• Title/Summary/Keyword: Nondestructive Technique

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Determination of Uranium in Groundwater by Instrumental Neutron Activation Analysis (중성자방사화분석에 의한 지하수중 우라늄의 정량)

  • 정용삼;문종화;정영주;박광원
    • Journal of the Korean Society of Groundwater Environment
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    • v.5 no.4
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    • pp.210-214
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    • 1998
  • In general the concentration of uranium in natural water such as fresh water and sea water is in the range of 0.01∼5 ppb, therefore trace analytical technique is required. The aim of present work is to compare a direct and preconcentration methods by evaporation and to investigate rapid and accurate trace analysis of uranium in groundwater using Instrumental Neutron Activation Analysis (INAA) which are sensitive and nondestructive method. Identification of analytical procedure was carried out using uranium standard solution of the range of 0.5∼100 ppb. In the given concentration, the deviation of calibration curve was less than 2%, and the standard deviation of measured values at each concentration was the range of 2∼12%. The difference of U content with sampling time for the same sample site was about 10.3%. Using this established method, the concentrations of uranium in samples collected at the 17 spring of Choongchung areas were found to be in the range of 1∼80 ppb.

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Development and Evaluation of Parallel Beam Optic for X-ray (엑스선용 평행빔 광학소자 개발 및 평가)

  • Park, Byunghun;Cho, Hyungwook;Chon, Kwonsu
    • Journal of the Korean Society of Radiology
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    • v.6 no.6
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    • pp.477-481
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    • 2012
  • An X-ray diffractometer which has various X-ray optics can give qualitative and quantitative information for a sample using a nondestructive analysis method. A parallel beam optic passes the parallel beam and removes divergent beam generated from an X-ray tube. The parallel beam optic used in the X-ray diffractometer was fabricated by wire cut and grading of stainless steel plates and was evaluated its performance using an X-ray imaging system. The measured parallelization of 6.6 mrad for the fabricated the parallel beam optic was a very close to the expected value of 6 mrad. An X-ray imaging technique for evaluating the parallel beam optics can estimate parallelization for each plate and can be used to other X-ray optics.

Exploratory research on ultra-long polymer optical fiber-based corrosion sensing for buried metal pipelines

  • Luo, Dong;Li, Yuanyuan;Yang, Hangzhou;Sun, Hao;Chen, Hongbin
    • Smart Structures and Systems
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    • v.26 no.4
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    • pp.507-520
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    • 2020
  • In order to achieve effective corrosion monitoring of buried metal pipelines, a Novel nondestructive Testing (NDT) methodology using ultra-long (250 mm) Polymer Optical Fiber (POF) sensors coated with the Fe-C alloy film is proposed in this study. The theoretical principle is investigated to clarify the monitoring mechanism of this method, and the detailed fabrication process of this novel POF sensor is presented. To validate the feasibility of this novel POF sensor, exploratory research of the proposed method was performed using simulated corrosion tests. For simplicity, the geometric shape of the buried pipeline was simulated as a round hot-rolled plain steel bar. A thin nickel layer was applied as the inner plated layer, and the Fe-C alloy film was coated using an electroless plating technique to precisely control the thickness of the alloy film. In the end, systematic sensitivity analysis on corrosion severity was further performed with experimental studies on three sensors fabricated with different metal layer thicknesses of 25 ㎛, 30 ㎛ and 35 ㎛. The experimental observation demonstrated that the sensor coated with 25 ㎛ Fe-C alloy film presented the highest effectiveness with the corrosion sensitivity of 0.3364 mV/g at Δm = 9.32 × 10-4 g in Stage I and 0.0121 mV/g in Stage III. The research findings indicate that the detection accuracy of the novel POF sensor proposed in this study is satisfying. Moreover, the simple fabrication of the high-sensitivity sensor makes it cost-effective and suitable for the on-site corrosion monitoring of buried metal pipelines.

Estimating the Important Components in Three Different Sample Types of Soybean by Near Infrared Reflectance Spectroscopy

