• 대한치과기공학회지
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• 제40권4호
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• pp.201-207
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• 2018

Purpose: The purpose of this study is to evaluate the fitness of lower jaw compete denture with glass fiber. Methods: Lower jaw edentulous model was selected as the master model. Ten study models were produced using Type IV stone(n=10). Lower jaw trial dentures were produced by the wax denture base and artificial teeth. Conventional complete denture (CD) group was fabricated by excluding glass fiber reinforcement (n=5). Glass fiber complete denture (GD) group was fabricated with glass fiber reinforcement (n=5). The lower jaw trial complete denture was invested using a plaster. PMMA resin was injected and curing was performed. The CD and GD groups measured the fit using silicone replica technology. The measured data was verified by t-test. Results: The anterior area of the CD group showed the smallest value. There was a statistically significant difference in the anterior area of the CD group and the GD group (p<0.05), but there was no statistically significant difference in the posterior area (p>0.05). Conclusion : Complete denture with glass fiber showed low fitness and further study is needed to apply it clinically.

• 대한치과보철학회지
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• 제41권6호
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• pp.732-746
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• 2003

Statement of problem. Soft lining materials, also referred to as tissue conditioning materials, tissue heating materials, relining materials, soft liners or tissue conditioners, were first introduced to dentistry by a plastic manufacturer in 1959. Since the introduction of the materials to the dental field, their material properties have been continually improved through the effort of many researchers. Soft lining materials have become widely accepted, particularly by prosthodontists, because of their numerous clinical advantages and ease of manipulation. Unfortunately, few reports have been issued upon the topic of increasing the bond strength between the base metal alloy used in cast denture bases and PMMA soft liner modified with 4-META, nor upon the pattern of debonding and material change in wet environment like a intra oral situation. Purpose. The purposes of this study were comparing the bond strength between base metal alloy used for the cast denture bases and PMMA soft liner modified with 4-META, and describing the pattern of debonding and material property change in wet environment like the intraoral situation. Material and Methods. This study consisted of four experiments: 1. The in vitro measurement of shear bond strength of the adhesive soft liner. 2. The in vitro measurement of shear bond strength of the adhesive soft liner after 2 weeks of aging. 3. A comparison of debonding patterns. 4. An evaluation the Relation time of modified soft liner. The soft liner used in this study was commercially available as Coe-soft (GC America.IL.,USA), which is provided in forms of powder and liquid. This is a PMMA soft liner commonly used in dental clinics. The metal primer used in this study was 4-META containing primer packed in Meta fast denture base resin (Sun Medical Co., Osaka, Japan). The specimens were formed in a single lap joint desist which is useful for evaluating the apparent shear bond strength of adhesively bonded metal plate by tensile loading. Using the $20{\times}20mm$ transparent grid, percent area of adhesive soft liner remaining on the shear area was calculated to classify the debonding patterns. To evaluate the change of the initial flow of the modified adhesive soft liner, the gelation time was measured with an oscillating rheometer (Haake RS150W/ TC50, Haake Co., Germany). It was a stress control and parallel plate type with the diameter of 35mm. Conclusion. Within the conditions and limitations of this study, the following conclusions were drawn as follows. 1. There was significant increase of bond strength in the 5% 4-META, 10% 4-META containing groups and in the primer coated groups versus the control group(P<0.05). 2. After 2 weeks of aging, no significant increase in bond strength was found except for the group containing 10% 4-META (P<0.05). 3. The gelation times of the modified soft liner were 9.3 minutes for the 5% 4-META containing liner and 11.5 minutes for the 10% 4-META liner. 4. The debonding patterns of the 4-META containing group after 2 weeks of aging were similar to those of immediaely after preparation, but the debonding pattern of the primer group showed more adhesive failure after 2 weeks of aging.

• 대한치과보철학회지
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• 제41권5호
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• pp.626-639
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• 2003

