• 제목/요약/키워드: Nd:YAG

검색결과 1,085건 처리시간 0.028초

근접장 마이크로파 현미경을 이용한 로돕신의 광학적 특성 연구 (Optical Characterization of Sensory Rhodopsin II Thin Films using a Near-field Scanning Microwave Microscope)

  • 유경선;김송희;윤영운;이기진;이정하;최아름;정광환
    • 한국전기전자재료학회논문지
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    • 제20권1호
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    • pp.80-85
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    • 2007
  • We report the electro-optical properties of the sensory rhodopsin II using a near-field scanning microwave microscope(NSMM). Rhodopsin was known as a photoreceptor pigment with a retinal as a chromophore via a protonated Schiff base and consists of seven ${\alpha}-helical$ transmembrane segments. The sensory rhodopsin II, expressing E. coli UT5600 with endogenous retinal biosynthesis system and purified with $Ni^{-2}-NTA$ affinity chromatography in the presence of 0.02 % DM (Dodecyl Maltoside) from Natronomonas pharaonis. We measured the absorption spectra and the transients difference of sensory rhodopsin II from Natronomonas pharaonis using a UV/VIS spectrophotometer with Nd-Yag Laser (532 nm). The absorption spectra of NpSR II showed a typical rhodopsin spectrum with a left shoulder region and the photointermediates spectra of NpSR II-ground state (${\lambda}max=498\;nm$), NpSR II-M state (${\lambda}max=390\;nm$), and NpSR II-O state (${\lambda}max=550\;nm$) during the photocycle. The observed photocycle reaction was confirmed by measuring the microwave reflection coefficient $S_{11}$ at an operating frequency of f=3.93-3.95 GHz and compared with the results of a photocycle of NpSR II.

High Power Diode Laser을 이용한 금형재료용 구상화 주철의 모서리부 표면처리 (Surface Treatment in Edge Position of Spheroidal Cast Iron for Mold Materials by Using High Power Diode Laser)

  • 황현태;송현수;김종도;송무근;김영국
    • 한국재료학회지
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    • 제19권9호
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    • pp.457-461
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    • 2009
  • Recently, metal molding has become essential not only for automobile parts, but also mass production, and has greatly influenced production costs as well as the quality of products. Its surface has been treated by carburizing, nitriding and induction hardening, but these existing treatments cause considerable deformation and increase the expense of postprocessing after treatment; furthermore, these treatments cannot be easily applied to parts that requiring the hardening of only a certain section. This is because the treatment cannot heat the material homogeneously, nor can it heat all of it. Laser surface treatment was developed to overcome these disadvantages, and, when the laser beam is irradiated on the surface and laser speed is appropriate, the laser focal position is rapidly heated and the thermal energy of surface penetrates the material after irradiation, finally imbuing it with a new mechanical characteristic by the process of self-quenching. This research estimates the material characteristic after efficient and functional surface treatment using HPDL, which is more efficient than the existing CW Nd:YAG laser heat source. To estimate this, microstructural changes and hardness characteristics of three parts (the surface treatment part, heat affect zone, and parental material) are observed with the change of laser beam speed and surface temperature. Moreover, the depth of the hardened area is observed with the change of the laser beam speed and temperature.

요추간판 탈출증에서 레이저를 이용한 경피적 추간판절제술 -증례 보고- (Percutaneous Laser Discectomy in Lumbar Disc Herniation -A case report-)

  • 김원옥;윤덕미;장원석;오경미;김효은
    • The Korean Journal of Pain
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    • 제14권2호
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    • pp.234-238
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    • 2001
  • Percutaneous laser discectomy has potential advantages over conservative therapy and classical open surgery as a minimally invasive procedure, although clinical experiences are limited. We experienced a patient treated with herniated lumbar discs using Nd:YAG laser. A 55-year-old woman complained of severe back pain with sciatica on L4/5 and L5/S1 dermatome for several months. The MRI finding showed bulging discs at L4/5 and L5/S1. Epidural, transsacral and root block treatments were attempted without effect. Under fluoroscopic guidance, a 14 G biopsy needle was inserted into the L4/5 and L5/S1 disc spaces to the margin of the nucleus pulposus. Laser irradiation for vaporization of tissue was performed at 20 W/second to 1200 J. A laser fiber ($600{\mu}m$) was advanced 1 cm from the tip of the needle. At the end of the procedure, the patient began to feel relief of pain (VAS changed from 9 to 4) and was discharged the same day after staying 2 hours in the recovery room. Antibiotics were administered for prevention of discitis. She had no complaints of pain until the 1-month follow up visit. Percutaneous laser discetomy technique has the disadvantages of expensive equipment, high temperature and amount of vaporing disc tissue is empirical. However, this technique, as one of the therapeutic modalities for disc herniation, provides faster relief from acute attack than conservative management techniques in carefully selected patients with sciatica due to disc prolapse.

