• Title/Summary/Keyword: PARTICLE SIZE

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The Effect of Reaction Condition on Particle Formation in the Synthesis of Silica Powder Using Emulsion (Emulsion법에 의한 실리카 분말의 합성에서 반응조건이 입자의 형성에 미치는 영향)

  • Lee S. G.;Jang Y. S.;Moon B. Y.;Kang B. S.;Park H. C.
    • Korean Journal of Materials Research
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    • v.15 no.11
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    • pp.717-721
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    • 2005
  • Silica powders were synthesized using emulsion solution containing water, nonionic surfactant of Triton N-57, and cyclohexane. Silica powders were prepared at low cost using inexpensive starting material of sodium silicate and ammonium sulfate. Morphology, size and size distribution were observed and determined using SEM. The powder was identified as silica by FT-IR and XRD analysis. Particle size and size distributions were affected by concentration of reactants, reaction time, and concentration of surfactant. Particle size were increased with increasing concentration of reactants and particles became dense with increasing reaction time. As R value increased, tile particle size was increased, reached a certain value and then decreased again. The silica powders synthesized under optimum condition were spherical in shape, $0.8{\mu}m$ in average particle size, narrow in particles size distribution, and well dispersed.

Quality Characteristics of Korean Red Ginseng Powder with Different Milling Methods (분쇄방법에 따른 고려홍삼분말의 품질특성)

  • 서창훈;이종원;도재호;김나미;양재원;장규원
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.32 no.3
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    • pp.370-374
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    • 2003
  • Cell cracking method using a non-collision was evaluated for the possibility of new red ginseng grinding technique. Based on particle size distribution analysis by 1size shaker, the ratios of 100 mesh penetrated particles were 94.9% for hammer mill (group A) and 95.6% for cell crack (group B). The ratio of 120 mesh penetrated particle of group A was higher than that in group B. The particle size distributions for 100 mesh non-penetrated Powder between 2 groups were not significantly different, and particle size distribution analysis by laser scattering analyzer showed that the particle size ranges were 0.77~128.07 ${\mu}{\textrm}{m}$ for group A and 4.24~180.07 ${\mu}{\textrm}{m}$ for group B. The Particle size distribution in group A was more broad than that in group B. The mean particle size in group B was larger than that in group A, while the standard deviation of particle size distribution in group B was less than that in group A. Structural surface characteristics, in group A, particle size distribution was broad and the distribution curve was amorphous. The structure of individual particles was similar to unequal stone which was roughly grinded and had soft cotton-like surface. In the contrary, in group B, particle size distribution was relatively narrow and also individual size particles were ubiquitously distributed. The structure of individual particles was unequal cut stone shape.

The Effects of Size Reduction and pH on Dispersion Characteristics of ATO (Antimony-Doped Tin Oxide) (입자 저감 및 pH가 ATO (안티몬도핑 산화주석)의 분산 특성에 미치는 영향)

  • Kim, Jin-Hoon;Jeong, Eui-Gyung;Lee, Sang-Hun;Han, Won-Hee;Lee, Young-Seak
    • Applied Chemistry for Engineering
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    • v.21 no.3
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    • pp.311-316
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    • 2010
  • This study aimed to prepare antimony-doped tin oxide (ATO) dispersion with high stability. The methods to achieve this goal were sought by investigating the changes of ATO particle size, size distribution, dispersion property as wet ball milling treatment time increased. And the changes of wet ball milled ATO dispersion property were also investigated, as pH increased. The changes of ATO particle size and size distribution, according to wet ball milling treatment time were evaluated with laser diffraction particle size analyzer and scanning electron microscope (SEM). The changes of ATO dispersion property, as wet ball milling treatment time and pH increased, were evaluated with zeta potential analysis and Turbiscan. By 60 min wet ball milling treatment time, ATO particle size decreased and size distribution became narrower, as the treatment time increased. After 60 min milling, the ATO particle size decreased to less than 30% of the initial size and the size distribution was narrowed to $0.1{\sim}5{\mu}m$ from $1{\sim}35{\mu}m$. However, more than 60 min milling, ATO particles aggregated and the particle size increased. ATO dispersion stability also increased as the treatment time and pH increased because the reduced particle size increased particle surface energy and repulsion between particles and the increased pH enhanced particle surface ionization. Hence, after proper length of wet ball milling treatment, highly stable ATO dispersion can be prepared, as increasing pH of the dispersion.

