• Title/Summary/Keyword: NbC

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A study on the relationship of various characterizations for undoped ZnO thin films (Undoped ZnO 박막의 다양한 특성의 상관관계에 대한 연구)

  • Baek, Kyung-Hyun;Park, Hyeong-Sik;Jang, Kyung-Soo;Jung, Sung-Wook;Ryu, Kyung-Yul;Yun, Eui-Jung;Yi, J.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.147-147
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    • 2010
  • PTC Thermistors specimens were fabricated by added $MnO_2$ as donors, and $Nb_2O_5$ as acceptors and sintered $1250^{\circ}C$/2hrs. Average grain size decreased with increased in added $MnO_2$, and increased with added in $Nb_2O_5$. But, appeared liquid phase as $Bi_2O_3$ and $TiO_2$, affect to grain growth. XRD result, peak strength waslowed then crystallization not well, but, secondary phase were not showed all specimens. All specimens resistance were so high, about $40M{\Omega}$ over, couldn't measured to those resistance and doesn't appear PTCR effect.

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Dielectric and piezoelectric properties of lead-free $(Na_{0.5}K_{0.5})NbO_3$-Ba(Ti, Sn)$O_3$ ceramics

  • Cha, Yoo-Jeong;Kim, Chang-Il;Jeong, Young-Hun;Lee, Young-Jin;Paik, Jong-Hoo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.30-30
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    • 2008
  • Lead-free piezoelectric ceramics 0.97$(Na_{0.5}K_{0.5})NbO_3$-0.03Ba$(Ti_{1-x}Sn_x)O_3$ [NKN-BTS-x] ceramics doped with 1 mol% $MnO_2$ have been fabricated by a sintering technique with muffling. The $MnO_2$-doped NKN-BTS-x ceramics with x$\leq$0.2 have pure orthorhombic perovskite structure at room temperature. The dense microstructure was developed with grain growth as an increase of amount of Sn. Moreover, the addition of Sn was found to have a significant influence on piezoelectric properties. In particular, the $MnO_2$-doped NKN-BTS-0.1 ceramics showed improved piezoelectric properties of piezoelectric constant ($d_{33}$=145pC/N), relatively large electromechanical coupling factor ($k_p$=43%), dielectic constant (${\varepsilon}^T_{33}/{\varepsilon}_0$=676) dielectric loss (tan$\delta$=1.3%).

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Magnesium diboride(MgB2) wires for applications

  • Patel, Dipak;Kim, Jung Ho
    • Progress in Superconductivity and Cryogenics
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    • v.18 no.1
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    • pp.1-5
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    • 2016
  • Field and temperature dependence of the critical current density, Jc, were measured for both un-doped and carbon doped $MgB_2/Nb/Monel$ wires manufactured by Hyper Tech Research, Inc. In particular, carbon incorporation into the $MgB_2$ structure using malic acid additive and a chemical solution method can be advantageous because of the highly uniform mixing between the carbon and boron powders. At 4.2 K and 10 T, Jc was estimated to be $25,000-25,300Acm^{-2}$ for the wire sintered at $600^{\circ}C$ for 4 hours. The irreversibility field, $B_{irr}$, of the malic acid doped wire was approximately 21.0 - 21.8 T, as obtained from a linear extrapolation of the J-B characteristic. Interestingly enough, the Jc of the malic acid doped sample exceeds $10^5Acm^{-2}$ at 6 T and 4.2 K, which is comparable to that of commercial Nb-Ti wires.

Processing and Properties of RAINBOW Piezoelectric Actuator (RAINBOW 압전 액츄에이터의 제조와 물성)

