• Title/Summary/Keyword: Nanoparticle deposition

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Experimental study on the role of nanoparticle deposition in pool boiling CHF enhancement using nanofluids (나노유체 이용한 풀비등 임계열유속 증가에서 나노입자 유착물의 영향에 관한 실험적 연구)

  • Kim, Hyung-Dae;Kim, Seon-Tae;Ahn, Ho-Seon;Kim, Moo-Hwan
    • Proceedings of the KSME Conference
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    • 2007.05b
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    • pp.1906-1911
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    • 2007
  • It has been well known that pool boiling CHF in nanofluids compared to pure water significantly increase due to the deposition of nanoparticles on heater surface. This study concerns the characteristics of the nanoparticle deposition layer and its influence on CHF. Pool boiling experiments were carried out with 0.01vol.% water-$TiO_2$ nanofluids to obtain various nanoparticle-deposited heaters. CHF on the prepared heaters was measured during pool boiling in pure water. The heater surfaces were visualized using scanning electron microscope (SEM) and also characterized using contact angle and capillarity. The results showed that the CHF enhancement in nanofluids was completely dependent upon the structural and physicochemical characteristics of the nanoparticle deposition layer.

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A Study on the Deposition of Permalloy Nanostructured Thin Film Utilizing Supersonic Deposition of Nanoparticles Formed by Laser Ablation of Microparticles (마이크로입자의 레이저 Ablation으로 형성된 나노입자의 수펴소닉 적층법을 이용한 퍼멀로이 나노구조박막 적층에 관한 연구)

  • Yun, Eui-Jung;Jung, Myunghee
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.5
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    • pp.478-483
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    • 2005
  • In this paper, we synthesized 10 to 20 nm diameter NiFe nanoparticles and nanoparticle films utilizing supersonic jet deposition of nanoparticle aerosols generated by laser ablation of $30\;to\;45{\mu}m$ diameter permalloy $(Ni_{81}Fe_{19} \;at\;{\%})$ microparticles. The component and composition of the nanoparticles were characterized by an energy dispersive X-ray spectroscopy. The morphology of the nanoparticles and nanoparticle films was analyzed by a high-resolution transmission electron microscopy and a scanning electron microscopy, respectively. The experimental results showed that the nanoparticles and nanoparticle films have remarkable properties with an excellent preservation of the composition of feedstock permalloy microparticles. The purpose of the present work is to present details on the composition and nanostructural characterizations for NiFe nanoparticles and nanoparticle films prepared by laser ablation of microparticles (LAM).

Experimental Investigations on Pool Boiling CHE of Nano-Fluids (나노유체의 풀비등 임계열유속에 대한 실험적 연구)

  • Kim, Hyung-Dae;Kim, Moo-Hwan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.11
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    • pp.949-956
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    • 2007
  • Pool boiling critical heat flux (CHF) of nanofluids with oxide nanoparticles of $TiO_2$ or $Al_2O_3$ was experimentally investigated under atmospheric pressure. The results showed that a dispersion of oxide nanoparticles significantly enhances the CHF over that of pure water. Moreover it was found that nanoparticles were seriously deposited on the heater surface during pool boiling of nanofluids. CHF of pure water on a nanoparticle-deposited surface, which is produced during the boiling of nanofluids, was not less than that of nanofluids. The result reveals that the CHF enhancement of nanofluids is absolutely attributed to modification of the heater surface by the nanoparticle deposition. Then, the nanoparticle-deposited surface was characterized with parameters closely related to pool boiling CHF, such as surface roughness, contact angle, and capillary wicking. Finally, reason of the CHF enhancement of nanofluids is discussed based on the changes of the parameters.

A Study on the Silver Nanoparticle Deposition for Optical Amplification (광 증폭용 플라즈모닉 나노구조 제작을 위한 은 나노입자 증착 연구)

  • Kang, J.S.;Kim, J.H.;Jeong, M.Y.
    • Journal of the Microelectronics and Packaging Society
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    • v.25 no.1
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    • pp.11-15
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    • 2018
  • In this study, we deposited silver nanoparticles on the nanocone array structure which was fabricated by the UV nanoimprint process for optical signal amplification. The deposition of the silver nanoparticles was based on the evaporation behavior of the solution droplet according to wettability of surface and the deposition pattern changed from the center of the droplet to the edge depending on the difference of thermal energy. The optical property of silver nanoparticles that were deposited on imprinted nanohole patterns was simulated by the Finite difference time domain (FDTD) analysis method, and it was confirmed that energy was concentrated around the silver nanoparticle of the finally fabricated structure.