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초정밀 레이저용접을 이용한 티타늄 안경테 제조 (Manufacturing Ti-Alloy Frames of Classes with High-Precision Laser Beam Welding)

  • 황용화;김수성;이형권;민덕기;고진현
    • 한국산학기술학회논문지
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    • 제1권2호
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    • pp.1-8
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    • 2000
  • 본 연구에서는 상용 순수 티타늄 소재를 사용하여 안경테를 레이저 빔 용접으로 제조하기 위하여 광섬유로 전송되는 가변 펄스곡 80 ㎲-10 ms. 최대 평균출력 200 W, 첨두출력 12 kW와 최대 펄스에너지 50J성능의 초정밀 Nd:YAG 레이저 용접장치를 설계 제작하고 이 장치를 사용하여 안경테 제조를 위한 최적 용접조건을 선정하기 위한 실험을 수행하였다. 안경테를 위한 T이음 및 맞대기 이음형상을 용접할 때 평균출력, 광섬유 형태, 초점위치 등에서 용입상태와 용접결함을 조사하여 최적 용접조건을 선정하였고 안경테 부품 장석(temple hinge)과 다리, 톱바를 레이저 용접으로 시제품을 제작하였다.

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펄스레이저 증착법으로 제작된 ($Pb_{0.72}La_{0.28}$)$Ti_{0.93}O_{3}$박막의 레이저 파장 변화에 따른 특성 연구 (Effect Of Variation Of Laser Wavelength OH Properties of ($Pb_{0.72}La_{0.28}$)$Ti_{0.93}O_{3}$Thin Films Fabricated by Pulsed Laser Deposition)

  • 한경보;허창회;이상렬
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 하계학술대회 논문집
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    • pp.170-173
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    • 2001
  • Thin films of phase-pure perovskite (P $b_{0.72}$L $a_{0.28}$) $Ti_{0.93}$ $O_3$(PLT) were deposited in-situ onto Pt/Ti/ $SiO_2$/Si substrates by pulsed laser deposition. We have systematically investigated the variation of grain sizes depending on the process condition. Both in-situ annealing and ex-situ annealing treatments have been compared depending on the annealing time. Two-step process to grow (P $b_{0.72}$L $a_{0.28}$) $Ti_{0.93}$ $O_3$(PLT) films was adopted and verified to be useful to enlarge the grain size of the film and to enhance the leakage current characteristics. The grain sizes of PLT thin films were successfully controlled 260 to 350 nm by changing process parameters. Electrical properties including dielectric constant, ferroelectric characteristics, crystallization and leakage current of PLT thin films were shown to be strongly inf1uenced by grain size. Also PLT thin films on p-type(100) Si substrate will be fabricated by pulsed laser deposition technique using a Nd:YAG laser with different wavelengths of 355, 532 and 1064 nm. Effect of the variation of laser wavelength on dielectric properties will be discussed. Microstructural and electrical properties of the film were investigated by C-V measurement leakage current measurement and SEM.ent and SEM.

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2차 비선형 광학 초분지형 폴리에스테르의 합성 및 특성 (Synthesis and Properties of Hyperbranched Polyester with Second-Order Outical Nonlinearity)

  • 이종협;이광섭
    • 폴리머
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    • 제25권6호
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    • pp.803-810
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    • 2001
  • 새로운 개념의 초분지형 비선형 광학 고분자 (PE-Azo/Hyper)를 AB$_2$형의 기능기를 가지는 단량체 4-[N,N-bis(hydroxyethyl)amino-4'-formyl]azobenzene (CHO-DOH)으로부터 Knoevenagel 축중합 반응을 통하여 합성하였다. 겔크로마토그래피상에서 폴리스티렌을 기준시료로 측정된 중합체의 무게평균분자량은 M$_{w}$ =61,800 (M$_{W}$ /M$_{n}$=1.86)이었고 중합체의 용해도를 조사한 결과 1-methyl-2-pyrrolidinone, N,N-dimethylformamide 등의 반양자성극성 유기용매에 잘 녹았으며 따라서 이들 용매를 이용하여 양질의 박막성형이 가능하였다. 또한 열시차 분석법으로 중합체 PE-Azo/Hvper의 열적 성질을 조사한 결과 녹는점이 관찰되지 않아 무정형으로 판명되었으며 유리 전이 온도는 $121^{\circ}C$로 나타났다. 폴링에 의하여 극성 배향된 중합체 박막의 2차 비선형 계수를 Nd : YAG 레이저 (1064 nm)를 이용하여 Maker fringe 방법으로 측정한 결과 $d_{33}$= 25.4 pm/V로 비교적 높은 값을 나타내어 초분지형 고분자에서도 극성배향이 이루어져 비선형성이 발현됨을 관찰할 수 있었다.