Mechanical Properties of Denture Base Resin through Controlling of Particle Size and Molecular Weight of PMMA (폴리(메틸 메타아크릴레이트) 입자 크기 및 분자량 제어에 따른 의치상 재료로서의 기계적 물성 변화)

  • 양경모;정동준
    • Polymer(Korea)
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    • v.27 no.5
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    • pp.493-501
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    • 2003
  • Poly(methyl methacrylate) (PMMA) particles, denture base resin, were synthesized by suspension polymerization through control of polymerization conditions (stabilizer concentration, co-monomer concentration, and the agitation speed) and evaluated changes in molecular weight and particle size. We also investigated their mechanical properties of compression-molded samples which were from synthesized polymer powder mixed with methyl methacrylate (MMA) solution. under the condition of volumetric ratio as 2:1(PMMA powder and MMA solution). The results shows that the mechanical properties were mainly affected by particle size over 100 ${\mu}$m (in particle size) and by molecular weight under 100 ${\mu}$m (in particle size). From these results, we concluded that the most appropriate particle size of PMMA powder for heat-cured denture base resins is around 100 ${\mu}$m. and its molecular weight is around 300000 (M$\sub$n/).

Tribological Properties of Reaction-Bonded SiC/Graphite Composite According to Particle Size of Graphite (반응소결 SiC/Graphite 복합체에서 Graphite 입자의 크기에 따른 마찰마모특성)

  • Baik, Yong-Hyuck;Seo, Young-Hean;Choi, Woong;Lee, Jong-Ho
    • Journal of the Korean Ceramic Society
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    • v.34 no.8
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    • pp.854-860
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    • 1997
  • The tribological property of ceramics is very important for use in seal rings, pump parts, thread guides and mechanical seal, etc. In the present study, which RBSC/graphite composites were manufactured by adding graphite powders with different particle sizes to mixtures of SiC powder, metallic silicon, carbon black and alumina, effects on the tribological property of each RBSC/graphite composite was investigated in accordance with the particle size of the added graphite powder. The water absorption, the bending strength and the resistance for the friction and wear were measured, and the crystalline phase and the microstructure were respectively examined by using XRD and SEM. In case that the particle size of the graphite powder was fine(2${\mu}{\textrm}{m}$), the formation of $\beta$-SiC was accelerated, thereby making the increase of the bending strength and the decrease of the water absorption, but no improvement for the tribological properties. Furthermore, in case that the particle size of the graphite powder was some large(88~149${\mu}{\textrm}{m}$), the formation of $\beta$-SiC was not accelerated, to thereby make the decrease of the bending strength and the increase of the water absorption, but the improvement for the tribological property of only the composite having the graphite powder of 20 vol%. In addition, in case that the particle size distribution of the graphite powder was large (under 53 ${\mu}{\textrm}{m}$), there was no improvement for every properties. However, the composites, which the graphite powder with the particle size of 53~88 ${\mu}{\textrm}{m}$ was added in 10~15 vol%, had the most increased resistance for the friction and wear which show the worn out amount of 0.4~0.6$\times$10-3 $\textrm{cm}^2$, and the value of the bending strength is 380~520 kg/$\textrm{cm}^2$.

