• 제목/요약/키워드: Over-preparation

검색결과 1,029건 처리시간 0.034초

광전자회절을 이용한 Ni(111)(2×2)-O/CO의 표면 흡착 구조: 시편준비의 온도 의존성 (Quantitative Structure Determination of Ni(111)(2×2)-O/CO: temperature Dependent Study)

  • 강지훈
    • 한국자기학회지
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    • 제16권1호
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    • pp.92-97
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    • 2006
  • C 1s에너지 스캔 방식 광전자회절을 이용하여 Ni(111)$(2\times2)$-O/CO에 공동 흡착된 CO의 흡착구조를 시편의 준비 온도에 따라 연구하였다. 실온근방에서 준비한 시편의 경우 표면진동분광결과와 잘 일치하는 결과인 atop 흡착을 얻었으나, 저온시편의 경우 atop흡착 외에 상당량의 CO가 hollow 흡착으로 해석되었다. 일부분의 hollow 흡착 CO는 미리 흡착된 산소의 precoverage가 적거나 없는 곳에 흡착된 곳으로 해석된다. 유사한 결과가 C 1s와 O 1s를 통행 얻은 고 분해능 XPS에서 얻은 흡착위치에서도 확인되었다.

노인의 노후준비가 삶의 만족도에 미치는 영향과 사회적 지지의 매개효과 (The Effects of Preparation for Aging of the Elderly on Life Satisfaction & Mediating Effects of Social Support)

  • 송기영
    • 한국콘텐츠학회논문지
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    • 제19권9호
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    • pp.593-600
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    • 2019
  • 본 연구는 노인의 삶의 질 향상에 대한 관심으로부터 출발하여 인구의 노령화에 따라 늘어난 노년기에 대한 준비로 삶의 만족도 수준을 높이는 것을 궁극적인 목표로 삼았다. 이를 위해 노후준비의 하위 유형을 신체적 노후준비, 경제적 노후준비, 정서 사회적 노후준비로 구성하여 이를 다중 독립변인으로 설정하였다. 또한 사회적 지지를 매개변인, 삶의 만족도를 종속변인으로 하여 각 변인 간 구조적 관계를 밝히고, 노후준비의 하위유형과 삶의 만족도 간 사회적 지지가 매개효과를 갖는지 검증하고자 하였다. 본 연구의 대상은 국민노후보장패널(Korean Retirement and Income Study: KReIS) 3차 및 5차 부가조사 자료로부터 추출한 65세 이상의 노인 4,058명이다. 자료 분석을 위해서는 SPSS 25.0과 SPSS PROCESS macro v2.16을 활용하였다. 연구결과 노후준비의 하위 유형 중 정서 사회적 노후준비는 삶의 만족도에 유의미한 직접효과를 발생시켰을 뿐만 아니라, 사회적 지지의 매개를 통해서도 삶의 만족도에 영향을 미치는 결과를 보였다. 이러한 연구결과를 바탕으로 노인의 삶의 만족도를 달성하는 데 중요한 변수인 정서 사회적 노후준비와 사회적 지지 제고를 위한 사회복지 정책 및 실천적 방안을 제언하였다.

LC-MS/MS를 이용한 조피볼락 근육에서 구충제 febantel 및 그 대사체들의 정량분석을 위한 시료 전처리 방법의 비교 분석 (Comparison of sample preparation methods for quantification of febantel, an anthelmintic agent, and its metabolites in rockfish (Sebastes schlegeli) muscle using liquid chromatography-tandem mass spectrometry)

