• Journal of the Korean Society of Propulsion Engineers
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• v.20 no.2
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• pp.11-17
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• 2016

Powder metallurgy nickel based superalloy has been used in a high temperature part of turbine engine for airplane. The fatigue crack growth behavior was investigated using CT specimens for the materials at room temperature(R.T.), $600^{\circ}C$ and $700^{\circ}C$. The direct current potential drop(DCPD) method suggested by ASTM E647 was used to measure the crack length during fatigue crack growth at various stress ratios. The fatigue crack growth rate at R=0.5 was faster than that at R=0.1 for all temperature conditions and increased with the increase of stress ratio and temperature. Fractography was conducted for analysis of fracture mechanism.

• Transactions of Materials Processing
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• v.25 no.4
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• pp.254-260
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• 2016

In this study, hot isostatic pressed Ni-base superalloy was subjected by high-pressure torsion process to improve the dispersion of gamma prime phase, mechanical properties and remove prior particle boundaries. The resulting microstructural size decreases and prior particle boundaries removed with increasing strain by high-pressure torsion process. Moreover, the microhardness values and room temperature tensile strength were enhanced. However, the tensile elongation was decreased as increasing strain due to fast crack propagation along the refined and well dispersed gamma prime particles.

• Journal of Welding and Joining
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• v.35 no.3
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• pp.52-61
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• 2017

Transient liquid phase (TLP) bonding is essential technology to repair micro-cracking on the airfoil of blades and vanes for gas turbines. Understanding of the characteristics of TLP bonding of the superalloys is necessary in the application of the technology for repairing these components. In this study, the focus was on investigating TLP bonding characteristics of ${\gamma}^{\prime}$ precipitation strengthened Ni based superalloy. TLP bonding was carried out with an amorphous filler metal in various bonding conditions, and the microstructural characterization was investigated through optical microscopy (OM) and electron probe micro-analysis (EPMA). The experimantal results explained clearly that bonding temperatures had critical effects on the TLP bonding behaviors, and that isothermal solidication of the joints made at higher temperatures than $1170^{\circ}C$ was controlled by Ti diffusion instead of B.

• Journal of Powder Materials
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• v.23 no.3
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• pp.247-253
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• 2016

In this study, solid solution heat treatment of consolidated nickel-based superalloy powders is carried out by hot isotactic pressing. The effects of the cooling rate of salt quenching, and air cooling on the microstructures and the mechanical properties of the specimens are analyzed. The specimen that is air cooled shows the formation of serrated grain boundaries due to their obstruction by the carbide particles. Moreover, the specimen that is salt quenched shows higher strength than the one that is air cooled due to the presence of fine and close-packed tertiary gamma prime phase. The tensile elongation at high temperatures improves due to the presence of grain boundary serrations in the specimen that is air cooled. On the contrary, the specimen that is salt quenched and consists of unserrated grain boundaries shows better creep properties than the air cooled specimen with the serrated grain boundaries, due to the negative creep phenomenon.

• Korean Journal of Materials Research
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• v.25 no.11
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• pp.630-635
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• 2015

The fatigue strength of a nickel-base superalloy was studied. Stress-controlled fatigue tests were carried out at $700^{\circ}C$ and 5 Hz using triangular wave forms. In this study, two kinds of testing procedures were adopted. One is the conventional tension-zero fatigue test(R = 0). The other was a procedure in which the maximum stress was held at 1000 MPa and the minimum stress was diverse from zero to 1000 MPa at 24 and $700^{\circ}C$. The results of the fatigue tests at $700^{\circ}C$ indicate that the fracture mechanism changed according to both the mean stress and the stress range. At a higher stress range, ${\gamma}^{\prime}$ precipitates are sheared by a/2<110> dislocation pairs coupled by APB. Therefore, in a large stress range, the deformation occurred by shearing of ${\gamma}^{\prime}$ by a/2<110> dislocations, which brought about crystallographic shear fracture. As the stress range was decreased, the fracture mode gradually changed from crystallographic shear fracture to gradual growth of fatigue cracks. At an intermediate stress range, as it became more difficult for a/2<110> dislocation pairs to shear ${\gamma}^{\prime}$ particles, cracks started to propagate in the matrix, avoiding the harder ${\gamma}^{\prime}$ particles. High mean stress induced creep deformation, that is, ${\gamma}^{\prime}$ particles were sheared by {111}<112> slip systems, which led to the formation of stacking faults in the precipitates. Thus, the change in fracture mechanism brought about the inversion of the S-N curves.

