, we have for the first time applied fractional precipitation with hydrophilic polymer in order to decrease the particle size of the anticancer agent paclitaxel from plant cell cultures. When compared with the case where no hydrophilic polymer was employed, the addition of hydrophilic polymer in fractional precipitation resulted in a decrease in the size of the paclitaxel precipitate. Among the polymers used, HPMC 2910 was the most effective for inhibition of precipitate growth. A polymer concentration of 0.2% (w/v) obtained the smallest particle size. The particle size was reduced by ~35% compared to control. In addition, the precipitate size was inversely correlated with the absolute value of the zeta potential.

• Journal of the Korean Ceramic Society
• /
• v.35 no.10
• /
• pp.1055-1060
• /
• 1998

The effects of particle size distribution have been investigated on the high frequency low loss Mn-Zn fer-rites. The particle size distribution was controlled by milling time. Zirconia ball and engineering plastic jar were employed to avoid iron contamination from the milling media. As increasing the milling time BET value was increased from 0.55 to 3.21m2/g and mean particle size was decreased from 2.1 $\mu\textrm{m}$ to 1.0$\mu\textrm{m}$ The large specific surface area of initial powder resulted in the high density of sintered core. However starting powders with high BET lead to inhomogeneous grain growth as well as poor electromagnetic pro-perties at sintering temperature above 1300$^{\circ}C$.

• Journal of Institute of Control, Robotics and Systems
• /
• v.17 no.11
• /
• pp.1095-1100
• /
• 2011

In this paper, PHM (Prognostics and Health Management) techniques are briefly outlined. Prognostics, being a central step within the PHM, is explained in more detail, stating that there are three approaches - experience based, data-driven and model based approaches. Representative articles in the field of prognostics are also given in terms of the type of faults. Model based method is illustrated by introducing a case study that was conducted to the crack growth of the gear plate in UH-60A helicopter. The paper also addresses the comparison of the OBM (Overall Bayesian Method), which was developed by the authors with the PF (Particle Filtering) method, which draws great attention recently in prognostics, through the study on a simple crack growth problem. Their performances are examined by evaluating the metrics introduced by PHM society.

• Journal of the Korean Ceramic Society
• /
• v.37 no.2
• /
• pp.152-157
• /
• 2000

Si3N4/SiC nanocomposite ceramics containing 5 wt%dispersed SiC particles were prepared by gas-pressure-sintering at 200$0^{\circ}C$ under nitrogen atmosphere. SiC particles with average sizes of 0.2 and 0.5${\mu}{\textrm}{m}$ were used, and the effect of the SiC particle size on the microstructure was investigated. The addition of SiC particles effectively suppressed the growth of the Si3N4 matrix grains. The effect of grain growth inhibition was higher in the nanocomposites dispersed with fine SiC. SiC particles were dispersed uniformly inside Si3N4 matrix grains and on grain boundaries. When the fine SiC particles were added, large fraction of the SiC particles was trapped inside the grains. On the other hand, when the large SiC particles were added, most of the SiC particles were located on grain boundaries. Typically, the fraction of SiC particles located at grain boundaries was higher in the specimen prepared from $\beta$-Si3N4 than in the specimen prepared from $\alpha$-Si3N4.

• Journal of the Korean Ceramic Society
• /
• v.50 no.6
• /
• pp.489-494
• /
• 2013

Nano-sized titanium oxide powders were synthesized by a polymer matrix technique using pulp and Titanium tetraisopropoxide (TTIP) as starting materials. The synthesized powders were characterized by XRD and FE-SEM. The particle size of the powders was controlled by preparation conditions, such as heat treatment temperature and time. After investigating various drying and heat treatment conditions, 50-100 nm sized homogeneous titanium oxide particles were obtained by treating at $600^{\circ}C$ for 1 h. The crystallization and rapid growth of particles was accelerated by increasing heat treatment temperature and time. Anatase phase generated below $600^{\circ}C$ transformed to the rutile phase with increasing heat treatment temperature. Moreover, above $800^{\circ}C$, heat treatment time had a very large influence on particle growth, and changing the heating condition also had a large influence on crystal growth.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.6 no.1
• /
• pp.11-18
• /
• 1996

Grown-in defects like OISF and FPD in the large diameter(> 8 inch)of silicon crystal are characterized. It was revealed that the presence of the ring-patterned OISF would deterorate the minority life time of the silicon crystal. Through the cooling experiment from the $1250^{\circ}C$, the nucleation of the OISF was confirmed to follow the homogeneous nucleation and growth process. In addition to OISF nucleus, crystal originated particle, which was known to be closely related with FPD (Flow Pattern Defects), was found to depend on the pulling rate of the crystal. Combination of the lower rate of the pulling and the faster cooling near the $950^{\circ}C$ is proposed to be effective method in reducing the generation of these grown-in defects.

• Composites Research
• /
• v.22 no.3
• /
• pp.74-81
• /
• 2009

Reversed plane bending fatigue tests were conducted on SiC particle reinforced and SiC whisker reinforced aluminum composite. The initiation and growth behaviors of small surface fatigue cracks were continuously monitored by the replica technique and the causes of fracture and fracture mechanism were investigated by SEM. The relationship between da/dn and $K_{max}$ show that da/dn increases in high stress level while decrease and again increases with increasing of $K_{max}$ in low stress level for two materials.

• 한국정보디스플레이학회:학술대회논문집
• /
• 2002.08a
• /
• pp.674-677
• /
• 2002

Vertically aligned CNTs were grown on Fe-deposited $SiO_2$ substrates using thermal CVD of acetylene gas. The size of Fe particle is controlled by the flow rate of $NH_3$ and pretreatment time, which leads to control the diameter of CNTs. As the diameter of CNTs decreases, the growth rate is enhanced with an inverse dependence of the CNT diameter. The growth rate of CNTs increases linearly as the growth time increases until 30 min but is rapidly decreased over 40 min. We found an inverse relation between the diameter and growth rate of carbon nanotubes. As the diameter of CNTs increases, the compartment layers of bamboo-shaped CNTs appear more frequently. A base-growth model is suitable to explain the dependence of growth rate and structure of CNTs on the diameter size of catalytic particles.

• Tunnel and Underground Space
• /
• v.23 no.6
• /
• pp.470-479
• /
• 2013

Hydraulic fracturing is used as a method for promoting the fluid flow in the rock and, in the energy field such as geothermal development and the development of sales gas, many studies has been actively conducted. In many cases, hydraulic fracturing is not performed in isotropic rock and especially in the case of sedimentary rocks, hydraulic fracturing is conducted in the transverse isotropic rock. The direction of the crack growth on hydraulic fracturing does not necessarily coincides with the direction of maximum principal stress in the transverse isotropic rock. Therefore, in this study, bonded particle model with hydro-mechanical coupling analysis was adopted for analyzing the characteristics of hydraulic fracturing in transverse isotropic rock. In addition, experiments of hydraulic fracturing were conducted in laboratory-scale to verify the validity of numerical analysis. In this study, the crack growth and crack patterns showed significant differences depending on the viscosity of injection fluid, the angle of bedding plane and the influence of anisotropy. In the case of transverse isotropic model, the shear crack growth due to hydraulic fracturing appeared prominently.