• Journal of the Korean Magnetics Society
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• v.4 no.4
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• pp.326-334
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• 1994

This paper describes the fabrication of the hydrophilic magnetic fluid with high viscosity and its application to oil seal apparatus used with the Nd-permanent magnet. The results are as follows. 1) The ultrafine magnetite particles under the size of $100\;{\AA}$ are first coated by the oleic acid ion and again adsorbed by the hydrophilic D. B. S. ion, and there by hydrophilic magnetic fluid with high viscosity could be made by dispersing them into the ethylene glycol. 2) In development of the oil seal apparatus using magnetic fluid and Nd-permanent magnet, the viscosity and magnetic susceptibility show high when the $Fe_{3}O_{4}$ content is over 50%(g/cc) in the fluid, so that such properties could improve highly the capability of oil seal. 3) The maximum of the resisting pressure of the oil seal using the ethylene glycol base magnetic fluid and the Nd-permanent magnet, is about $50\;g/\textrm{cm}^2$, under the condition of this experiment. Therefore the oil seal may not be suitable for the ship engine and the driving part of the automobile, and thus it needs a lot further complementary reserch. However, it is quite favourable for such an oil seal apparatus as speed reducer under the condition of atmospheric pressure.

• The Transactions of the Korean Institute of Electrical Engineers C
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• v.48 no.2
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• pp.147-152
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• 1999

Semiconductor piezoresistive type vibration sensor was fabricated by using semiconductor process and micromachining technology. To measure the micro electromagnetic force between coil and magnet, fabricated vibration sensor was used. Toapply micro electromagnetic force produced from the micro exciter, small-sized NdFeB permanent magnet was attached on the mass of the fabricated vibration sensor. The measured electromagnetic force are about 5~180dyne when the applied sinusoidal current of 1KHz in the range of 1.5~8mA. The measurement of micro electromagnetic forcewas performed by changing the distance between coil and magnet. Output characteristics of micro electromagnetic force according to the applied coil current were linear. Furthermore, output results were used to get the transfer constant that is important to decide the efficiency and the performance of the coil and magnet.

• Transactions of Materials Processing
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• v.10 no.6
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• pp.478-484
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• 2001

Tube Process (TP) is a process to produce permanent magnets using a deformable tube for densification of magnet powder. This process claims that it can accomplish both densification and anisotropication in one step forming. This process is distinguished from other processes since it uses a deformable copper tube for densification of magnet powder. In this paper, simulation has been carried out for tile Tube Process in a closed die considering the compressibility of powdered material, arbitrary curved shape and deformable body contact between Nd-Fe-B magnet powder and a copper tube. Results show that the finite element analysis of the Tube Process plays an important role in the stage of preform design.

• Proceedings of the Korean Magnestics Society Conference
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• 2013.12a
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• pp.110-110
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• 2013

• Journal of Powder Materials
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• v.23 no.6
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• pp.432-436
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• 2016

We investigate the microstructural and magnetic property changes of $DyH_2$, $Cu+DyH_2$, and $Al+DyH_2$ diffusion-treated NdFeB sintered magnets with the post annealing (PA) temperature. The coercivity of all the diffusion-treated magnets increases with increasing heat treatment temperature except at $910^{\circ}C$, where it decreases slightly. Moreover, at $880^{\circ}C$, the coercivity increases by 3.8 kOe in Cu and 4.7 kOe in Al-mixed $DyH_2$-coated magnets, whereas this increase is relatively low (3.0 kOe) in the magnet coated with only $DyH_2$. Both Cu and Al have an almost similar effect on the coercivity improvement, particularly over the heat treatment temperature range of $790-880^{\circ}C$. The diffusivity and diffusion depth of Dy increases in those magnets that are treated with Cu or Al-mixed $DyH_2$, mainly because of the comparatively easy diffusion path provided by Cu and Al owing to their solubility in the Nd-rich grain boundary phase. The formation of a highly anisotropic $(Nd,\;Dy)_2Fe_{14}B$ phase layer, which acts as the shell in the core-shell-type structure so as to prevent the reverse domain movement, is the cause of enhanced coercivity of diffusion-treated Nd-Fe-B magnets.