  • 임재웅;권인영;김태호;김위식;강소영
    • 한국어병학회지
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    • 제34권2호
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    • pp.261-269
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    • 2021
  • This study presents the evaluation of sample extraction and purification procedure for the determination of residues of febantel and its metabolites, fenbendazole, oxfendazole and oxfendazole sulfone in rockfish (Sebastes schlegeli) muscle using liquid chromatography-tandem mass spectrometry. Residues of febantel and its metabolites in rockfish muscle were analyzed using each different sample preparation method from Korean Food Standards Codex (KFSC), Food Safety and Inspection Service (FSIS, USA), and the modified FSIS method using QuEChERS kit (FSIS-Q), respectively. Each method was compared for mean recoveries and repeatabilities. Since FSIS-Q showed higher repeatabilities (coefficient of variation, CV of 2.4%~10.9%) than those of FSIS method (CV of 4.6%~17.5%), recoveries from FSIS-Q were compared with those from KFSC method. FSIS-Q showed significantly higher recoveries of 83.1%~110.1% (P < 0.05) than those from KFSC method of 64.7%~107.4%. In addition, FSIS-Q showed a good linearity over the range of 2.5~200 ㎍/kg, and excellent sensitivities with limit of detection of 0.46~0.71 ㎍/kg and limit of quantification of 1.08~2.15 ㎍/kg. Although all the sample preparation methods turned out to be able to meet CODEX guideline for all the compounds, FSIS method and FSIS-Q validated in this study could be applied to screening and quantification for residues of febantel and its metabolites in rockfish muscle with efficient preparation procedures.

공무원들의 노후생활에 대한 인식 및 준비정도 (Degree of Recognition and Preparation for the Old Age Life of Public Servants)

  • 박현숙;임정도
    • 한국콘텐츠학회논문지
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    • 제12권12호
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    • pp.248-260
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    • 2012
  • 부산, 울산, 경남지역에 근무하는 공무원 중 편의표본 추출한 30대 및 40대를 중심으로 731명을 대상으로 하여 노후 생활에 대한 인식 및 준비정도 등을 조사하였다. 노후의 1차적 부양책임은 본인 및 배우자라는 응답은 83.9%였다. 노후생활 지역은 대도시 근교의 전원생활이라는 응답이 25.9% 였다. 노후생활에 예상되는 경제력 문제점에 대한 인식은 매우 문제가 될 것이다라는 응답이 33.0% 였다. 여가활동 문제점에 대한 인식에서는 그저 그렇다라는 응답이 43.4% 였다. 공무원들이 노후생활 경제력에 대해 나름대로 준비하고 있다는 응답은 75.0%였다. 노후생활의 공적연금의 충족정도는 부족하다가 56.0%, 적정하다가 17.2%, 모르겠다가 26.8%였다. 공무원들의 노후생활의 공적연금의 충족정도는 부족하다(409명 56.0%)가 이였으며, 공적연금의 충족정도에 따른 노후생활에 대한 경제적 준비내용은 먼저 공적연금 외 경제적 대책 준비정도와 공적연금의 충족정도 군별로 비교한 결과 부동산 투자, 부족분 자녀도움, 자신의 보유자산 이용에서 유의한 차이가 있었다. 분석결과, 중년층이 노후의 준비를 하는 데 있어서는 개인 스스로 노후준비의 필요성을 인식하고 장 단기적인 관점에서 경제적 신체적 사회적 측면에서 노후 대책을 마련하고 실천해 나가는 것이 가장 중요하였다.

초임부의 교육 요구와 만족도에 관한 연구 (A Study on the Educational Needs and Satisfaction of Primigravida during the Antepartal Period)