Statement of problem : Recently, in attempts to reinforce the acrylic resin and to reduce the polymerization shrinkage, it has been reported that adding vinyloligo-silsesquioxane (vinyl-POSS) to PMMA significantly compensates for polymerization shrinkage and somewhat increases the fracture resistance. Purpose : There haven't been any studies on abrasion that can affect the adaptation of the denture in long-term use. In this study abrasion resistance was compared between acrylic resin with vinyl-POSS and commercialized acrylic resin for denture base. In addition, the difference in abrasion resistance according to molding methods was compared. Material and method : Using PaladentR 20 including vinyl-POSS. PaladentR 20, Lucitone 199R, SR IvocapR, denture bases were fabricated using compression molding technique and continuous-pressure injection technique. Surface hardness and abrasion were measured for each group, and the worn surfaces were observed under a scanning electron microscope. Results : 1. When surface hardness was measured for each material and molding technique, there was no statistically significant difference among the materials. (p<0.05) 2. When same denture base material and molding technique were used, the abrasion due to toothpaste solution was 5 times as severe as the abrasion due to soap solution. 3, When toothpaste solution was used, the abrasion decreased in the order of PaladentR20, PaladentR 20 including vinyl-POSS, SR IvocapR, and Lucitone 199R. However statistically significant difference was seen only among PaladentR 20, SR IvocapR, and Lucitone 199R. (p<0.05). 4. When soap solution was used, the abrasion was more severe in PaladentR 20 and including vinyl-POSS PaladentR 20 groups than in SR IvocapR and Lucitone 199R groups. (p<0.05). Conclusion : Addition of vinyl-POSS doesn't improve the abrasion resistance, and the abrasion resistance was similar to those of existing materials. Additional studies under different conditions are needed. For clinical application of vinyl-POSS, further investigations with different requirements and conditions are necessary.

• The Journal of Advanced Prosthodontics
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• 제5권3호
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• pp.287-295
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• 2013

PURPOSE. This study investigated the effect of laser parameters and air-abrasion on the peel strength of silicon-based soft denture liner to different denture resins. MATERIALS AND METHODS. Specimens (N=180) were prepared out of three different denture base resins (Rodex, cross-linked denture base acrylic resin; Paladent, heat-cured acrylic resin; Deflex, Polyamide resin) ($75mm{\times}25mm{\times}3mm$). A silicon-based soft denture liner (Molloplast B) was applied to the denture resins after the following conditioning methods: a) Air-abrasion ($50{\mu}m$), b) Er,Cr:YSGG laser (Waterlase MD Turbo, Biolase Technology) at 2 W-20 Hz, c) Er,Cr:YSGG laser at 2 W-30 Hz, d) Er,Cr:YSGG laser at 3 W-20 Hz, e) Er,Cr:YSGG laser at 3 W-30 Hz. Non-conditioned group acted as the control group. Peel test was performed in a universal testing machine. Failure modes were evaluated visually. Data were analyzed using two-way ANOVA and Tukey's test (${\alpha}$=.05). RESULTS. Denture liner tested showed increased peel strength after laser treatment with different parameters ($3.9{\pm}0.4-5.58{\pm}0.6$ MPa) compared to the control ($3.64{\pm}0.5-4.58{\pm}0.5$ MPa) and air-abraded groups ($3.1{\pm}0.6-4.46{\pm}0.3$ MPa), but the results were not statistically significant except for Paladent, with the pretreatment of Er,Cr:YSGG laser at 3 W-20 Hz. Polyamide resin after air-abrasion showed significantly lower peel strength than those of other groups ($3.1{\pm}0.6$ MPa). CONCLUSION. Heat-cured acrylic resin, PMMA, may benefit from Er,Cr:YSGG laser treatment at 3 W-20 Hz irradiation. Air-abrasion of polyamide resins should be avoided not to impair their peel bond strengths to silicon-based soft denture liners.

• The Journal of Advanced Prosthodontics
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• 제13권3호
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• pp.160-171
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• 2021

Purpose. This in-vitro study evaluated and compared the color stability of 3D-printed and conventional heat-polymerized acrylic resins following aging, mechanical brushing, and immersion in staining medium. Materials and methods. Forty disc-shaped specimens (10 mm in diameter and 3 mm thick) were prepared from two 3D-printed [DentaBASE (DB) and Denture 3D+ (D3D)] and one conventional polymethylmethacrylate (PMMA) denture materials. The specimens were thermo-cycled, subjected to mechanical brushing, and were immersed in either coffee, lemon juice, coke, or artificial saliva (AS) to simulate one and two years of oral use. Color measurements of the specimens were recorded by a spectrophotometer at baseline (T0), and after one (T1) and two years (T2) of simulation. The color changes (ΔE) were determined and also quantified according to the National Bureau of Standards (NBS) units. Descriptive statistics, followed by factorial ANOVA and Bonferroni post-hoc test (α=.05), were applied for data analysis. Results. The independent factors, namely material, staining medium, and immersion time, and interaction among these factors significantly influenced ΔE (P<.009). Irrespective of the materials, treatments, and time, the highest and the lowest mean ΔEs were observed for PMMA in lemon juice (4.58 ± 1.30) and DB in AS (0.41 ± 0.18), respectively. Regarding the material type, PMMA demonstrated the highest mean ΔE (2.31 ± 1.37), followed by D3D (1.67 ± 0.66), and DB (0.85 ± 0.52), and the difference in ΔE between the materials were statistically significant (P<.001). All the specimens demonstrated a decreased color changes at T2 compared to T1, and this difference in mean ΔE was statistically significant (P<.001). Conclusion. The color changes of 3D-printed denture resins were low compared to conventional heat polymerized PMMA. All the tested materials, irrespective of the staining medium used, demonstrated a significant decrease in ΔE values over time.

