• Proceedings of the Korean Vacuum Society Conference
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• 2015.08a
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• pp.109.2-109.2
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• 2015

Graphene, as a single layer of $sp^2$-bonded carbon atoms packed into a 2D honeycomb crystal lattice, has attracted much attention due to its outstanding properties such as high carrier mobility, chemical stability, and optical transparency. In order to synthesize high quality graphene, transition metals, such as nickel and copper, have been widely employed as catalysts, which need transfer to desired substrates for various applications. However, the transfer steps inevitably induce defects, impurities, wrinkles, and cracks of graphene. Here, we report a facile transfer-free graphene synthesis method through nickel and carbon co-deposited layer, which does not require separately deposited catalytic nickel and carbon source layers. The 100 nm NiC layer was deposited on the top of $SiO_2/Si$ substrates by nickel and carbon co-deposition. When the sample was annealed at $1000^{\circ}C$, the carbon atoms diffused through the NiC layer and deposited on both sides of the layer to form graphene upon cooling. The remained NiC layer was removed by using nickel etchant, and graphene was then directly obtained on $SiO_2/Si$ without any transfer process. Raman spectroscopy was carried out to confirm the quality of resulted graphene layer. Raman spectra revealed that the resulted graphene was at high quality with low degree of $sp^3$-type structural defects. Furthermore, the Raman analysis results also demonstrated that gas flow ratio (Ar : $CH_4$) during the NiC deposition and annealing temperature significantly influence not only the number of graphene layers but also structural defects. This facile non-transfer process would consequently facilitate the future graphene research and industrial applications.

• Journal of the Korean Society of Systems Engineering
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• v.12 no.1
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• pp.59-71
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• 2016

The Nuclear and Fossil Steam Turbines record a considerable number of failures annually. Some of these failures reported are as result of blade failure. The failure of the L-0 blade in a Steam Turbine is one of the most reported blade failure in Nuclear and Fossil steam turbines. This paper seeks to identify the best Non Destructive Evaluation (NDE) method or methods to be used in the steam turbine L-0 blades inspection process. The development of systems engineering processes presents an opportunity to apply NDE inspection to the L-0 blades. This process apply computer modelling of the L-0 using ANSYS and by simulating the stresses experienced by the L-0 blade during operation it is possible to identify the most susceptible areas for crack formation and growth. The results from these models compared to industry data for validation. The analysis of these results used to predict the most probable failure location and failure modes. Therefore NDE inspection can be applied to these areas with greater degree of accuracy. This would be beneficial in the increasing the accuracy in the detection of cracks and hence save inspection time and the overall inspection cost. Furthermore, not only the location for crack formation and NDE inspection determined but also best the NDE inspection technique/techniques to be applied appropriately on the L-0 blade are prescribed.

• Journal of the Korean Society for Precision Engineering
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• v.32 no.6
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• pp.529-536
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• 2015

A defect could be generated in bolts for a use of oil filters for the manufacturing process and then may affect to the safety and quality in bolts. Also, fine defects may be imbedded in oil filter system. So it is very important that such defects be investigated and screened during the multiple manufacturing processes. Therefore, in order effectively to evaluate the fine defects, the FEM simulations were performed to make characterization in the crack detection of the bolts and the parameters such as number of turns of the coil, the coil size, applied frequency were calculated based on the simulation results. Simulations were carried out for the defect signal of eddy current probe. Exciter and receiver were utilized. In this paper, the FEM simulations were performed in both bobbin-type and pancake-type probe, both probes were optimized under Eddy current FEM simulations and the results of calculation were discussed.

• Journal of Biosystems Engineering
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• v.42 no.4
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• pp.251-257
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• 2017

Purpose: A chisel mounted on working implement, such as agricultural machinery used in irregular farming conditions, is subjected to highly variable fatigue loading during work. To ensure the safety of the chisel on a working implement for the duration of its service life, fatigue testing must be performed with the proper fatigue test load conditions. In this study, working loads for a chisel were developed by reconstructing loads from strain gage data collected during field tests and used to conduct fatigue tests on the chisel component. Methods: FE analysis with nCode software was utilized to select the proper quantity and locations of strain gages for load measurements. A fatigue test was performed to experimentally verify the fatigue strength of the chisel and to evaluate the validity of the load history developed with the load reconstruction technique. Results: A strain history for the chisel was obtained from data collected during field tests. The data was filtered for the 14-16 km/h speed range, connected, and merged. The chisel load history was developed using the load reconstruction technique. The resulting load history was expressed as a load spectrum using the rain-flow counting method. Conclusions: A fatigue test was conducted on a chisel under a constant load condition with an equivalent load amplitude and number of cycles, as calculated by Miner's Rule for linear damage accumulation. During the fatigue test, there were no cracks at any position. It is concluded that the fatigue test method proposed in this study can be utilized successfully as a durability evaluation method for the chisel.