  • 전영자
    • 여성건강간호학회지
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    • 제4권2호
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    • pp.187-202
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    • 1998
  • This study was carried out to identify the difference between educational needs and levels of satisfaction of primigravida during the antepartum period. The goal of the study was to obtain data needed to develope educational programs and to improve the nursing quality for antepartal clients. The subjects were 106 primigravida who attend antenatal clinic at 3 general hospitals in the Seoul area. The data was gathered using a questionnaire which, consist of 71 items, was developed by the researcher from May 4 to June 3, 1998. Results found are as follows : 1. The characteristics of subjects : The majority of subjects were aged 25-29 years(73.6%), college graduates(61.3%), jobless(68.9%), had no religion(38.7%), attended antenatal clinic regularly(91.5%), duration of pregnancy was 38-39 weeks(49.06%), pregnancy was planned(67%), and 42.5% have had some sort of prenatal education. 2. Over all level of educational needs was relatively high(Mn. 3.97) but the level of satisfaction was of average level(Mn. 3.01). Therefore, differences between the level of educational needs and satisfaction was significant(P=.0001). 3. The educational needs by category, the highest need was on birth preparation(Mn. 4.18), self care of the mother and infant care(Mn 4.10), health maintenance and promotion(Mn. 3.79), the lowest was care of discomfort(Mn 3.66). The level of satisfaction was higher on postpartum self care(Mn 3.15), but the lowest was infant care(Mn 2.84). Differences between educational needs and satisfaction by categories was significant(P=.0001). 4. Relationship between educational needs and levels of satisfaction among primigravida of different characteristics were as follows : 1) Educational needs of minor discomforts area were significantly high among age of 25-29(P=.0108), and over 35 years of age, was satisfied on preparation of labor & delivery, postpartum self care (P=.036, .02). 2) With regard to different level of education, middle school graduates had higher educational needs on discomfort care and postpartum self care(P=.0014, .014). College graduates have had higher educational needs on health maintenance(P=.008) and were more satisfied on preparation of birth(P=.0025) 3) With regard to whether pregnancy was planned or not, no difference was found on educational needs. But the levels of satisfaction was significantly higher in the group of planned pregnancy(discomfort care P=.0454, birth preparation P=.0256, postpartum self care P=.0092). 4) with regard to antenatal education, those who have had some sort of antenatal education, educational needs on birth preparation(P=.0345) was significantly high. And also the levels of satisfaction were significantly higher on every category(P=.0004-.0001). 5) No difference was found on educational needs or level of satisfaction by Job, religions, regularity of antenatal care and complication of pregnancy.

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Preparation and characterization of niobium carbide crystallites

  • Choi, Jeang-Gil
    • 한국결정성장학회지
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    • 제19권3호
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    • pp.125-129
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    • 2009
  • The preparation and characterization of niobium carbide crystallites were investigated in this study, and in particular, the effect of preparation conditions were studied on the synthesis of niobium carbides crystallites. For this purpose, various characterization techniques including x-ray diffraction, BET surface area, and oxygen uptake measurements were employed to characterize the synthesized niobium carbide crystallites. The niobium carbide crystallites were prepared using niobium oxide and methane gas or methane-hydrogen mixture. Using x-ray diffraction a lattice parameter of $4.45{\AA}$ and a crystallite size ranging from $52{\AA}$ to $580{\AA}$ was found. BET surface areas ranged from $3.2\;m^2/g$ to $16.6\;m^2/g$ and oxygen uptake values varied from $0.5{\mu}mol/g$ to $6.1{\mu}mol/g$. It was observed that niobium carbide crystallites were active for ammonia decomposition reaction. While the BET surface area increased with increasing the oxygen uptake, the conversion of ammonia decomposition reaction decreased. These results indicated that the ammonia decomposition over these materials was considered to be structure-sensitive.

환경영향평가 대상사업별 중점평가항목의 도출에 관한 연구 (Study on the Establishing a Guideline for Selecting Major Environmental Factors by the Project Type Criteria in EIA)

  • 성현찬;한상욱
    • 환경영향평가
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    • 제3권1호
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    • pp.9-30
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    • 1994
  • Environmental Impact Assessment System, ever since its enactment in Korea fourteen years ago, has been steadily improved by introduction and implementation of new concepts and methodologies which include Environmental Impact Statement(EIS) preparation technique, selection of environmental factors, and the like. However, current guideline requires that every EIS, regardless of the specifics of the project type or characteristics of the site, must evaluate and study for all twenty-two environmental factors as set forth in the regulation. The situation causes many undesirable problems like; lack of site specific evaluation in most EISs, over-sized EIS drafts, consuming too much time and costs for EIS preparation, and so on. The objectives of this study are: - To establish a set of criteria to classify the types of the projects in terms of features of the project content and the characteristics of the site area. - To establish a guideline for selecting major environmental factors of the project type criteria, and - To provide basic materials for the preparation of complets draft EIS of the Amendment of Environmental Impact Assessment Act.