• 대한치과보철학회지
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• 제39권6호
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• pp.589-598
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• 2001

The fracture of acrylic resin dentures remains an unsolved problem. Therefore, many investigations have been performed and various approaches to strengthening acrylic resin, for example, the reinforcement of heat-cured PMMA resin using glass fibers, have been suggested over the years. The aim of the present study was to investigate the effect of short glass fibers treated with silane coupling agent on the transverse strength of heat-polymerized PMMA denture base resin. To avoid fiber bunching and achieve even fiber distribution, glass fiber bundles were mixed with PMMA powder in conventional mixer whose blade was modified to be blunt. Composite of glass fiber($11{\mu}m$ diameter, 3mm & 6mm length, silane treated) and PMMA resin was made. Transverse strength and Young's modulus were estimated. Glass fibers were incorporated with 1%, 3%, 6% and 9% by weight. Plasticity and workability of dough was evaluated. Fracture surface of specimens was investigated by SEM. The results of this study were as follows 1. 6% and 9% incorporation of 3mm glass fibers in the PMMA resin enhanced the transverse strength of the test specimens(p<0.05). 2. 6% incorporation of 6mm glass fibers in the PMMA resin increased transverse strength, but 9% incorporation of it decreased transverse strength(p<0.05). 3. When more than 3% of 3mm glass fibers and more than 6% of 6mm glass fibers were incorporated, Young's modulus increased significantly(p<0.05). 4. Workability decreased gradually as the percentage of the fibers increased. 5. Workability decreased gradually as the length of the fibers increased. 6. In SEM and LM, there was no bunching of fibers and no shortening of fibers.

• 대한치과보철학회지
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• 제45권3호
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• pp.310-320
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• 2007

Statement of the problem. The fracture of acrylic resin dentures remains an unsolved problem. Therefore, many investigations have been performed and various approaches to strengthening acrylic resin, for example, the reinforcement of heat-cured acrylic resin using glass fibers, have been suggested over the years. But problems such as poor workability, rough surface, poor adhesion of glass fiber resin complex are not solved yet. Purpose. The aim of the present study was to investigate the effect of short glass fibers on the transverse strength of heat-polymerized denture base acrylic resin and roughness of resin complex after abrasion test. Material and methods. To avoid fiber bunching and achieve even fiber distribution, glass fiber bundles were mixed with acrylic resin powder in conventional mixer with a non-cutting blade, to produce the glass fiber($10{\mu}m$ diameter, 3mm length, silane treated) resin composite. Glass fibers were incorporated at 0%, 3%, 6% and 9% by weight. Transverse strength were measured. After abrasion test, surface roughness was evaluated and scanning electron microscope view was taken for clinical application. Results. 1. 6% and 9% incorporation of 3mm glass fibers in the acrylic resin enhanced the transverse strength of the test specimens(p<0.05). 2. Before abrasion test, incorporation of 0%, 3%, 9% glass fiber in the resin showed no dirrerence in roughness statisticaly(p>0.05). 3. After abrasion test, incorporation of 0%, 3%, 6% glass fiber in the resin showed same surface roughness value statistically(p>0.05). 4. In SEM, surface roughness increased as the percentage of the fibers increased. 5. In the areas where glass fiber bunchings are formated, a remarkably high roughness was noticed. Conclusion. 6% and 9% addition of silane-treated short glass fibers into denture base acrylic resin increased transverse strength significantly. Before and after abrasion test, incorporation of 0%, 3%, 6% glass fiber in the resin showed same surface roughness value statistically.

• 대한치과보철학회지
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• 제37권6호
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• pp.809-818
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• 1999

This study was performed to evaluate the tensile bond strength and modulus of elasticity of three permanent soft denture liners (Molloplast $B^{(R)}$, Ufi Gel $C^{(R)},\;Tokuyama^{(R)}$) before and after thermocycling. And their water sorption were also evaluated. Each soft denture liner was bonded to PMMA denture base resin blocks and the tensile bond strength and modulus of elasticity were measured by using universal testing machine. For the water sorption, weight measured after immersion of sea denture liners in $37{\pm}1^{\circ}C$ water bath for 4 weeks. The results were as follows : 1. Molloplast $B^{(R)}$ had the highest tensile bond strength, while Tokuyama had the lowest tensile bond strength. There was no significant difference between $Tokuyama^{(R)}$ and Molloplast $B^{(R)}$ in the both nonthermocycling and thermocycling. There was significant difference in tensile strength of $Tokuyama^{(R)}$ before and after thermocycling(p<0.05). 2. For the modulus of elasticity, there was no significant difference between Ufi Gel $C^{(R)}\;and\;Tokuyama^{(R)}$ in the both nonthermocycling and thermocycling. There was significant difference in modulus of elasticity of $Tokuyama^{(R)}$ before and after thermocycling(p<0.05). 3 The failure modes of Molloplast $B^{(R)}$ and Ufi Gel $C^{(R)}$ were mainley adhesive type and that of $Tokuyama^{(R)}$ was mainly mixed type in case of nonthermocycling and cohesive type after thermocycling. 4. The water sorption of each soft liners was within ${\pm}2%$ in times (p<0.05) but. there was no significant difference among the soft liners in times.

