• Title/Summary/Keyword: PLE

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The formation of Paper and the Measurement of Formation

  • Komppa, Olavi
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.29 no.2
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    • pp.76-82
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    • 1997
  • In paper the evenness of planar distribution of mass in a small scale is called formation (orbetter:mass formation). Traditionally formation has been assessed visually, by looking the sheet of paper against transmitted light. Different kinds of optieal testers are being usd to obtain quantitative rankings htat would be independent of the observer but would well correspond to the visual assessment. However, various raw-material and process factors do influence light trans-mittance in paper and do impair the correspondence between basis weight and the optical formation measurement (or visual assessment). As the optical formation test methods do not incorporate an efficient calib ration routine, the formation of the sophisticated paper grades of today the is rather difficult to measure optically and may lead to erroneous results. It may be concluded that the optical measurement is not suitable for paper grades with high filler content. coating, heavy calendering or that are made of heavily beaten pulp, nordoes it apply for dyed or printed papers. For this reason, visual assessment and optical evaluation shoild be replaced with a measurement that gives reliable results independent on paper grode and manufacturing process. Formation measuremend based on beta radiation is suitable for all paper grades regardless to the material contents or process treatment. It is possible to measure even dyed or printed samples. Thonks to a sim ple and relioble calibration, the results are converted to real basis weight balues that remain reliable even with time. The only beta tester commercially available is the AMBERTEC Beta Formation Tester. Formation of paper does vary locally in the web. Typically there exists a formation profile, too similarly to other properties of paper. Therefore, formation should ? ays be expressed as a mean of a sufficient amount of parallel determinations. All formation measurements should be calibrated against basis weight.

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Determination of Tiapride in Human Plasma Using Hydrophilic Interaction Liquid Chromatography-Tandem Mass Spectrometry

  • Moon, Ya;Paek, In-Bok;Kim, Hui-Hyun;Ji, Hye-Young;Lee, Hye-Won;Park, Hyoung-Geun;Lee, Hye-Suk
    • Archives of Pharmacal Research
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    • v.27 no.9
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    • pp.901-905
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    • 2004
  • A rapid, sensitive and selective hydrophilic interaction liquid chromatography-tandem mass spectrometric(HILIC-MS/MS) method for the determination of tiapride in human plasma was developed. Tiapride and internal standard, metoclopramide were extracted from human plasma with dichloromethane at basic pH and analyzed on an Atlantis HILIC silica column with the mobile phase of acetonitrile-ammonium formate (190 mM, pH 3.0) (94:6, v/v). The ana-Iytes were detected using an electrospray ionization tandem mass spectrometry in the multi-ple-reaction-monitoring mode. The standard curve was linear (r=0.999) over the concentration range of 1.00-200 ng/mL. The coefficient of variation and relative error for intra- and inter-assay at three QC levels were 6.4∼8.8% and -2.0∼3.6%, respectively. The recoveries of tiapride ranged from 96.3 to 97.4%, with that of metoclopramide (internal standard) being 94.2%. The lower limit of quantification for tiapride was 1.00 ng/mL using 1 00 $\mu$L of plasma sample.

Eine Studie $\"{u}ber$ die Valenz verbaler Phraseolexeme der deutschen Gegenwartssprache (현대 독일어 동사 관용구의 결합가 연구)