  • Lee, Ho-Sun;Kim, Jung-Bong;Lee, Young-Yi;Lee, Sok-Young;Gwag, Jae-Gyun;Baek, Hyung-Jin;Kim, Chung-Kon;Yoon, Mun-Sup
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.56 no.1
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    • pp.88-93
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    • 2011
  • This experiment was carried out to find suitable sample type for the more accurate prediction and non-destructive way in the application of near infrared reflectance spectroscopy (NIRS) technique for estimation the protein, total amino acids, and total isoflavone of soybean by comparing three different sample types, single seed, whole seeds, and milled seeds powder. The coefficient of determination in calibration ($R^2$) and coefficient of determination in cross-validation (1-VR) for three components analyzed using NIRS revealed that milled powder sample type yielded the highest, followed by single seed, and the whole seeds as the lowest. The coefficient of determination in calibration for single seed was moderately low($R^2$ 0.70-0.84), while the calibration equation developed with NIRS data scanned with whole seeds showed the lowest accuracy and reliability compared with other sample groups. The scatter plot for NIRS data versus the reference data of whole seeds showed the widest data cloud, in contrary with the milled powder type which showed flatter data cloud. By comparison of NIRS results for total isoflavone, total amino acids, and protein of soybean seeds with three sample types, the powder sample could be estimated for the most accurate prediction. However, based from the results, the use of single bean samples, without grinding the seeds and in consideration with NIRS application for more nondestructive and faster prediction, is proven to be a promising strategy for soybean component estimation using NIRS.

Compressive Strength Estimation Technique of Underwater Concrete Structures using Both Rebound Hardness and Ultrasonic Pulse Velocity Values (반발경도와 초음파속도를 이용한 수중 콘크리트 구조물의 압축강도 예측 기술)

  • Shin, Eun-Seok;Lee, Ji-Sung;Park, Seung-Hee;Han, Sang-Hun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.18 no.4
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    • pp.118-125
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    • 2014
  • As the earth's current global warming has caused elevation of sea water temperature, size of storms is foreseen to increase and consequently large damages on port facilities are to be expected. In addition, due to the improved processing efficiency of port cargo volume and increasing necessity for construction of eco-friendly port, demands for various forms of port facilities are anticipated. In this study, two kinds of nondestructive evaluation (NDE) techniques (rebound hardness and ultrasonic pulse velocity methods) are investigated for the effective maintenance of smart green harbor system. A new methodology to estimate the underwater concrete strengths is proposed and its feasibility is verified throughout a series of experimental works.

DESIGN OPTIMIZATION OF RADIATION SHIELDING STRUCTURE FOR LEAD SLOWING-DOWN SPECTROMETER SYSTEM

  • KIM, JEONG DONG;AHN, SANGJOON;LEE, YONG DEOK;PARK, CHANG JE
    • Nuclear Engineering and Technology
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    • v.47 no.3
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    • pp.380-387
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    • 2015
  • A lead slowing-down spectrometer (LSDS) system is a promising nondestructive assay technique that enables a quantitative measurement of the isotopic contents of major fissile isotopes in spent nuclear fuel and its pyroprocessing counterparts, such as $^{235}U$, $^{239}Pu$, $^{241}Pu$, and, potentially, minor actinides. The LSDS system currently under development at the Korea Atomic Energy Research Institute (Daejeon, Korea) is planned to utilize a high-flux ($>10^{12}n/cm^2{\cdot}s$) neutron source comprised of a high-energy (30 MeV)/high-current (~2 A) electron beam and a heavy metal target, which results in a very intense and complex radiation field for the facility, thus demanding structural shielding to guarantee the safety. Optimization of the structural shielding design was conducted using MCNPX for neutron dose rate evaluation of several representative hypothetical designs. In order to satisfy the construction cost and neutron attenuation capability of the facility, while simultaneously achieving the aimed dose rate limit (< $0.06{\mu}Sv/h$), a few shielding materials [high-density polyethylene (HDPE)eBorax, $B_4C$, and $Li_2CO_3$] were considered for the main neutron absorber layer, which is encapsulated within the double-sided concrete wall. The MCNP simulation indicated that HDPE-Borax is the most efficient among the aforementioned candidate materials, and the combined thickness of the shielding layers should exceed 100 cm to satisfy the dose limit on the outside surface of the shielding wall of the facility when limiting the thickness of the HDPE-Borax intermediate layer to below 5 cm. However, the shielding wall must include the instrumentation and installation holes for the LSDS system. The radiation leakage through the holes was substantially mitigated by adopting a zigzag-shape with concrete covers on both sides. The suggested optimized design of the shielding structure satisfies the dose rate limit and can be used for the construction of a facility in the near future.

Study on the Manufacturing of Horizontal plate armour Excavated from Mangi-Sanseong(Castle) with X-ray Radiograph (방사선투과시험에 의한 망이산성 횡장판갑(橫長板甲)의 제작기법 연구)

  • Kim, Hyunjoung;Kim, Midori;Oh, Kwangseob;Lee, Yangsu;Cho, Namchul
    • Conservation Science in Museum
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    • v.7
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    • pp.11-24
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    • 2006
  • Plate armour is an important cultural property that reflects the ancient weaponry and the manufacturing technology of ironware as they are. Among the kinds of iron armour, horizontal plate armour has been very rarely excavated, and there are a few artifacts in their unimpaired shape like the plate armour excavated from Mangisanseong. This report reviews the manufacturing technology of ancient plate armour through its radiograph using appliable nondestructive irradiation and scientific conservation treatment. The seven-tiered plate armour excavated from Mangisanseong has ring hinge to open and shut the right side neck guard. The readout result of radiograph proved iron safety guard of Godaepan (a plate that links neck plate and horizontal plate) and leather safety guard of the right armpit with plate overlap and perforation interval; perforations that seem to have linked shoulder strap on wearing the armour are also observed. In particular, it is identified that the perforation and riveting technique avoided the connection of more than three plates with a rivet. This is an important material to illustrate the best use of function of plate armour overcoming its limit.