Palladium Layers on an Au(111) Nanoparticle and Their Catalytic Activity to Formic Acid Oxidation

  • Kim, Byeong-Gwon;Seo, Dae-Ha;Song, Hyeon-Jun;Gwak, Ju-Hyeon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.206-206
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    • 2011
  • Nanoparticles have been received great attention from many researchers for several decades because of their good and unique properties. In particular, researches in the field of synthesis of bimetallic nanoparticles showed good results for the past ten years. In this research, Pd thinlayer on Au nanoparticles were synthesized by electrochemical deposition method. Well-defined Au(111) nanoparticles were synthesized by solution based reduction method. Electrochemical deposition conditions for Pd thinlayer on Au(111) nanoparticles surface were carefully regulated by controlling parameters of cyclic voltammetry. To calculate exact mass and surface area catalytic activities of deposited Pd thinlayer on Au(111) nanoparticle, electrochemically active surface area (ECSA) and mass of the deposited Pd thinlayer were measured by cyclic voltammetry in 0.1 M HClO4 solution. Afterward, catalytic activities of the deposited Pd thinlayer were measured in 0.1 M HClO4 + 0.2 M formic acid solution. In case of less negative deposition potential, the amounts of deposited Pd mass and surface area were small. However, mass and ECSA activity of the deposited Pd to oxidize formic acid were increased.

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Experimental Investigation on the Pool Boiling Critical Heat Flux of Water-Based Alumina and Titania Nanofluids on a Flat Plate Heater (평판형 히터를 이용한 알루미늄과 타이타늄 산화물 나노유체의 풀비등 임계열유속에 관한 실험적 연구)

  • Ahn, Ho-Seon;Kim, Hyung-Dae;Jo, Hang-Jin;Kang, Soon-Ho;Kim, Moo-Hwan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.33 no.10
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    • pp.729-736
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    • 2009
  • Pool boiling heat transfer and critical heat flux (CHF) of water-based nanofluids with alumina and titania nanoparticles of 0.01% by volume were investigated on a disk heater at saturated and atmospheric conditions. The experimental results showed that the boiling in nanofluids caused the considerable increase in CHF on the flat surface heater. It was revealed by visualization of the heater surface subsequent to the boiling experiments that a major amount of nanoparticles deposited on the surface during the boiling process. Pool boiling of pure water on the surface modified by such nanoparticle deposition resulted in the same CHF increases as what boiling nanofluids, thus suggesting the CHF enhancement in nanofluids was an effect of the surface modification through the nanoparticle deposition during nanofluid boiling. Possible reasons for CHF enhancement in pool boiling of nanofluids are discussed with surface property changes caused by the nanoparticle deposition.

Synthesis and characterization of GaN nanoparticles by pulsed laser deposition (펄스레이저증착법에 의한 GaN 나노입자의 합성 및 특성분석)

  • ;;;Koshizaki Naoto
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.13 no.2
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    • pp.79-82
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    • 2003
  • GaN nanoparticles were synthesized by the pulsed laser deposition (PLD) process on $SiO_2$substrate after irradiating the surface of the GaN sintered pellet by the ArF (193 nm) excimer laser. At this moment Ar gas pressure of 100 Pa, 50 Pa, 10 Pa and 1 Pa were applied during the ablation process and laser power of 100 mJ and 200 mJ were also applied. The synthesized fan nanoparticles were characterized by XRD, SEM, TEM, XPS and optical absorption spectra. The synthesized GaN nanoparticles had the crystallite sizes of 20~30 nm, and besides, GaN nanoparticles synthesized under low Ar gas pressure compared to the others corresponded with stoichiometry, and the optical band edge of the GaN nanoparticles was blueshifted.

Support Effect of Arc Plasma Deposited Pt Nanoparticles/TiO2 Substrate on Catalytic Activity of CO Oxidation

  • Qadir, Kamran;Kim, Sang Hoon;Kim, Sun Mi;Ha, Heonphil;Park, Jeong Young
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.261-261
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    • 2013
  • The smart design of nanocatalysts can improve the catalytic activity of transition metals on reducible oxide supports, such as titania, via strong metal-support interactions. In this work, we investigatedtwo-dimensional Pt nanoparticle/titania catalytic systems under the CO oxidation reaction. Arc plasma deposition (APD) and metal impregnation techniques were employed to achieve Pt nanoparticle deposition on titania supports, which were prepared by multitarget sputtering and sol-gel techniques. APD Pt nanoparticles with an average size of 2.7 nm were deposited on sputtered and sol-gel-prepared titania films to assess the role of the titania support on the catalytic activity of Pt under CO oxidation. In order to study the nature of the dispersed metallic phase and its effect on the activity of the catalytic CO oxidation reaction, Pt nanoparticles were deposited in varying surface coverages on sputtered titania films using arc plasma deposition. Our results show an enhanced activity of Pt nanoparticles when the nanoparticle/titania interfaces are exposed. APD Pt shows superior catalytic activity under CO oxidation, as compared to impregnated Pt nanoparticles, due to the catalytically active nature of the mild surface oxidation and the active Pt metal, suggesting that APD can be used for large-scale synthesis of active metal nanocatalysts.

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