• Proceedings of the KSME Conference
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• 2003.11a
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• pp.424-429
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• 2003

Hot gas path components, which are made of nickel based superalloys, are subject to periodic replacement due to degradation of thermomechanical properties that might bring catastrophic failure during normal operation of gas turbine units. In order to rejuvenate the metallurgical condition of the serviced components, heat treating techniques such as solution annealing and aging heat treatments have widely been employed. However, the effectiveness of those typical heat treatments is not apparent enough in terms of quantitative grounds. On the other hand the demand of the rejuvenation heat treatment and hot isostatic pressing (HIP) have constantly been raised by the end users. Therefore it is necessary to verify how the typical heat treating techniques affect to the aged and degraded material. As the result of experimental work in this study, GTD-111 and GTD-222 Ni-based superalloys were collected and analyzed quantitatively through microscopic observation, microhardness evaluation and creep test.

• Journal of the Korea Institute of Information and Communication Engineering
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• v.27 no.1
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• pp.15-26
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• 2023

The purpose of this study is to determine the artificial intelligence-based degradation index from the image of the cross-section of the microstructure taken with a scanning electron microscope of the specimen obtained by the creep test of DA-5161 SX, a nickel-based superalloy used as a material for high-temperature parts. It proposes a new method of quantification and proposes a model that predicts degradation based on Bayesian inference without destroying components of high-temperature parts of operating equipment and a creep life prediction model that predicts Larson-Miller Parameter (LMP). It is proposed that the new degradation indexing method that infers a consistent representative value from a small amount of images based on the geometrical characteristics of the gamma prime phase, a nickel-base superalloy microstructure, and the prediction method of degradation index and LMP with information on the environmental conditions of the material without destroying high-temperature parts.

• Corrosion Science and Technology
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• v.2 no.1
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• pp.53-57
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• 2003

The MarM247 based superalloy (8wt.%Cr- 9wt.%Co- 3wt.%Ta- 1.5wt.%Hf- 5.6%wt.Al- 9.5wt.%W- Bal. Ni) specimens were diffusion aluminized by for types of pack cementation methods, and their coating structure and their high temperature oxidation resistance were investigated. The coated specimens treated at 973K in high aluminum concentration pack had a coating layer containing large hafunium rich precipitates, which were originally included in substrate alloy. After the high temperature oxidation test in air containing 30 vol.% $H_2O$ at 1273K ~ 323K, the deep localized corrosion which reached to the substrate were observed along with these hafnium rich precipitates. On the other hand, the coated specimens treated at 1323K using low aluminum concentration pack showed the coating layer without the large hafunium rich precipitates, and after the high temperature oxidation test at 1273K for 1800 ksec, it did not show the deep localized corrosion. The nickel electroplating before the aluminizing forms thick hafnium free area, and its high temperature oxidation resistance were comparable to platinum modified aluminizing coatings at 1273K.

• Journal of Power System Engineering
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• v.5 no.2
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• pp.57-62
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• 2001

Gas turbine performance is highly dependent on the engine performance which is closely related to the engine materials since they are exposed to severe working environments, i.e, high temperature and high stresses. For this reason, advanced materials with improved properties are required for the engine. The purpose of this research is to develop key materials technologies for aircraft industry and to tester domestic production of related parts. In this paper, the real-time prediction of high temperature creep strength and creep life for nickel-based superalloy Udimet 720(high-temperature and high-pressure the gas turbine engine materials) was performed on round-bar type specimens under pure load at the temperatures of 538, 649 and $704^{\circ}C$.

• Proceedings of the KWS Conference
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• 2005.11a
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• pp.195-197
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• 2005

An intermediate heat exchanger(IHX) is a key component in a next-generation VHTR with process heat applications such as hydrogen production and also for an indirect gas turbine system. Therefore, high temperature brazing with nickel-based filler metal(MBF-15) was carried out to study the joining characteristic(microstucture, joining strength) of nickel-based superalloy(Haynes 230) by vacuum brazing. The experimental brazing was carried out at the brazing process, an applied pressure of about 0.74Mpa and the three kinds of brazing temperatures were 1100, 1150, and $1190^{\circ}C$ with holding time 5 minute. It's joining phenomena were analyzed by optical microscopy and scanning electron microscopy with EPMA. The results of microstructure in the centre-line region of a joint brazed with MBF-15 show a typical ternary eutectic of v-nickel, nickel boride and chromium boride.