• Elastomers and Composites
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• v.53 no.3
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• pp.124-130
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• 2018

Recently, microwaves have been used for desulfurization because they can selectively dissociate C-S and S-S bonds present in vulcanized rubber. In this study, we investigated the changes in structural and physical properties of EPDM (Ethylene propylene diene monomer) rubber by irradiating it with microwaves for different durations. The surface chemical composition of the irradiated EPDM rubber was analyzed by FT-IR, XPS, and EDS analyses. It was confirmed by XPS that C-S and S-S S2p peak heights greatly decreased when microwave irradiation was performed for more than 5 min. In the EPDM sample irradiated with microwaves for 10 min, the number of S-O bonds significantly increased owing to oxidation. As the microwave irradiation time was increased, SEM images showed cracks and voids on the EPDM surface. The 20% decomposition temperature of the EPDM rubber sample was investigated by TGA, and it was found to be about $435.23^{\circ}C$ for the EPDM rubber irradiated for 10 min. The crosslinking density of the EPDM rubber was determined by measuring the degree of swelling, and the highest value was observed for the E5 sample irradiated for 5 min. The degree of swelling of the E10 sample irradiated for 10 min was lower than that of the E5 sample. These results indicate that when irradiated with microwaves for more than a certain time, desulfurization occurs and the side chain of the EPDM rubber dissociates and forms additional crosslinking bonds.

• Journal of the Semiconductor & Display Technology
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• v.17 no.4
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• pp.42-45
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• 2018

As The semiconductor decrease from 10 nanometer to 7 nanometer, It is suggested that "More than Moore" is needed to follow Moore's Law, which has been a guide for the semiconductor industry. Fan-Out Wafer Level Package(FOWLP) is considered as the key to "More than Moore" to lead the next generation in semiconductors, and the reasons are as follows. the fan-out WLP does not require a substrate, unlike conventional wire bonding and flip-chip bonding packages. As a result, the thickness of the package reduces, and the interconnection becomes shorter. It is easy to increase the number of I / Os and apply it to the multi-layered 3D package. However, FOWLP has many issues that need to be resolved in order for mass production to become feasible. One of the most critical problem is the warpage problem in a process. Due to the nature of the FOWLP structure, the RDL is wired to multiple layers. The warpage problem arises when a new RDL layer is created. It occurs because the solder ball reflow process is exposed to high temperatures for long periods of time, which may cause cracks inside the package. For this reason, we have studied warpage in the FOWLP structure using commercial simulation software through the implementation of the reflow process. Simulation was performed to reproduce the experiment of products of molding compound company. Young's modulus and poisson's ratio were found to be influenced by the order of influence of the factors affecting the distortion. We confirmed that the lower young's modulus and poisson's ratio, the lower warpage.

• Korean Journal of Metals and Materials
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• v.50 no.4
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• pp.271-279
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• 2012

9-12% Cr steels have been used in thermal power plants which repeat start and stop operations. Major factors of fatigue life are temperature, frequency, stress ratio, holding time, microstructure, and environment. Normally, fatigue life decreases at high temperature, low frequency, high stress ratio, and long holding time conditions. A Mod.9Cr-1Mo steel, called G91, was developed at ORNL (Oak Ridge National Laboratory, USA) and was adopted as a high-temperature structural material in the ASME Code in 2004. However, its low-cycle fatigue and fatigue crack growth characteristics have been rarely studied. In this work, we have investigated the low-cycle fatigue crack growth behaviors of G91 steel under various test conditions in terms of temperature and stress ratio. As temperature and stress ratio increase, the crack growth rate becomes faster and striation distance also increases. On the other hand, the number of branch cracks decreases.

• The Journal of the Acoustical Society of Korea
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• v.28 no.4
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• pp.308-317
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• 2009

In the present work, a sensor system composed of an oscillator sensor and a Lamb wave sensor is proposed for the purpose of structural health monitoring. The oscillator sensing system detecting the shift of a structural resonant frequency in proportion to the amount of defects in the structure is a pretty sensitive and simple device, but its detectable range is limited to its local zone. The Lamb wave sensor system, however, is applicable to global detection of the defects. This study is aimed at investigating the feasible combination of the two systems to exploits their merits simultaneously. The scheme to use PZT patches as the oscillator sensor as well as the Lamb wave sensor was proposed to identify the position, length and number of cracks by means of TOF and amplitude of signals, and its validity was confirmed through experiments.

• Journal of the Korean Society for Nondestructive Testing
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• v.35 no.3
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• pp.179-184
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• 2015

In this study, the flap fatigue test of a 48 m long wind turbine blade was performed for 1 million cycles to evaluate the characteristics of acoustic emission signals generated from fatigue damage of the wind blades. As the number of hits and total energy continued to increase during the first 0.6 million cycles, blade damage was constant. The rise-time result showed that the major aspects of damage were initiation and propagation of matrix cracks. In addition, the signal analysis of each channel showed that the most seriously damaged sections were the joint between the skin and spar, 20 m from the connection, and the spot of actual damage was observable by visual inspection. It turned out that the event source location was related to the change in each channel's total energy. It is expected that these findings will be useful for the optimal design of wind turbine blades.

• Tunnel and Underground Space
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• v.14 no.4
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• pp.248-260
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• 2004

Damage in brittle rock due to stress increase starts from initiation of microcracks, and then results in failure by forming macro failure planes due to propagation and coalescence of these discrete cracks. Conventionally, continuum approaches using macro-failure criteria or a number of elasto-plastic models have been major solution to implement rock damage and failure. However, actual brittle failure processes can be better described in phenomenological approach if initiation and propagation of discrete fractures are explicitly considered. This study presents damage and failure process of rock using a boundary element code, FRACOD, which has been developed to model fracturing process of rocks. Through a series of numerical uniaxial compressive tests, the feasibility of the developed model was verified, and realistic rock failure process was reproduced considering scale effects in rocks. In addition, the fracturing process and the corresponding rock damage in the vicinity of deep shaft in rock mass were presented as an application of this approach. This approach will be expected to contribute to finding better engineering solutions for the analysis of stability problems in brittle rock masses.