• Title/Summary/Keyword: NbS

Search Result 740, Processing Time 0.024 seconds

Biomimetic Deposition of Apatite on Zr-1Nb and Ti-6Al-4V

  • Kim, J.;Choi, Y.C.;Kim, H.S.;Hong, S.I.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09b
    • /
    • pp.1089-1090
    • /
    • 2006
  • Biomimetic apatite deposition behaviors on Zr-1Nb and Ti-6Al-4V plate with various surface conditions were examined. Both alloys were polished with abrasive papers to have different roughness and some of them were treated in NaOH before exposition in simulated body fluid. NaOH treatment was found to enhance the deposition rate of apatite on Ti-6Al-4V significantly. On the other hand, the deposition rate of Zr-1Nb was not influenced by NaOH treatment. Without NaOH treatment, the polished Zr-1Nb with abrasive paper was found to induce more apatite nucleation than the polished Zr-6Al-4V.

  • PDF

Effect of Hot Isostatic Pressing on the Microstructure and Properties of Kinetic Sprayed Nb Coating Material (Kinetic Spray 공정으로 제조된 Nb 코팅 소재의 미세조직 및 물성에 미치는 열간 등압 성형(HIP)의 영향)

  • Lee, Ji-Hye;Yang, Sangsun;Lee, Kee-Ahn
    • Journal of Powder Materials
    • /
    • v.23 no.1
    • /
    • pp.15-20
    • /
    • 2016
  • Niobium is one of the most important and rarest metals, and is used in the electronic and energy industries. However, it's extremely high melting point and oxygen affinity limits the manufacture of Nb coating materials. Here, a Nb coating material is manufactured using a kinetic spray process followed by hot isotactic pressing to improve its properties. OM (optical microscope), XRD (X-ray diffraction), SEM (scanning electron microscopy), and Vickers hardness and EPMA (electron probe micro analyzer) tests are employed to investigate the macroscopic properties of the manufactured Nb materials. The powder used to manufacture the material has angular-shaped particles with an average particle size of $23.8{\mu}m$. The porosity and hardness of the manufactured Nb material are 0.18% and 221 Hv, respectively. Additional HIP is applied to the manufactured Nb material for 4 h under an Ar atmosphere after which the porosity decreases to 0.08% and the hardness increases to 253 Hv. Phase analysis after the HIP shows the presence of only pure Nb. The study also discusses the possibility of using the manufactured Nb material as a sputtering target.

Influence of Nb Addition and Austenitizing Temperature on the Hardenability of Low-Carbon Boron Steels (저탄소 보론강의 경화능에 미치는 Nb 첨가와 오스테나이트화 온도의 영향)

  • Hwang, Byoungchul
    • Korean Journal of Materials Research
    • /
    • v.25 no.11
    • /
    • pp.577-582
    • /
    • 2015
  • The present study is concerned with the influence of niobium(Nb) addition and austenitizing temperature on the hardenability of low-carbon boron steels. The steel specimens were austenitized at different temperatures and cooled with different cooling rates using dilatometry; their microstructures and hardness were analyzed to estimate the hardenability. The addition of Nb hardly affected the transformation start and finish temperatures at lower austenitizing temperatures, whereas it significantly decreased the transformation finish temperature at higher austenitizing temperatures. This could be explained by the non-equilibrium segregation mechanism of boron atoms. When the Nb-added boron steel specimens were austenitized at higher temperatures, it is possible that Nb and carbon atoms present in the austenite phase retarded the diffusion of carbon towards the austenite grain boundaries during cooling due to the formation of NbC precipitate and Nb-C clusters, thus preventing the precipitation of $M_{23}(C,B)_6$ along the austenite grain boundaries and thereby improving the hardenability of the boron steels. As a result, because it considerably decreases the transformation finish temperature and prohibits the nucleation of proeutectoid ferrite even at the slow cooling rate of $3^{\circ}C/s$, irrespective of the austenitizing temperature, the addition of 0.05 wt.% Nb had nearly the same hardenability-enhancing effect as did the addition of 0.2 wt.% Mo.