  • Kim Soo-Nam
    • Koreanishche Zeitschrift fur Deutsche Sprachwissenschaft
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    • v.1
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    • pp.69-90
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    • 1999
  • Die vorliegende Arbeit setzte sich zum Ziel, deutsche verbale Phraseolexeme(vPL) auf der Grundlage einer Mehrebenenbeschreibung syntaktisch sowie semantisch zu untersuchen. Dabei $st\"{u}tzten$ wir uns vor allem auf die Valenz- und Kasustheorie sowie das 6-Stufen-Modell von G. Helbig(1983) und das Mehrebenenmodell $f\"{u}r$ vPL von B. Wotjak(1992), das seinerseits vom methodischen Ansatz her in engem Zusammenhang zu dem Beschreibungsansatz steht. Aber Wir modifizierten teilweise das Modell yon B. Wotjak(1992) und stellten einige vPL exemplarisch dar. Dieser Untersuchung lag eine verbozentrische Auffassung des Satzes zugrunde: Das Verb bildet das organisierende Zentrum des Satzes und ist fur die Grundstruktur des Satzes verantwortlich. Das Verb als $Valenztr\"{a}ger\;er\"{o}ffnet$ um sich herum bestimmte Leerstellen, deren Zahl und Art letztlich von der Verbbedeutung her determiniert sind. Auch vPL kann als $Valenztr\"{a}ger$ - wie das Verb - das strukturelle Zentrum des Satzes darstellen, d.h. vPL bildet als Ganzes das $Pr\"{a}dikat$, das wendungsextern eine bestimmte Zahl von Leerstellen $er\"{o}ffnet$ und determiniert im Satz mit seinen $inh\"{a}renten$ semantischen Merkmalen seine semantische und syntaktische Umgebung. Bei der Analyse von vPL gingen wir von der Auffassung von B. Wotjak aus, $da\ss$ Modelle zur Beschreibung von Verben prinzipiell auch auf die Beschreibung von verbalen PL anwendbar sind. In dieser Untersuchung verwendeten wir - in Anlehnung an B. Wotjak(1996:4f.) - den Terminus 'Phraseologismus' als Oberbegriff, der a) Kollokationen, $b)\;Funktionsverbgef\"{u}ge\;(FVG)$, c) Wortidiome (wortwertige idiomatische Redewendungen oder Phraseolexeme), d) Satzidiome(satzwertige idiomatische Redewendungen bzw. kommunikative Formeln/ Routineformeln), e) $Sprichw\"{o}rter\;umfa{\ss}t$. Wir $beschr\"{a}nkten$ uns den Gegenstand unserer Untersuchung auf verbale Phraseolexeme(vPL), d.h. wie oben genannte Wortidiome. VPL lassen sich $prim\"{a}r$ in bezug auf das wendungsexterne ($\"{a}u{\ss}ere$) Aktantenpotential(PLe) und $sekund\"{a}r$ in bezug auf die interne Kom­ponentenstruktur des PL(PLi) klassifizieren. Unsere Studie soil nicht nur Hintergrundwissen $f\"{u}r$ Lexikonein­tragungen vertiefen helfen, sondern auch $f\"{u}r$ den Fremdsprachen­unterricht von Nutzen sein.

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Transient coupled thermoelastic analysis by finite element method (유한요소법에 의한 과도연성 열탄성 해석)

  • 이태원;심우진
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.14 no.6
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    • pp.1408-1416
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    • 1990
  • A powerful and efficient method for finding approximate solutions to initial-boundary-value problems in the transient coupled thermoelasticity is formulated in time domain using the finite element technique with time-marching strategy. The final system equations can be derived by the Guritin's variational principle using the definition of convolution integral. But, the finite element formulation for the equations of motion is modified by differentiating in time. Numerical results to some test problems are compared with analytical and other sophisticated approximate solutions. Stable responces are observed in all the given examples irrespective of incremental time steps and mesh shapes. In addition, it is shown that good numerical results are obtained even in coarser mesh or larger time step comparing to other numerical methods.

