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http://dx.doi.org/10.5012/bkcs.2012.33.5.1664

Open Tubular Molecular Imprinted Polymer Fabricated in Silica Capillary for the Chiral Recognition of Neutral Enantiomers in Capillary Electrochromatography  

Yang, Song-Hee (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University)
Zaidi, Shabi Abbas (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University)
Cheong, Won-Jo (Department of Chemistry, Nano Fine Center, and Institute of Basic Research, Inha University)
ALOthman, Zeid A. (Department of Chemistry, College of Science, King Saud University)
ALMajid, Abdullah M. (Department of Chemistry, College of Science, King Saud University)
Publication Information
Bulletin of the Korean Chemical Society / v.33, no.5, 2012 , pp. 1664-1668 More about this Journal
Abstract
In this study, we have expanded the applicability of the pre-established generalized preparation protocol to MIPs with a neutral template. The ($4S,5R$hyl-5-phenyl-2-oxazolidinone MIP layer was formed inside a pretreated and silanized fused silica capillary, and its chiral separation performance was examined. Optimization of chiral separation was also carried out. This is the very first report of somewhat successful application of the generalized preparation protocol to a MIP with a genuine neutral template.
Keywords
Neutral template; Molecule imprinted polymer; Chiral separation; Open tubular capillary; Capillary electrochromatography;
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