• 대한화학회지
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• 제45권2호
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• pp.143-148
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• 2001

본 연구에서는 작은 양의 시료를 분석할 수 있는 이온 크로마토그래피용 open tubular capillary 컬럼을 개발하였다. 내경이 작은 모세관 컬럼을 사용하는 경우 이동상의 유속은 보통 1~10㎕/min 정도 되고 컬럽의 길이는 1.0~5.0m 정도이다. 컬럼은 fused silica 모세관(내경 : 50㎛)과 DMEOHA latex particles를 이용하여 만들었다. 또한 이런 모세관 컬럼에 맞는 새로운 전도도 셀과 억압장치도 함께 개발하여 사용하였다. 이 모세관 컬럼을 이용하여 실제 음이온들(fluoride, nitrite, chlorate, phosphate, sulfate)을 분석한 결과재현성 있고 좋은 크로마토그램을 얻었다.

• 한국재난관리표준학회지
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• 제2권4호
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• pp.49-57
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• 2009

대구경 강관을 이용한 지하구조물 공사방법은 교통지연 및 안전사고 가능성이 높은 지하시설물 공사에 대해서 지상 교통상황에 영향을 최소화 할 수 있는 비개착 터널공법으로 시공단계별 구조적 안전성 확보가 중요하다. 본 연구에서는 상용구조해석 프로그램인 ANSYS를 이용하여 공법의 주요 부재인 대구경 강관의 관경별 구조적 거통특성을 분석하였다. 또한, 위험시공단계를 선정하고 위험시공단계에서의 웅력집중부위의 응력상태를 검토하였다. 마지막으로 관경 및 관 두께에 따른 구조물의 거동과 응력상태 변화를 확인하여 효율적인 대구경 강관의 사용을 제안하였다.

• Bulletin of the Korean Chemical Society
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• 제27권9호
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• pp.1459-1462
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• 2006

• Bulletin of the Korean Chemical Society
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• 제35권10호
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• pp.3115-3118
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• 2014

• Steel and Composite Structures
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• 제6권2호
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• pp.103-122
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• 2006

The capacity of tubular truss chords subjected to concentrated reaction forces in the vicinity of the open end (i.e., the bearing region) is not directly treated by existing design specifications; although capacity equations are promulgated for related tubular joint configurations. The lack of direct treatment of bearing capacity in existing design specifications seems to represent an unsatisfactory situation given the fact that connections very often control the design of long-span tubular structures comprised of members with slender cross-sections. The case of the simple-span overhead highway sign truss is studied, in which the bearing reaction is applied near the chord end. The present research is aimed at assessing the validity of adapting existing specifications' capacity equations from related cases so as to be applicable in determining design capacity in tubular truss bearing regions. These modified capacity equations are subsequently used in comparisons with full-scale experimental results obtained from testing carried out at the University of Pittsburgh.

• Bulletin of the Korean Chemical Society
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• 제33권5호
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• pp.1664-1668
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• 2012

In this study, we have expanded the applicability of the pre-established generalized preparation protocol to MIPs with a neutral template. The ($4S,5R$hyl-5-phenyl-2-oxazolidinone MIP layer was formed inside a pretreated and silanized fused silica capillary, and its chiral separation performance was examined. Optimization of chiral separation was also carried out. This is the very first report of somewhat successful application of the generalized preparation protocol to a MIP with a genuine neutral template.

• Steel and Composite Structures
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• 제5권1호
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• pp.49-70
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• 2005

This paper reports on finite element analysis techniques that may be applied to the study of circular hollow structural sections and related bearing connection geometries. Specifically, a connection detail involving curved steel saddle bearings and a Structural Tee (ST) connected directly to a large-diameter Hollow Structural Section (HSS) truss chord, near its open end, is considered. The modeling is carried out using experimentally verified techniques. It is determined that the primary mechanism of failure involves a flexural collapse of the HSS chord through plastification of the chord wall into a well-defined yield line mechanism; a limit state for which a shell-based finite element model is well-suited to capture. It is also found that classical metal plasticity material models may be somewhat limited in their applicability to steels in fabricated tubular members.

• Steel and Composite Structures
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• 제22권6호
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• pp.1465-1486
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• 2016

Conventional plate I-girders are sensitive to local buckling of the web when they are subjected mainly to shear action because the slenderness of the web in out-of-plane direction is much bigger. The local buckling of the web can also cause the distorsion of the plate flange under compression as a thin-walled plate has very low torsional stiffness due to its open section. A new I-girder consisted of corrugated web, a concrete-filled rectangular tubular flange under compression and a plate flange under tension is presented to improve its resistance to local buckling of the web and distorsion of the flat plate flange under compression. Experimental tests on a conventional plate I-girder and a new presented I-girder are conducted to study the failure process and the failure mechanisms of the two specimens. Strain developments at some critical positions, load-lateral displacement curves, and load-deflection curves of the two specimens have all be measured and analyzed. Based on these results, the failure mechanisms of the two kinds of I-girders are discussed.

• 한국터널지하공간학회 논문집
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• 제6권4호
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• pp.345-356
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• 2004

지하구조물을 축조하는 공법으로 기존에 가장 많이 사용해 온 것이 개착식 공법이나, 지상교통 흐름을 방해하고 공사소음 및 주변 지반의 침하로 인한 민원 발생 등 많은 문제점을 야기해 왔다. 많은 경우에 있어 지중에 매설된 상수도관 하수도관 도시가스관 고압 전력구 통신 케이블 등 지중 매설물의 위치가 정확하게 파악되지 않아서 안전한 시공에 어려움이 크고, 개착공사 시 지하지장물의 이설로 인한 공지지연 및 추가공사비가 소요될 것으로 판단되다. 따라서 본 논문에서는 기존 지하구조물 축조공법을 개선하여 슬래브강관과 PC벽체 트렌치를 이용한 터널축조공법 (T.R.c.M.)을 서울지하철 현장에 적용한 시공사례를 소개하고자 한다. 연구결과, T.R.c.M.공법은 진동과 소음을 최소화하여 주변환경과 교통의 흐름에 전혀 지장을 주지 않고 안정적으로 터널을 축조할 수 있는 공법임을 알 수 있었다.

• Food Science and Biotechnology
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• 제14권4호
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• pp.456-460
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• 2005

To enforce the maximum residue limit for residual hexane (0.005 g/kg) in commercially available Korean vegetable oil, convenient and accurate quantification methods were investigated. Using dual surrogate standards, pentane and heptane were dissolved in ethanol, and then added to hexane-tree sunflower oil for setting up the calibration curve. Gas Chromatograph-Flame Ionization Detector with a porous layer open tubular column, indicated good chromatographic separation of hexane from other inhibiting matrix components. The lowest calibration level was $0.5\;{\mu}g/g$, not exceeding a relative standard deviation of 10% (RSD%), and 1.0\;{\mu}g/g$ not exceeding a deviation of 22% RSD% using heptane as an internal standard for the Static headspace analysis by using a headspace auto-sampler and manual injection, respectively. The residual hexane was detected in nine of the samples among 87 vegetable oil samples purchased on the local market.