  • Paik Jong-Hoo;Lim Eun-Kyeong;Kim Chang-il;Lee Mi-Jae;Jee Mi-Jung;Choi Byung-Hyun;Kim Sei-Ki
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.19 no.3
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    • pp.222-227
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    • 2006
  • RAINBOW(Reduced And Internally Biased Oxide Wafers) are a new class of high-displacement, piezoelectric actuator produced by selectively removing oxygen from one surface of ceramic using a high-temperature chemical reduction process. In this paper, RAINBOW actuator materials of $0.4Pb(Ni_{1/3}Nb_{2/3})O_3-0.6Pb(Zr_{x}Ti_{1-x})O_3$ ceramics were prepared. Its dielectric and piezoelectric properties were investigated in the vicinity of MPB. The piezoelectric properties showed the maximum value of ${\epsilon}r$ = 4871, $d_{33}$ = 610 ($10^{-12}$ m/V), $d_{31}$ = -299 ($10^{-12}$ m/V), $k_{33}$ = $71\%$, Qm = 70, in $0.4Pb(Ni_{1/3}Nb_{2/3})O_{3}-0.6Pb(Zr_{405}Ti_{595})O_3$ composition sintered at $1250^{\circ}C$. The strain - electric field characteristics of RAINBOW actuator were significantly improved comparison with the conventional bulk actuator. The prepared RAINBOW actuator showed about $390\;{\mu}m/100\;V$ displacement.

The study on preparation of $Sr_xBa_{1-x}$ $Nb_2O_6$ piezoelectric Thin Film of tungsten-bronze type by Metal Organic Decomposition Process and their properties (MOD 공법을 이용한 텅스텐 브론즈구조의 $Sr_x Ba_{1-x}$ $Nb_2O_6$ 압전 박막의 제조 및 특성 연구)

  • Kim, Kwang-Sik;Kim, Kyoung-Won;Jang, Gun-Ik;Ur, Soon-Chul
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.248-249
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    • 2005
  • The tungsten bronze type of strontium barium niobate(SBN) thin film was synthesized by metal organic decomposion method for SBN stock solution and the SBN thin film process were deposited by spin-coating process on Pt-deposited si-wafer(100) by magnetron sputtering system. The thickness of SBN thin film was 150$\sim$200 nm and were optimized for rpm of spin-coater system. The structural variation of SBN thin film was studied by TG-DTA and XRD. The deposited SBN stock solution on annealing at $400\sim800^{\circ}C$ a pure tungsten bronze SBN phase and the corresponding average grain size about 500$\sim$1000 nm influenced by annealing temperature.

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Effects of α2/β Volume Fraction on the Superplastic Deformation (2 상 Ti3Al-xNb 계 금속간 화합물들의 초소성 특성에 미치는 상분율의 영향)

  • 김지식
    • Transactions of Materials Processing
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    • v.11 no.5
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    • pp.447-456
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    • 2002
  • A study has been made to investigate the boundary sliding and its accommodation mode with respect to the variation of $\alpha$$_2$/$eta$ volume fraction during superplastic deformation of two-phase Ti$_3$Al-xNb intermetallics. Step strain rate and load relaxation tests have been performed at 950, 970 and 99$0^{\circ}C$ to obtain the flow stress curves and to analyze the deformation characteristics by the theory of inelastic deformation. The results show that the grain matrix deformation and boundary sliding of the three intermetallics containing 21, 50 and 77% in $eta$ volume fractions are well described by the plastic deformation and viscous flow equations. Due to the equal accommodation of both $a^2$ and $\beta$ phases, the accommodation modes for fine-grained materials are in good agreement with the iso-strain rate models. The sliding resistance analyzed for the different boundaries is the lowest in the $\alpha$$_2$/$\alpha$$_2$ boundary, and increases in the order of $\alpha$$_2$/$\alpha$$_2$<< $\alpha$$_2$/$\beta$ = $\beta$/$\beta$, which plays an important role in controlling the superplasticity of the alloys with the various $\alpha$$_2$/$\beta$ phase ratio.

Dielectric and Piezoelectric Properties of Pb(Zn,Ni,Nb)O3-Pb(Zr,Ti)O3 Ceramics for AE Sensor (음향 방출 센서용 Pb(Zn,Ni,Nb)O3-Pb(Zr,Ti)O3 세라믹스의 유전 및 압전 특성)

  • Han, Jong-Dae;Yoo, Ju-Hyun;Jeong, Hoy-Seung;Seo, Dong-Hir
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.8
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    • pp.466-469
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    • 2016
  • In this study, in order to develop composition ceramics for Acoustic Emission (abbreviated as AE) sensor application, the PZT system ceramics was fabricated by conventional solid state reaction method. When x=0.48, the density, electromechanical coupling factor($k_p$), piezoelectric coefficient $d_{33}$ and piezoelectric voltage constant $g_{33}$ of the maximum values of $7.857g/cm^3$, 0.51, 190[pC/N], 52[$10^{-3}mV/N$] were obtained, respectively, suitable for AE sensor.