• Transactions of Materials Processing
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• v.31 no.3
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• pp.124-128
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• 2022

NdFeB magnets have been positioned as the core materials in advanced technologies such as MRI (magnetic resonance imaging), FA (factory automation system), robot, motors, and so on based on the highest magnetic properties. To effectively improve the refined microstructure, the plastic deformation has been known as the good alternatives by the recrystallization. However, it has been regarded as being impossible because of the few slip systems in the RE-Fe-B magnets at room temperature. The purpose of this study was to investigate the possibility of control of grain refinement and magnetic anisotropy of NdFeB alloy powder by the severe plastic deformation. The NdFeB magnet powder was fabricated by gas atomization process, and the powder was pre-compacted at high temperature. The pre-compacted billets were deformed by HPT (high pressure torsion), and then the deformed billets were observed microstructure and magnetic properties. After the HPT process at room temperature, the grain size decreased with increasing because of the melted Nd-rich phase, and the anisotropy of Nd₂Fe₁₄B phase was formed after the HPT process.

• Archives of Metallurgy and Materials
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• v.65 no.4
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• pp.1293-1296
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• 2020

NdFeB anisotropic sintered permanent magnets are typically fabricated by strip casting or melt spinning. In this study, the plastic deformability of an NdFeB alloy was investigated to study the possibility of fabricating anisotropic sintered magnets using gas atomized powders. The results show that the stoichiometric composition Nd₁₂Fe₈₂B₆ softens at high temperatures. The aspect ratio and orientation factor of Nd₁₂Fe₈₂B₆ billets after plastic deformation were found to increase with increasing plastic deformation temperature, particularly above 800℃. This confirms that softening at high temperatures can lead to plastic deformation of Nd₂Fe₁₄B hard magnetic phases.

• Korean Journal of Materials Research
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• v.11 no.7
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• pp.609-614
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• 2001

This study was carried out to obtain a basic data on the production of the Nd-Fe-B system rare earth anisotropic bonded magnet by R-D & HDDR process. The reduction reaction of Nd$_2$O$_3$by metallic Ca and the diffusion reaction of Nd into Fe-B alloy powder were investigated for the production the Nd-Fe-B alloy powder. We concluded that a proper quantity of metallic Ca was about 1.3 times of theoretical equivalent from the yields of Nd and B after the R-D reaction at 100$0^{\circ}C$ for 1h. In the XRD analysis the diffusion reaction of Nd into the center of Fe-B alloy powder for the completed homogenization was required through about 45min at 110$0^{\circ}C$ for the R-D reaction, and also the maximum efficiency on the yield of Nd was obtained with such a condition. Residual Ca and oxygen contents of the final powder sample after washing were detected in 0.17wt% and 0.42wt% by ICP and oxygen analyzer, respectively.

• Resources Recycling
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• v.13 no.6
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• pp.43-48
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• 2004

For the separation of neodymium from NdFeB permanent magnet scrap, the scrap was roasted for oxidizing, and leached with acetic acid followed by fractional crystallization for selective separation. From the analysis results of the leached solution, the optimum condition for the recovery of neodymium was found that leaching temperature, leaching time and pulp density are 80$^{\circ}C$, 3 hours, and 35%, respectively. At this optimum condition, more than 90% of neodymium could be recovered. Concentration of neodymium acetate in acetic acid. The optimum condition for the recovery of neodymium acetate crystal from the leached solution was that the initial leaching solution was evaporated until the remaining volume was about 1/5 of the initial volume. At this condition, 67.5% of neodymium was recovered from the leached solution. The neodymium remaining in the concentrated solution was recovered by reacting it with oxalic acid.

• The KSFM Journal of Fluid Machinery
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• v.6 no.4 s.21
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• pp.45-49
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• 2003

This work focuses on eliminating tiny particles from the coolant in a nuclear pipe line by using a permanent magnet on the exterior surface of the pipe. This method have some merits compared with the currently applied methods and is expected to be applied to most of the pipe lines in the nuclear plant. For instance in this method, a ring is attacked to the exterior surface of the pipe, so that it does not affect the inflows directly. Further, the cost needed in the initial build-up of the facility is low.