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The Effect of Particle Size on the Detergency of Particulate Soil (고형오구 입자크기가 고형오구의 세척성에 미치는 영향)

  • Mun, Mi-Hwa;Kang, In-Sook
    • Journal of the Korean Society of Clothing and Textiles
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    • v.34 no.4
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    • pp.653-662
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    • 2010
  • This study investigates the effect of particle size on the detergency of particulate soil using an $\alpha-Fe_2O_3$ particle as the model. Monodispersed spherical $\alpha-Fe_2O_3$ particles were prepared by the hydrothermal aging of an acidic $FeCl_3$ and HCl solution. The $\xi$-potential of PET fiber was measured by the streaming potential method. The potential energy of interaction between the particle and fiber was calculated using the heterocoagulation theory for a sphere-plate model. The $\xi$-potential of PET fiber and potential energy of interaction between particles and fiber increased with a decreasing particle size in a DBS solution. However, in the nonionic surfactant solution, the $\xi$-potential signs of PET fiber and $\alpha-Fe_2O_3$ particles were (-) and (+), respectively; there was no repulsive power between the particles and substrate. The adhesion of particles to the fabric increased with increasing particle size in the anionic surfactant solution and their removal from the fabric increased with a decreasing particle size. The adhesion of particles to the fabric and their removal from the fabric was biphasic with a maximum and minimum at 0.1% concentration of the surfactant solution. In the nonionic surfactant solution the adhesion of particles to fabric and their removal from the fabric were greater than the ones in the anionic surfactant DBS solution.

Simulation study on draft force prediction of moldboard plow according to cohesive soil particle size using the discrete element method (이산요소법을 활용한 점성토 환경에서의 토양 입자 크기에 따른 몰드보드 플라우 견인력 예측 시뮬레이션)

  • Min Seung Kim;Bo Min Bae;Dae Wi Jung;Jang Hyeon An;Se O Choi;Sang Hyeon Lee;Si Won Sung;Yeon Soo Kim;Yong Joo Kim
    • Journal of Drive and Control
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    • v.21 no.3
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    • pp.46-55
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    • 2024
  • In the agricultural machinery field, load analysis is mostly done through field tests. However, field tests are time-consuming and costly. There are also limitations in test conditions due to weather conditions. To overcome these environmental limitations, research on load analysis through simulation in a virtual environment is actively being conducted. This study aimed to select the most appropriate soil particle size for modeling by analyzing the effect of soil particle size on the prediction of draft force of the implement using simulation and soil particle modeling in a virtual environment with the discrete element method (DEM) software. The accuracy was verified by simulating the draft force for the same moving speed by soil particle size. For soil particle modeling, DEM soil modeling was performed by designing soil property measurement procedure. Soil particle correction was performed with a virtual vane shear test. Average DEM simulation results showed an error of 27.39% (19.43~40.66%) compared to actual measured data. The possibility of improvement was confirmed through additional research. Results of this study provide useful information for selecting soil particle size in soil modeling using DEM from the perspective of agricultural machinery research.

Characteristics of Particle Deposition onto the Cleanroom Wall Panel with Electrostatic Voltages (정전압에 따른 클린룸 벽체에서의 입자침착 특성)

  • Noh, Kwang-Chul;Son, Young-Tae;Kim, Jong-Jun;Oh, Myung-Do
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.18 no.12
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    • pp.1033-1038
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    • 2006
  • We carried out the experiments on particle deposition onto the cleanroom wall panels. And then we investigated the particle deposition characteristic coefficients for electrostatic voltages and particle size. It was found that there is little difference in characteristics of the particle deposition between the steel panel and the anti-static coating panel. In case of that the particle size is under $1.0{\mu}m$, the particle deposition characteristic coefficient becomes larger as the electrostatic voltage induced to the cleanroom wall panel is increasing. Where in case of that the particle size is over $3.0{\mu}m$, the particle deposition characteristic coefficients do not show any differences with the electrostatic voltages. It is due to that the electrostatic force is the major particle transport mechanism for submicron particles, while the gravitational settling is the major particle transport mechanism for overmicron particles when the electro-static voltages are induced to the cleanroom wall panel.

The effect of particle size on tool wear of SiCp-reinforced metal matrix composite

  • Sahin, Y.;Sur, G.
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.237-239
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    • 2002
  • The effect of particle sizes of the metal matrix composites containing 10 wt.%SiCp was investigated with using various tools. The results showed that tool life decreased considerably with increasing particle size and cutting speed. The wear resistance of TiC-coated tools was considerably higher than that of the other tools. It was observed that abrasive wear was the main responsible mechanism for wear of the tool thermal cracks were at high speed while a built-edge formation was also evident at lower speed.

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