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GHz 대역용 전파흡수체의 개발 (Development of EM Wave Absorbers for GHz Frequency)

  • 문상현;신승재;김동일;송재만;최정현;김기만
    • 한국항해항만학회:학술대회논문집
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    • 한국항해항만학회 2004년도 춘계학술대회 논문집
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    • pp.17-22
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    • 2004
  • 폐 처리된 Ba, Sr 페라이트를 사용하여 GHz 대역용 전파흡수체를 개발하였다. 도전 손실재인 카본의 첨가에 따른 전파흡수능의 변화와 시편의 뚜께 그리고 시편 제작시 제작온도 변화에 따른 전파흡수능의 변화를 조사하였다. 이와 같은 실험을 통하여 CHz 대역용 Ba, Sr 페라이트 전파흡수체를 개발하는데 있어 카본의 첨가가 매우 유효함을 알았으며, 시편의 제작온도 또한 우수한 전파흡수체를 개발하는데 있어 반드시 고려되어야 함을 밝혔다. 이와 같은 실험을 실시하여 20dB 이상의 전파흡수체를 개발 할 수 있었다.

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제조라인 통합 설계 및 분석(II) - 디지털 가상생산 기술 적용을 통한 지속적인 라인 설계, 분석 및 최적화 프로세스 (The Integrated Design and Analysis of Manufacturing Lines (II) - Continuous Design, Analysis and Optimization through Digital Virtual Manufacturing)

  • 최상수;성낙윤;신연식;노상도
    • 한국CDE학회논문집
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    • 제19권2호
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    • pp.148-156
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    • 2014
  • Generally, over 95% of manufacturing cost is determined in the design and manufacturing preparation step, especially a great part of productivity is determined in the manufacturing preparation step. In order to improve the manufacturing competitiveness, we have to verify the problems that can be occurred in the production step and remove the unnecessary factors in the manufacturing preparation step. Thus, manufacturing industries are adopting digital manufacturing system based on modeling & simulation. In this paper, we introduce e-FEED system (electronic based Front End Engineering and Design) that is the integrated design and analysis system for optimized manufacturing line development based on simulation automation and explain the work process (Design, Analysis and Optimization) about manufacturing line development using e-FEED system. Also, the effect is described through the real implementation cases.

전통 밑반찬의 인지도와 이용실태에 관한 조사연구 I - 장아찌류- (A study on the knowledge and utilization of Korea traditional basic side dishes I -Jangachies-)

  • 윤계순
    • 한국식생활문화학회지
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    • 제10권5호
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    • pp.457-463
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    • 1995
  • This study was undertaken to investigate the knowledge and the use of Korea traditional basic side dishes, Jangachies, by housewives. Among the 58 kinds Jangachies, the most well-known Jangachies (above 80% of subjects) turned out to be Perilla leaf, Red pepper leaf, Garlic, Young stem of garlic, Green red leaf, Cucumber and dried Radish Jangachi in the order. In cooking experience of Jangachi, 40% of subjects in Perilla leaf, 28.0% in Green red pepper, 24.8% in Garlic and 24.1% in Red pepper leaf Jangachi have cooked frequently. The proportion of subjests who has bought the marketed Jangachi products were 51.6%. Major problem of that products was pointed out for a sanitary condition, high price and poor taste. If marketed Jangachies were improved over the aspects, the proportion of subjects who would buy the products was 76.2%. The frequency of Jangachi intake was very low on a average due to too salty taste and the difficulty in preparation. The older in age, the more in interest level for Jangachi (p<0.05). 39.6% of subject have had preparation ability of Jangachies. With increasing age (p<0.01), decreasing education level (p<0.01) and those who live in rural area (p<0.05), preparation ability of Jangachi tended to be higher.

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