• 대한치과보철학회지
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• 제58권3호
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• pp.207-216
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• 2020

목적: 최근 치과에 도입된 polyetherketoneketone (PEKK)의 연마 특성이 Candida albicans의 부착에 미치는 영향을 기존 의치상재료인 polymethylmethacrylate (PMMA)와 비교하고자 하였다. 재료 및 방법: PEKK(그룹 E)와 PMMA(그룹 M)를 사용하여 직경 8 mm, 두께 2 mm인 원판 형태 시편을 제작한 후 연마 정도에 따라 각각 2개 그룹으로 세분하였다(ER, MR: rough; EP, MP: polished, 각 그룹당 시편 12개). 연마는 SiC 연마지로 시행하였으며, ER과 MR 그룹에서는 600 grit SiC 연마지만으로, EP와 MP 그룹에서는 600, 800, 1,000, 1,200 grit SiC 연마지로 단계적으로 연마하였다. 표면의 평균 거칠기는 원자력간 현미경(AFM)을 사용하여 Sa값을 측정하였고 주사전자 현미경으로 1,000배와 20,000배 확대하여 표면을 관찰하였다. 24-well 세포배양 용기에 연마된 시편 및 C. albicans 현탁액을 넣고 37℃에서 2시간 동안 배양하여 C. albicans의 부착을 유도하였으며, 부착된 진균을 피펫팅을 통해 분리하고 현탁액을 10 배씩 단계적으로 10³ 배까지 희석한 후, Sabouraud dextrose 고체배지에 스프레더를 이용하여 접종하였다. 48시간 후 각 고체배지에 형성된 집락의 개수(CFU/plate)를 세어 기록하였다. 측정된 값들의 통계적 차이를 확인하기 위해 one-way ANOVA와 Tukey HSD test를 수행하고 유의수준을 0.05로 정하였다. 결과: 평균 Sa 값은 MR 그룹이 다른 그룹에 비해 유의하게 더 높게 나타나 단계적 연마지 연마법은 PMMA 시편에서만 유의한 효과가 있었음을 확인할 수 있었다 (P < .05). MP 그룹과 EP 그룹간에 Sa 값은 유의한 차이가 없었다. 주사전자현미경 관찰결과 PEKK 시편들의 표면에서 다수의 보풀 같은 돌기가 형성되어 있는 것을 볼 수 있었고 EP 그룹에서 더 심해진 것을 관찰할 수 있었다. CFU/plate의 평균값은 EP 그룹에서 가장 높게 나왔으며 가장 낮은 MP 그룹과 유의한 차이를 보였다 (P < .05). 결론: PMMA와 비교하여 PEKK에서는 단계적 연마지를 이용한 연마를 시행 시 C. albicans의 부착 증가로 이어질 수 있으며, 임상에서도 이러한 점에 대한 신중한 고려가 필요할 것으로 사료된다.

• 대한치과기공학회지
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• 제42권2호
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• pp.91-98
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• 2020

Purpose: This study is to compare the flexural strength and modulus by inserting a mesh and stick type fiberglass reinforcement into resin specimens. Methods: Wax specimens (length 64 mm, width 39 mm, thickness 5 mm) are prepared according to ISO 20795-1:2013. Mesh type and stick type glass fiber reinforcements were prepared. The prepared wax specimens were used plaster and flask for investment. The flask was separated and the wax was removed. The heat curing resin was injected into the flask, and then a mesh type and stick type fiberglass reinforcement were inserted. The prepared resin specimen was cut into three equal parts (length 64 mm, width 10 mm, thickness 3.3 mm). The mesh type glass fiber reinforcement (MT group) and the stick type glass fiber reinforcement (ST group) were classified into two groups. The prepared specimen was measured using a universal testing machine (UTM). The data were analyzed by Mann-Whitney U test, and the significance level was set to 0.05. Results: In the flexural strength, the ST group was higher than the MT group, and there was a significant difference between the two groups (p<0.05). In the flexural modulus, the ST group was higher than the MT group, and there was a significant difference between the two groups (p<0.05). Conclusion: The stick-type glass fiber inreased the flexural strength than the mesh-type glass fiber reinforcement.