Coercivity of Hot-pressed Compacts of Nd-Fe-B-type HDDR-treated Powder

  • Abdul Matin, Md.;Kwon, Hae-Woong;Lee, Jung-Goo;Yu, Ji-Hun
    • Journal of Magnetics
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    • v.19 no.2
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    • pp.106-110
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    • 2014
  • $Nd_{12.5}Fe_{80.6}B_{6.4}Ga_{0.3}Nb_{0.2}$ HDDR-treated powder was compacted by hot-pressing using different configurations of dies and heating rates. The die configurations were especially different in terms of the evacuation system that was used in heating for hot-pressing. The coercivity in the compacts was influenced by the evacuation system of the die and heating rate. In spite of the identical hot-pressing temperature and heating rate, coercivity was radically reduced above $600^{\circ}C$ in the compacts prepared in the closed-type die compared to that in the compacts prepared in the open-type die. The coercivity in the compacts prepared in the closed-type die decreased with increasing heating rate and the value further increased when extreme high heating rate was employed. $Nd_{12.5}Fe_{80.6}B_{6.4}Ga_{0.3}Nb_{0.2}$ HDDR-treated powder contained a significant amount of residual hydrogen (approx. 1500 ppm) in the form of $Nd_2Fe_{14}BH_x$ hydride. The dramatic coercivity decrease in the compact prepared in the closed die is attributed to the disproportionation of $Nd_2Fe_{14}BH_x$ hydride. High coercivity is mainly due to the effective desorption of hydrogen or the suppression of hydrogen-related disproportionation upon hot-pressing.

Effects of Ceramics on Dielectric Properties of Polystyrene / Ceramics Composites at Microwave Frequencies

  • Jeon, Chang-Jun;Kim, Eung-Soo
    • Journal of the Korean Ceramic Society
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    • v.48 no.3
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    • pp.257-262
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    • 2011
  • Dependencies of dielectric properties on $MgTa_2O_6$, $MgNb_2O_6$, and $MgWO_4$ (Mg-based ceramics) fillers of the polystyrene (PS) matrix composites were investigated as a function of frequency. With increasing frequency from 1 GHz to 7.3 GHz, the dielectric constant (K) of the composites was not changed significantly, while the dielectric loss (tan${\delta}$) of the composites was slightly decreased. The K, tan${\delta}$, and temperature coefficient of resonant frequency (TCF) of the composites were dependent on the type and amount of ceramics at 11 GHz. Also, several theoretical models have been employed to predict the effective dielectric constant of the composites and the results were compared with experimental data. Typically, a K value of 6.67, tan${\delta}$ of $0.56{\times}10^{-3}$, and TCF of -4.99 $ppm/^{\circ}C$ were obtained for the PS composites with 0.4 volume fraction of $MgNb_2O_6$ at 11 GHz.

Piezoelectric Properties of Y-Substituted Pb(Ni1/3Nb2/3)-PbZrO3-PbTiO3 Ceramics and Their Application to Multilayer Piezoelectric Actuators (Y 치환에 따른 Pb(Ni1/3Nb2/3)-PbZrO3-PbTiO3 세라믹의 압전특성 및 적층형 압전 액츄에이터 응용)

  • 권정호;최문석;이대수;정연학;김일원;송재성;정순종;이재신
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.2
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    • pp.184-189
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    • 2004
  • The effects of $Y_2$ $O_3$-substitution on the piezoelectric properties of Pb[(N $i_{1}$3/N $b_{2}$3/)$_{0.15}$(Z $r_{1}$2/ $Ti_{1}$2/)$_{0.85}$] $O_3$ceramics were investigated. It was found that $Y^{3+}$ ions incorporate into Pb-sites of the ceramics, resulting in a increased lattice anisotropy and formation of Pb-vacancies. As a result, an orthorhombic-tetragonal phase transition was induced when $\chi$>0.005. At the morphotropic phase boundary of x=0.005, piezoelectric constants( $k_{p}$, $k_{33}$, and $d_{33}$) showed maximum values of 0.53, 0.58, and 350pC/N, respectively. A 30-layer actuator fabricated with the above material showed a maximum strain of 0.12% under 100V DC bias.