Preparation of Eu-doped $YVO_4$ Red Phosphors by Solid-State Reaction Technique

  • Jang, Jae-Yeong;Bang, Jun-Hyeok;An, Se-Hyeok;Ma, Gwon-Do;Kim, Chun-Su;Jo, Sin-Ho
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.330-331
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    • 2011
  • 희토류 이온이 첨가된 형광체는 조명, 정보 디스플레이, 태양 에너지 변환 소자에 응용 가능하기 때문에 상당한 주목을 받고 있다. 특히, 결정 입자의 형상과 크기는 산업체 응용에 있어서 중요한 변수 중의 하나이다. 구형의 형광체 입자는 형광층의 광학 및 기하학적 구조를 최적화 시킬 수 있고, 결정 입자의 크기는 양질의 코팅을 위해 필요한 결정 입자의 양에 영향을 미친다. 본 연구에서는, $YVO_4$ 모체 결정에 Eu 이온의 농도를 선택적으로 주입하여 발광 효율이 높은 적색 형광체를 합성하고자 한다. 형광체 분말 시료는 활성체인 Eu의 함량을 0.00, 0.05, 0.10, 0.15, 0.20 mol로 변화시키면서 고상 반응법을 사용하여 합성하였다. 볼밀링 작업을 수행한 후에, 60$^{\circ}C$에서 20시간 건조하였고, 잘게 갈아서 체로 걸러낸 다음에 세라믹 도가니에 넣고 전기로에서 서서히 온도를 승온시켜 500$^{\circ}C$에서 10시간 동안 하소를 실시한 후에 1,100$^{\circ}C$에서 5시간 동안 소결하였다. Eu 이온의 함량비를 변화시켜 합성한 $YVO_4$ : Eu 형광체 분말 시료의 발광 세기의 변화, 결정 구조와 표면 형상을 각각 PL과 PLE, XRD, FE-SEM 장치를 사용하여 측정한 결과들을 종합해 볼 때, Eu 이온의 비가 0.15 mol일때 발광 세기가 최대값을 나타냄을 알 수 있었으며, 더욱 Eu의 함량을 증가시키자 농도 억제 현상에 의하여 발광 세기는 급격히 감소함을 보였다. SEM으로 촬영한 결정 입자의 형상의 경우에, Eu 이온의 함량비가 증가함에 따라 결정 입자들이 더욱 조밀하게 구형에 가까운 형상을 나타냄을 관측할 수 있었다(Fig. 1). 형광체 분말의 형광 스펙트럼의 경우에, 619 nm에 주 피크를 갖는 적색 형광 스펙트럼들이 관측되었으며, Eu 이온의 함량비에 따라 형광 세기는 상당한 의존성을 나타내었다(Fig. 2). Eu 함량에 따른 결정입자의 크기, 형광 세기와 회절 피크의 반치폭 사이의 상관 관계를 제시하고자 한다.

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Synthesis and Luminescence Properties of $GdNbO_4$ : $Eu^{3+}$ Phosphors

  • Gwon, Bang-Gil;Jo, Sin-Ho
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.324-325
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    • 2011
  • 최근에 고효율의 적색 형광체를 합성하여 형광 램프, 음극선관, X-선 검출기, 전계 발광 디스플레이에 응용하기 위하여 다양한 모체 결정과 활성체를 도핑하는 연구가 활발히 진행되고 있다. 본 연구에서는 $GdNbO_4$ 모체 결정에 $Eu^{3+}$ 이온 활성체를 주입하여 합성함으로써 새로운 적색 형광체의 발광 세기와 입자의 형상을 최적화 시키고자 한다. 형광체 분말 시료의 제조는 Eu의 함량을 0, 0.05, 0.10, 0.15, 0.20 mol로 변화시키면서 고상 반응법을 이용하여 합성하였다. 초기 물질 Gd2O3 (99.99%), $Nb_2O_5$ (99.99%), $Eu_2O_3$ (99.9%)를 화학 적량으로 측량하고 에탄올과 ZrO2 볼과 함께 플라스틱 병에 넣어 400 rpm의 속도로 24시간 볼밀 작업을 수행한 후에, 혼합된 분말의 볼을 걸러내고 60$^{\circ}C$에서 20시간 동안 건조하였다. 건조된 시료를 막자 사발에 넣고 잘게 갈아서 체로 걸러낸 다음에 세라믹 도가니에 넣고 전기로에서 분당 5$^{\circ}C$씩 승온하여 500$^{\circ}C$에서 10시간 동안 1차 하소한 후에, 계속 온도를 승온시켜 1,200$^{\circ}C$에서 3시간 동안 소결하여 합성하였다. XRD 회절 패턴의 경우에, $Eu^{3+}$의 함량에 관계없이 모든 세라믹은 JCPDS (22-1104)에 제시된 회절상과 일치하는 사방정계의 결정 구조를 가짐을 확인할 수 있었다. 주 피크는 28.4$^{\circ}$에서 최대값을 갖는 (121)면에서 발생하는 회절 신호이었다(Fig. 1). 적색 형광체 분말의 광학 및 표면 특성은 PL, PLE와 SEM으로 조사되었으며, 세라믹 분말의 형광 특성과 결정 구조, 표면 형상에 대한 자세한 논의가 제시될 것이다.

