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http://dx.doi.org/10.4191/kcers.2013.50.6.489

Preparation of Nano-sized Titanium Oxide Powder Using Natural Polymer Matrix  

Kim, Soo-Jong (Department of Advanced Materials & Chemical Engineering, Halla University)
Han, Cheong-Hwa (Department of Advanced Materials & Chemical Engineering, Halla University)
Shim, Jae-Ho (Department of Advanced Materials & Chemical Engineering, Halla University)
Publication Information
Journal of the Korean Ceramic Society / v.50, no.6, 2013 , pp. 489-494 More about this Journal
Abstract
Nano-sized titanium oxide powders were synthesized by a polymer matrix technique using pulp and Titanium tetraisopropoxide (TTIP) as starting materials. The synthesized powders were characterized by XRD and FE-SEM. The particle size of the powders was controlled by preparation conditions, such as heat treatment temperature and time. After investigating various drying and heat treatment conditions, 50-100 nm sized homogeneous titanium oxide particles were obtained by treating at $600^{\circ}C$ for 1 h. The crystallization and rapid growth of particles was accelerated by increasing heat treatment temperature and time. Anatase phase generated below $600^{\circ}C$ transformed to the rutile phase with increasing heat treatment temperature. Moreover, above $800^{\circ}C$, heat treatment time had a very large influence on particle growth, and changing the heating condition also had a large influence on crystal growth.
Keywords
$TiO_2$; Nanoparticle; Polymer matrix technique;
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Times Cited By KSCI : 3  (Citation Analysis)
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