Periodically domain inversion and optical properties of low-loss Ti : $LiNbO_3$ waveguides (저손실 Ti : $LiNbO_3$ 광도파로의 주기적 분극 반전과 광학특성)

  • Yang, W.S.;Kwon, S.W.;Lee, H.M.;Kim, W.K.;Yoon, D.H.;Lee, H.Y.
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.16 no.2
    • /
    • pp.49-52
    • /
    • 2006
  • Periodic electric field assisted poling low loss (${\sim}0.1dB/cm$) single-mode Ti-diffused waveguides in $LiNbO_3$ has been achieved using a periodically patterned electrode on the +Z surface of Ti : $LiNbO_3$ crystal and homogeneous LiCl solution. Using selective chemical etching, we confirmed the periodic (${\sim}16{\mu}m$) domain inverted structure and measured SH (second harmonic) properties of fabricated periodically poled Ti : $LiNbO_3$ waveguides.

Biochemical Characteristics of Lactobacillus acidophilus Isolated from a Breast-Fed Infant (모유 섭취 신생아 유래 Lactobacillus acidophilus의 생리적 특성)

  • Hong, Sung-Moon;So, Byung-Chun;Yoon, Seumg-Won;Kim, Cheol-Hyun
    • Journal of Dairy Science and Biotechnology
    • /
    • v.30 no.1
    • /
    • pp.45-53
    • /
    • 2012
  • Lactobacillus acidophilus isolated from the feces of a 7-day-old breast-fed infant was characterized to examine the scope of its commercial use. Forty-three Lactobacillus strains, which could grow at pH 5.5, were isolated. From these Lactobacillus isolates, 14 Lactobacillus strains were selected, which demonstrated more than 80% viability and homofermentative lactic fermentation. Finally, 9 L. acidophilus strains (NB 201~NB 209) were identified as candidate strains based upon biochemical properties, carbohydrate utilization, and cellular fatty acid composition. L. acidophilus isolates demonstrated a survival rate of more than 80% when exposed to pH 2.5 for 2 h. In particular, L. acidophilus NB 204 showed a strong acid tolerance, with a 71% survival rate even at pH 2.0. L. acidophilus isolates also manifested high bile acid tolerance; more than 87% of the cells survived on agar containing 1% bile extract, except for L. acidophilus NB 206, which showed a 73% survival rate. All L. acidophilus isolates were confirmed to have proteolytic activity; L. acidophilus NB 204 and NB 209 yielded higher levels of TCA-soluble peptides and free amino acids. The ${\beta}$-galactosidase activity of the L. acidophilus isolates was in the range of 1.97~2.45 units/mL.

  • PDF

Structural, FTIR and ac conductivity studies of NaMeO3 (Me ≡ Nb, Ta) ceramics

  • Roy, Sumit K.;Singh, S.N.;Kumar, K.;Prasad, K.
    • Advances in materials Research
    • /
    • v.2 no.3
    • /
    • pp.173-180
    • /
    • 2013
  • Lead-free complex perovskite ceramics $NaMeO_3$ ($Me{\equiv}Nb$, Ta) were synthesized using conventional solid state reaction technique and characterized by structural, FTIR and electrical (dielectric and ac conductivity) studies. The crystal symmetry, space group and unit cell dimensions were determined from the experimental results using FullProf software. XRD analysis of the compound indicated the formation of single-phase orthorhombic structure with the space group Pmmm (47). Dielectric studies showed the diffuse phase transition at $394^{\circ}C$ for $NaNbO_3$ and $430^{\circ}C$ for $NaTaO_3$. Ac conductivity in both the compounds follows Jonscher's power law.

Piezoelectric and dielectric properties of PMN-PZT ceramics with PNN substitution (PNN 치환에 따른 PMN-PZT 세라믹스의 유전 및 압전 특성)

  • Hwang, S.M.;Lee, J.S.;Yoon, K.H.;Yoo, J.H.;Jong, H.S.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2001.11b
    • /
    • pp.434-437
    • /
    • 2001
  • In this study piezoelectric and dielectric properties of $Pb(Mn_{1/3}Nb_{2/3})O_{3}-Pb(Zr,Ti)O_{3}$ ceramics were investigated with $Pb(Ni_{1/3}Nb_{2/3})O_{3}$ substitution. As the $Pb(Ni_{1/3}Nb_{2/3})O_{3}$ substitution was increased, dielectric constant and electromechanical coupling factor (kp) were increased while mechanical quality factor decreased.