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윤활영역에서 멀티크기 Laser Surface Texturing 효과 (Improvement of Tribological Characteristics of Multi-Scale Laser-Textured Surface in terms of Lubrication Regime)

  • 김종형;최시근;다윗제네베세구;정용섭;김석삼
    • Tribology and Lubricants
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    • 제30권1호
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    • pp.59-63
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    • 2014
  • Laser Surface Texturing(LST) is a surface engineering process used to improve tribological characteristics of materials by creating patterned microstructures on the mechanical contact surface. In LST technology, a pulsated laser beam is used to create arranged dimples on a surface by a material ablation process, which can improve such as load capacity, wear resistances, lubrication lifetime, and reduce friction coefficients. In the present study, the effect of multi-scale LST on lubricant regime was investigated. A pulsed Nd:YAG laser was applied on the bearing steel(AISI 52100) to create arranged dimples. To optimize the surface texturing effect on friction, multi-scale texture dimples with some specific formula arrays were fabricated by combining circles, ellipses and the laser ablation process. The tribological testing of multi-scale textured surface was performed by a flat-on-flat unidirectional tribometer under lubrication and the results compared with that of the non-textured surface. Through an increase in sliding speed, the beneficial effect of multi-scale LST performance was achieved. The multi-scale textured surface had lower friction coefficient performances than the non-textured surface due to the hydrodynamic lubrication effect.

염료 감응형 태양전지에서 Mesoproso $TiO_2$/FTO 사이에 완충층으로써의 PLD로 증착한 $TiO_2$ 박막에 관한 연구 (A Study on $TiO_2$ Thin Film by PLD for Buffer Layer between Mesoproso $TiO_2$ and FTO of Dye-sensitized Solar Cell)

  • 송상우;김성수;노지형;이경주;문병무;김현주
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.424-424
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    • 2008
  • Dye-sensitized Solar Cell (DSC) is a new type of solar cell by using photocatalytic properties of $TiO_2$. The electric potential distribution in DSCs has played a major role in the operation of such cells. Models based on a built-in electric field which sets the upper limit for the open circuit voltage(Voc) and/or the possibility of a Schottky barrier at the interface between the mesoporous wide band gap semiconductor and the transparent conducting substrate have been presented. $TiO_2$ thin films were deposited on the FTO substrate by Nd:YAG Pulsed Laser Deposition(PLD) at room temperature and post-deposition annealing at $500^{\circ}C$ in flowing $O_2$ atmosphere for 1 hour. The structural properties of $TiO_2$ thin films have investigated by X-ray diffraction(XRD) and atomic force microscope(AFM). Thickness of $TiO_2$ thin films were controlled deference deposition time and measurement by scanning electron microscope(SEM). Then we manufactured a DSC unit cells and I-V and efficiency were tested using solar simulator.

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4H-SiC 기판 위에 성장된 ZnO 박막의 온도에 따른 구조적 특성 분석 (Effect of Deposition Temperature on Structural Properties of ZnO Thin Films on 4H-SiC Substrate)

  • 김지홍;조대형;문병무;방욱;김상철;김남균;구상모
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.120-120
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    • 2008
  • We demonstrate epitaxial growth of ZnO thin films on 4H-SiC(0001) substrates using pulsed laser deposition (PLD). ZnO and SiC have attracted attention for their special material properties as wide band gap semiconductors. Especially, ZnO could be applied to optoelectronic applications such as light emitting devices and photo detectors due to its direct wide bandgap (Eg) of ~3.37eV and large exciton binding energy of ~60meV. SiC shows a good lattice matching to ZnO compared with other commonly used substrates and in this regard SiC is a good candidate as a substrate for ZnO. In this work, ZnO thin films were grown on 4H-SiC(0001) substrates by PLD using an Nd:YAG laser with a 355nm wavelength. The crystalline properties of the films were evaluated by x-ray diffraction (XRD) $\theta-2\theta$, rocking curve and pole figure measurements using a high-resolution diffractometer. The surface morphology of the films was studied by atomic force microscopy (AFM).

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펄스 레이저 증착법에 의한 BST 박막 가변 Capacitors 제작 (Fabrication of High Tunable BST Thin Film Capacitors using Pulsed Laser Deposition)

  • 김성수;송상우;노지형;김지홍;고중혁;문병무
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
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    • pp.79-79
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    • 2008
  • We report the growth of $Ba_{0.5}Sr_{0.5}TiO_3$(BST) thin films and their substrate-dependent electrical characteristics. BST thin films were deposited on alumina(non-single crystal), $Al_2O_3$(100) substrates by Nd:YAG Pulsed Laser Deposition(PLD) with a 355nm wavelength at substrate temperature of $700^{\circ}C$ and post-deposition annealing at $750^{\circ}C$ in flowing $O_2$ atmosphere for 1hours. BST materials had been chosen due to high dielectric permittivity and tunability for high frequency applications, To analyze the oxygen partial pressure effects, deposited films at 1, 10, 50, 100, 150, 200, 300 mTorr. The effects of oxygen pressure on structural properties of the deposited films have been investigated by X-ray diffraction(XRD) and atomic force microscope(AFM), respectively. Then we manufactured a inter-digital capacitor(IDC) patterns twenty fingers and $10{\mu}m$ gap, $700{\mu}m$ length and electrical properties were characterized. The results provide a basis for understanding the growth mechanisms and basic structural and electrical properties of BST thin films as required for tunable microwave devices applications such as varactors and tunable filters.

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