Study for Development of Nondestructive Inspection Device in Natural Gas Pipeline Using MFL Technology (MFL을 이용한 천연가스 배관용 비파괴 검사장비 개발에 관한 연구)

  • Cho S.H.;Kim D.K.;Park D.J.;Park S.S.;Yoo H.R.;Koo S.J.;Rho Y.W.;Kho Y.T.
    • Journal of the Korean Institute of Gas
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    • v.6 no.1 s.17
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    • pp.10-16
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    • 2002
  • This paper introduces developed prototype intelligent pig which detects corrosion on pipeline by using Magnetic Flux Leakage technology. The 8 inch developed MFL(Magnetic Flux Leakage) pig is composed of 5 yokes which magnetize pipeline wall and 45 Hall sensors which detect MFL signal. The designed MFL modules are analyzed by using magnetic circuit method in order to confirm whether pipeline wall is fully saturated. A variety of artificial defects are manufactured on 8 inch diameter steel pipeline in order to acquire MFL signals. So leakage flux of the axial, radial and circumferential component was acquired as defects. The results of this paper show that design technique for 8 inch MFL pig can be applied to large diameter MFL pig and 0.5mm defect depth can be detected.

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Review paper: Application of the Pulsed Eddy Current Technique to Inspect Pipelines of Nuclear Plants

  • Park, D.G.;Angani, C.S.;Kishore, M.B.;Vertesy, G.;Lee, D.H.
    • Journal of Magnetics
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    • v.18 no.3
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    • pp.342-347
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    • 2013
  • Local wall thinning in pipelines affects the structural integrity of industries, such as nuclear power plants (NPPs). In the present study, a development of pulsed eddy current (PEC) technology that detects the wall thinning of pipelines covered with insulation is reviewed. The methods and experimental results, which have two kinds of probe with a single and double core, were compared. For this purpose, the single and double core probes having one and two excitation coils have been devised, and the differential probe with two Hall sensors has been fabricated to measure the wall thinning in insulated pipelines. The test sample is a stainless steel having different thickness, laminated by plastic insulation to simulate the pipelines in NPPs. The excitation coils in the probe is driven by a rectangular current pulse, the difference of two Hall sensors has been measured as a resultant PEC signal. The peak value of the detected signal is used to describe the wall thinning. The double core probe has better performance to detect the wall thinning covered with insulation; the single core probe can detect the wall thinning up to an insulation thickness of 18 mm, whereas the double probe can detect up to 25 mm. The results show that the double core PEC probe has the potential to detect the wall thinning in an insulated pipeline of the NPPs.

Evaluation of 475 ℃ embrittlement in UNS S32750 super duplex stainless steel using four-point electric conductivity measurements

  • Gutierrez-Vargas, Gildardo;Ruiz, Alberto;Lopez-Morelos, Victor H.;Kim, Jin-Yeon;Gonzalez-Sanchez, Jorge;Medina-Flores, Ariosto
    • Nuclear Engineering and Technology
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    • v.53 no.9
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    • pp.2982-2989
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    • 2021
  • One of the consequences of the 475 ℃ embrittlement of duplex stainless steels is the reduction of the resistance to localized corrosion. Therefore, the detection of this type of embrittlement before the material exhibits significant loss in toughness, and corrosion resistance is important to ensure the structural integrity of critical components under corrosion threats. In this research, conductivity measurements are performed using the alternating current potential drop (ACPD) technique with using a portable four-point probe as a nondestructive evaluation (NDE) method for detecting the embrittlement in a 2507 (UNS S32750) super duplex stainless steel (SDSS) aged at 475 ℃ from as-received condition to 300 h. The electric conductivity results were compared against two electrochemical tests namely double loop electrochemical potentiokinetic reactivation (DL-EPR) and critical pitting temperature (CPT). Mechanical tests and the microstructure characterized using scanning electron microscopy (SEM) imaging are conducted to track the progress of embrittlement. It is shown that the electric conductivity correlates with the changes in impact energy, microhardness, and CPT corrosion tests result demonstrating the feasibility of the four-point probe as a possible field-deployable method for evaluating the 475 ℃ embrittlement of 2507 SDSS.