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Disign of Non-coherent Demodulator for LR-WPAN Systems (LR-WPAN 시스템을 위한 비동기 복조 알고리즘 및 하드웨어 구조설계)

  • Lee, Dong-Chan;Jang, Soo-Hyun;Jung, Yun-Ho
    • Journal of Advanced Navigation Technology
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    • v.17 no.6
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    • pp.705-711
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    • 2013
  • In this paper, we present a low-complexity non-coherent demodulation algorithm and hardware architecture for LR-WPAN systems which can support the variable data rate for various applications. The need for LR-WPAN systems that can support the variable data rate is increasing due to the emergence of various sensor applications. Since the existing symbol based double correlation (SBDC) algorithm requires the increase of complexity to support the variable data rate, we propose the sample based double correlation (SPDC) algorithm which can be implemented without the increase of complexity. The proposed non-coherent demodulator was designed by verilog HDL and implemented with FPGA prototype board.

Photoluminance Properties of ${Al_3}{GdB_4}{O_{12}}$ Phosphors Activated by $Tb^{3+} and Eu^{3+}$ ($Tb^{3+}$ 와 Eu^{3+}$로 활성화시킨${Al_3}{GdB_4}{O_{12}}$ 형광체의 발광 특성)

  • Kim, Ki-Woon;Kang, Sei-Sun;Lee, Rhim-Youl
    • Korean Journal of Materials Research
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    • v.10 no.1
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    • pp.49-54
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    • 2000
  • The new green $Al_3GdB_4O_{12}:Tb^{3+} and red Al_3GdB_4O_{12}:Eu_{3+}$ phosphors were synthesized and then characterized their optical properties for PDP application. And also the photoluminescence properties of these phosphors were compared with the commercial green $Zn_2SiO_4:Mn^{2+} and (Y,Gd)BO_3: Eu^{3+}$ red PDP phosphors. The phosphors were synthesized by solid state reaction at 115$0^{\circ}C$ for 4hr. It was found that the emitting brightness of $Al_3GdB_4O_{12}:Tb^{3+}$(15mol%) green phosphor under 147nm excitation was higher than that of commercial $Zn_2SiO_4: Mn^{2+}$ green PDP phosphor. However, the color coordinate of this new green phosphor was inferior to the commercial one. On the other hand, the emitting intensity of $Al_3GdB_4O_{12}:Eu^{3+}$(15mol%) red phosphor was smaller than the $commercial(Y,Gd)BO_3: Eu^{3+}$ red one, but the CIE coordinate was slightly improved. The excitation spectrum showed that $Al_3GdB_4O_{12}$ phosphors had a strong excitation band at $\lambda=160nm$ associated with the host absorption. And the photoluminance excitation (PLE) intensity in VUV range for $Al_3GdB_4O_{12}:Tb^{3+}$ green phosphor was higher than that of $Zn_2SiO_4: Mn^{2+}$, but the PLE intensity of $Al_3GdB_4O_{12}:Eu^{3+}$ red phosphor was smaller than $(Y,Gd)BO_3: Eu^{3+}$.

