• Journal of the Korean Chemical Society
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• v.45 no.2
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• pp.143-148
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• 2001

In this study, open tubular capillary columns for ion charomatography were developed to analyze trace amount of ions in samples. When small I,D. capillary column length is 1.0~5.0 m. The capillary columns were made using fused silica capillary(I.D:50㎛) and DMEOHA latex particles. The new conductivity cell and suppressor were also developed and made for capillary column ion chromatography. When several anions(fluoride, nitrite, nitale,chlorate,phosphte, sulfate) were analyzed using these capillary columns. reproducible and good chromatograms were obtained.

• Journal of Korean Society of societal Security
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• v.2 no.4
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• pp.49-57
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• 2009

The development and use of underground space in the city have been expanded considerably worldwide due to the growing population and traffic. Because the construction of underground causes some problems including traffic jam and safety accidents, the non-open excavation construction method are commonly used. NTR (New Tubular Roof) method which is one of the non-open excavation method is investigated in this study. The structural safety of underground structures by using NTR method is evaluated by ANSYS 9.0. The tubular roof according to diameters are analysed by ANSYS 9.0 at critical construction step. Finally, according the diameter and thickness of tubular roof the stress nad dispacement are analyzed and then the The efficient use of tubular roof is suggested from relationship between tubular's thickness and stress condition.

• Bulletin of the Korean Chemical Society
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• v.27 no.9
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• pp.1459-1462
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• 2006

• Bulletin of the Korean Chemical Society
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• v.35 no.10
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• pp.3115-3118
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• 2014

• Steel and Composite Structures
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• v.6 no.2
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• pp.103-122
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• 2006

The capacity of tubular truss chords subjected to concentrated reaction forces in the vicinity of the open end (i.e., the bearing region) is not directly treated by existing design specifications; although capacity equations are promulgated for related tubular joint configurations. The lack of direct treatment of bearing capacity in existing design specifications seems to represent an unsatisfactory situation given the fact that connections very often control the design of long-span tubular structures comprised of members with slender cross-sections. The case of the simple-span overhead highway sign truss is studied, in which the bearing reaction is applied near the chord end. The present research is aimed at assessing the validity of adapting existing specifications' capacity equations from related cases so as to be applicable in determining design capacity in tubular truss bearing regions. These modified capacity equations are subsequently used in comparisons with full-scale experimental results obtained from testing carried out at the University of Pittsburgh.

• Bulletin of the Korean Chemical Society
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• v.33 no.5
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• pp.1664-1668
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• 2012

In this study, we have expanded the applicability of the pre-established generalized preparation protocol to MIPs with a neutral template. The ($4S,5R$hyl-5-phenyl-2-oxazolidinone MIP layer was formed inside a pretreated and silanized fused silica capillary, and its chiral separation performance was examined. Optimization of chiral separation was also carried out. This is the very first report of somewhat successful application of the generalized preparation protocol to a MIP with a genuine neutral template.

• Steel and Composite Structures
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• v.5 no.1
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• pp.49-70
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• 2005

This paper reports on finite element analysis techniques that may be applied to the study of circular hollow structural sections and related bearing connection geometries. Specifically, a connection detail involving curved steel saddle bearings and a Structural Tee (ST) connected directly to a large-diameter Hollow Structural Section (HSS) truss chord, near its open end, is considered. The modeling is carried out using experimentally verified techniques. It is determined that the primary mechanism of failure involves a flexural collapse of the HSS chord through plastification of the chord wall into a well-defined yield line mechanism; a limit state for which a shell-based finite element model is well-suited to capture. It is also found that classical metal plasticity material models may be somewhat limited in their applicability to steels in fabricated tubular members.

• Steel and Composite Structures
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• v.22 no.6
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• pp.1465-1486
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• 2016

Conventional plate I-girders are sensitive to local buckling of the web when they are subjected mainly to shear action because the slenderness of the web in out-of-plane direction is much bigger. The local buckling of the web can also cause the distorsion of the plate flange under compression as a thin-walled plate has very low torsional stiffness due to its open section. A new I-girder consisted of corrugated web, a concrete-filled rectangular tubular flange under compression and a plate flange under tension is presented to improve its resistance to local buckling of the web and distorsion of the flat plate flange under compression. Experimental tests on a conventional plate I-girder and a new presented I-girder are conducted to study the failure process and the failure mechanisms of the two specimens. Strain developments at some critical positions, load-lateral displacement curves, and load-deflection curves of the two specimens have all be measured and analyzed. Based on these results, the failure mechanisms of the two kinds of I-girders are discussed.

• Journal of Korean Tunnelling and Underground Space Association
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• v.6 no.4
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• pp.345-356
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• 2004

Open-cut method has been widely used to construct underground structures, but it causes several problems such as traffic congestion and public resentment resulting from severe construction noise and ground settlement. In many cases, it is very difficult to build underground structures safely due to the unknown locations of buried facilities such as water pipes, drainage pipes, gas pipes and high-pressure cable conduits etc. Also in open-cut method, moving buried facilities causes additional cost and extension of construction period. Therefore, this paper is to present a case study in which Tubular Roof construction Method (T.R.c.M.), a newly developed construction method for underground structures using slab steel pipes and PC wall trench, is applied for the construction of a subway tunnel in Seoul. As a result, it is found that T.R.c.M. is a construction method by which tunnels can be constructed safely without any effect on the surrounding environment and traffic flow due to the minimized construction vibration and noise.

• Food Science and Biotechnology
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• v.14 no.4
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• pp.456-460
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• 2005

To enforce the maximum residue limit for residual hexane (0.005 g/kg) in commercially available Korean vegetable oil, convenient and accurate quantification methods were investigated. Using dual surrogate standards, pentane and heptane were dissolved in ethanol, and then added to hexane-tree sunflower oil for setting up the calibration curve. Gas Chromatograph-Flame Ionization Detector with a porous layer open tubular column, indicated good chromatographic separation of hexane from other inhibiting matrix components. The lowest calibration level was $0.5\;{\mu}g/g$, not exceeding a relative standard deviation of 10% (RSD%), and 1.0\;{\mu}g/g$ not exceeding a deviation of 22% RSD% using heptane as an internal standard for the Static headspace analysis by using a headspace auto-sampler and manual injection, respectively. The residual hexane was detected in nine of the samples among 87 vegetable oil samples purchased on the local market.