  • PDF

Effect of additives on the PTCR Electrical Properties with $Nb_2O_5$ addition ($Nb_2O_5$ 첨가제가 PTCR의 전기적 특성에 미치는 영향)

  • Choi, K.C.;Lee, N.H.;Park, S.H.;Kim, Y.H.;Chu, S.N.;Lee, D.C.
    • Proceedings of the KIEE Conference
    • /
    • 1999.07d
    • /
    • pp.1885-1887
    • /
    • 1999
  • 본 연구에서는 $BaTiO_3$를 기본조성으로하는 반도성 세라믹스인 PTC 써미스터에 $Nb_2O_5$을 미량 첨가하여 미세구조 및 PTCR의 전기적 특성에 대해서 연구하였다. 또한 복소 임피던스 측정을 통하여 $Nb_2O_5$ 첨가에 따른 grain, grain boundary 저항변화에 대해서도 고찰하였다. $(Ba_{0.9}Sr_{0.05}Ca_{0.05})TiO_3-0.01SiO_2-0.001MnCO_3$를 기본조성으로 하여 $Nb_2O_5$ 첨가량을 $0.15{\sim}0.2mol%$까지 변화시켰으며 소결조건은 소결온도 $1350^{\circ}C$, 2h 유지하였으며 냉각속도는 $100^{\circ}C/h$로 하였다 첨가된 Nb의 양이 증가할수록 grain의 크기는 점차로 작아졌으며 상온저항과 peak 저항이 함께 증가하였다. 0.15mol% 첨가된 시편의 경우 상온저항은 $19[\Omega]$이었으며 peak 저항은 $5{\times}10^6[{\Omega}]$정도가 되었다.

  • PDF

Effect of Alloy Addition (Ta, Nb) on Oxidation Behavior of cp-Ti for Biomaterials (생체용 Ti합금의 산화거동에 미치는 Ta 및 Nb 첨가의 영향)

  • Lee Doh-Jae;Oh Tae-Wook;Park Bum-Su;Kim Soo-Hak;Jun Choong-Geug;Yoon Kye-Lim
    • Korean Journal of Materials Research
    • /
    • v.14 no.3
    • /
    • pp.211-217
    • /
    • 2004
  • The oxidation behaviors of Ti-10Ta-10Nb alloy and Ti-6Al-4V alloy were studied in dry air atmosphere. Specimens were melted in consumable vacuum arc furnace and homogenized at $1050^{\circ}C$ for 24 h. Hot rolling was performed at $1000^{\circ}C$. Specimens of the alloys were oxidized as the temperature range $400~650^{\circ}C$ for 30 min. The oxidation behavior of the alloys was analysed by optical microscope, SEM/EDX, XRD, XPS and TGA. Immersion test was performed in 1% Lactic acid. In the microscope observation, oxide layer of Ti-10Ta-10Nb alloy was denser and thinner than Ti-6Al-4V's. The weight gains during the oxidation rapidly increased at the temperature above $600^{\circ}C$ in Ti-6Al-4V's alloy and$ 700^{\circ}C$ in Ti-10Ta-10Nb alloy. According to XRD results, oxide layers were composed of mostly $TiO_2$(rutile) phase. It was analysed that the passive film of the Ti alloys consisted of $TiO_2$ through X-ray photoelectron spectroscopy(XPS) analysis.

Effects of Nb$_2$O$_{5}$ Addition on the Electromagnetic Properties of Mn-Zn Ferrites (Nb$_2$O$_{5}$ 첨가가 Mn-Zn Ferrites의 전자기적 특성에 미치는 효과)

  • Suh, Jung-Ju;Shin, Myung-Seung;Han, Young-Ho
    • Korean Journal of Materials Research
    • /
    • v.5 no.8
    • /
    • pp.1026-1034
    • /
    • 1995
  • It is well known that the addition of CaO-SiO$_2$to Mn-Zn ferrites forms an insulating grain bounary layer with high electrical resistivity. This study investigated the effect of Nb$_2$O$_{5}$ on the electromagnetic properties of high frequency low loss Mn-Zn ferrites. The addition of 300ppm Nb$_2$O$_{5}$ developed an exaggerated grain growth while the addition of CaO-SiO$_2$addition with 200ppm Nb$_2$O$_{5}$ more effectively increased the density than that without Nb$_2$O$_{5}$. The addition of Nb$_2$O$_{5}$ showed the lower power loss below 100 ppm SiO$_2$and the Nb$_2$O$_{5}$-CaO addition lowered the power loss at higher sintering temperature.

  • PDF