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Antioxidant and Anti-Inflammatory Effects on Optimal Extraction Conditions of Different Edible Parts of Perilla (Perilla frutescens L.) (들깨 가식부위별 최적 추출 조건 확립을 위한 항산화 및 항염증 활성 평가)

  • Min Young Kim;Jung In Kim;Sang Woo Kim;Sungup Kim;Eunyoung Oh;Jeongeun Lee;Eunsoo Lee;Yeon Ju An;Myoung Hee Lee;Choon-Song Kim
    • The Korean Journal of Food And Nutrition
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    • v.36 no.6
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    • pp.551-560
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    • 2023
  • This study was performed to investigate antioxidant and anti-inflammatory activities of perilla(Perilla frutescens L.) seed, flower and leaf according to extraction condition. Perilla seed extracts(PSE), perilla flower extracts(PFE), perilla leaf extracts(PLE) was extracted by stirring extraction (STE, 25℃), shaking extraction (SHE, 80℃), and sonication assisted extraction(SAE, 25℃) with 94% ethanol, 60% ethanol and distilled water, followed by analysis of total polyphenol and flavonoid and testing radical scavenging activities. The highest total polyphenol content (5.47, 9.36, 38.58 mg gallic acid equivalent/g), total flavonoid content(5.77, 8.62, 46.44 mg catechin equivalent/g), ABTS(10.68, 19.46, 63.56 mg trolox equivalent/g) and DPPH(6.51, 7.69, 79.73 mg trolox equivalent/g) radical scavenging activity of PSE, PFE and PLE was observed in the HWE with 60% ethanol,. Among the three extraction method, SHE provided the best results for yield, polyphenol, flavonoid content of perilla seed, flower, leaf in comparison to STE or SAE. SHE with 60% ethanol of perilla seed, flower, leaf more effectively inhibited secretion of nitric oxide(NO) and pro-inflammatory cytokine in RAW 264.7 macrophage exposed to LPS compared to other extraction solvent and method. Therefore, these extracts obtained from perilla seed, flower, leaf could be used antioxidant and anti-inflammatory ingredients in the food industry.

Use of the Stomach as an Esophageal Substitute after Total Pharyngolaryngoesophagectomy for Treating Cervical Esophageal Cancer or Hypopharyngeal Cancer (경부식도암 및 하부인두암에서 근치적 전후두인두식도절제술 후 위를 이용한 재건술의 의의)

  • Lee, Sang-Hyuk;Lee, Sang-Hoon;Yoon, Ho-Young;Kim, Choong-Bai
    • Journal of Gastric Cancer
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    • v.7 no.4
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    • pp.200-205
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    • 2007
  • Purpose: The aim of this study was to analyze the post operative outcome of reconstruction with using the stomach after performing total pharyngolaryngoesophagectomy in patients with hypopharyngeal cancer or cervical esophageal cancer. Materials and Methods: We conducted a retrospective chart review of 23 patients who underwent gastric pull up for esophageal substitution at the Department of Surgery, Yonsei University College of Medicine, between January 1991 and December 2006. All the patients had transhiatal esophagectomy performed without thoracotomy. Results: There were seventeen males and six females with a median age of 58.1 years (range: 40-70 years). 19 cases were hypopharyngeal cancer, 13 cases had cancer in the pyriform sinus, 15 cases had cancer in the postcricoid area and one case had cancer in the glottic area. The rest were cervical esophageal cancers. The pathologic result was squamous cell carcinoma in all cases. The median total follow-up period was 33 months (range: 1-62 months) and there were two (8.6%) postoperative deaths: one was due to carotid rupture and the other was due to hepatic failure with liver metastasis. The complications were leakage in 1 patient (4.4%), pneumothorax in 1 patient (4.4%) and pneumonia in 1 patient (4.4%). Conclusion: The use of stomach for esophageal reconstruction has many benefits for treating hypopharyngeal cancer or cervical esophageal cancer, So, we made sure there was a sufficient length for the anastomosis after pharyngolaryngoesophagectomy and a rich blood supply from the stomach. There was a low incidence of the leakage at the anastomotic site, along with a low incidence of stenosis and bleeding.

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