• Title/Summary/Keyword: Nano-crystals

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The Quality Investigation of 6H-SiC Crystals Grown by a Conventional PVT Method with Various SiC Powders

  • Yeo, Im-Gyu;Lee, Tae-Woo;Lee, Won-Jae;Shin, Byoung-Chul;Choi, Jung-Woo;Ku, Kap-Ryeol;Kim, Young-Hee
    • Transactions on Electrical and Electronic Materials
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    • v.11 no.2
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    • pp.61-64
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    • 2010
  • In this paper, we investigate the quality difference of SiC crystals grown by a conventional physical vapor transport method using various SiC powders. While the growth rate was revealed to be dependent upon the particle size of the SiC powder, the growth rate of SiC bulk crystals grown using SiC powder with a smaller particle size (20 nm) was definitely higher than those using lager particle sizes with $0.1-0.2\;{\mu}m$ and $1-10\;{\mu}m$, respectively. All grown 2 inch SiC single crystals were proven to be the polytype of 6H-SiC and the carrier concentration levels of about $10^{17}\;cm^3$ were determined from Hall measurements. It was revealed that the particle size and process method of SiC powder played an important role in obtaining a good quality, high growth rate, and to reduce growth temperature.

Observation of Nano-scale Domain Boundary in $LiTaO_3$ Single Crystals ($LiTaO_3$ 단결정의 도메인 바운더리 관찰)

  • Jeong, Dae-Yong;Kim, Jin-Sang;Park, Young-Wook;Yoon, Seok-Jin;Cho, Yasuo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.06a
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    • pp.327-327
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    • 2007
  • $LiTaO_3$ single crystal has been studied for surface acoustic wave(SAW) applications. There are two kinds of $LiTaO_3$ single crystals, stoichiometric $LiTaO_3$ (SLT) and congruent $LiTaO_3$ (CLT). These two crystals show quite different dielectrical properties, which might be related with defects in crystals. In this study, we observed the domain boundary of SLT and CLT with scanning nonlinear dielectric microscopy and discussed the stress distribution in $LiTaO_3$ single crystals.

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Plasma discharge characteristics of MgO protection layer deposited by using targets made of single crystals, and nano powders

  • Yang, Choong-Jin;Park, Eun-Byeong;Lee, Ho-Sang;Park, Jung-Hoo
    • 한국정보디스플레이학회:학술대회논문집
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    • 2008.10a
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    • pp.157-160
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    • 2008
  • Improved properties of second electron emission was evaluated by assemble of 4 inch PDP panel. MgO protection layers were deposited and examined by using both pellets made of extremely pure MgO single crystals and sintered pellets using MgO nano powders. $\gamma$ coefficients higher than 0.11 were obtained from the panel by adopting dopant-controlled MgO single crystals. Especially the MgO layer deposited by sintered pellets made of nano powders showed the higher $\gamma$ coefficients at the operating voltage above 200 volts.

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Surface Discharge Characteristics of New Flat Fluorescent Lamp Enhanced by MgO Nano-Crystals

  • Lee, Yang-Kyu;Heo, Seung-Taek;Lee, You-Kook;Lee, Dong-Gu
    • 한국정보디스플레이학회:학술대회논문집
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    • 2009.10a
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    • pp.687-690
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    • 2009
  • It has been recently reported that nano-sized MgO single crystal powders emit ultraviolet by stimulation of electrons under vacuum condition. Therefore, in this study, nano-crystalline MgO powders were applied to a xenon plasma flat fluorescent lamp for LCD backlight to improve emission efficiency of the lamp by help of extra ultraviolet from nano-MgO. For comparison with nano-crystalline MgO powders, MgO nano-thin film was applied directly on phosphors inside a lamp panel through e-beam evaporation The luminance and efficiency of FFL with an addition of MgO nano-crystal powders on phosphors were improved by around 20%. Application of MgO thin film to phosphors worsened the emission characteristics of FFLs, even rather than FFL without MgO. The reason came from insufficient stimulation of phosphors by UV, crystallinity of MgO, and low secondary electron coefficient.

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Single Crystal Growth Behavior in High-Density Nano-Sized Aerosol Deposited Films

  • Lim, Ji-Ho;Kim, Seung-Wook;Kim, Samjung;Kang, Eun-Young;Lee, Min Lyul;Samal, Sneha;Jeong, Dae-Yong
    • Korean Journal of Materials Research
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    • v.31 no.9
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    • pp.488-495
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    • 2021
  • Solid state grain growth (SSCG) is a method of growing large single crystals from seed single crystals by abnormal grain growth in a small-grained matrix. During grain growth, pores are often trapped in the matrix and remain in single crystals. Aerosol deposition (AD) is a method of manufacturing films with almost full density from nano grains by causing high energy collision between substrates and ceramic powders. AD and SSCG are used to grow single crystals with few pores. BaTiO3 films are coated on (100) SrTiO3 seeds by AD. To generate grain growth, BaTiO3 films are heated to 1,300 ℃ and held for 10 h, and entire films are grown as single crystals. The condition of grain growth driving force is ∆Gmax < ∆Gc ≤ ∆Gseed. On the other hand, the condition of grain growth driving force in BaTiO3 AD films heat-treated at 1,100 and 1,200 ℃ is ∆Gc < ∆Gmax, and single crystals are not grown.

Effect of Nano-sized Calcium-silicate-hydrate (C-S-H) Crystals on Cement Hydration (나노 크기 칼슘-실리케이트-하이드레이트(C-S-H) 결정이 시멘트 수화에 미치는 영향 분석)

  • Gyeong-Tae Kim;Su-Ji Woo;Sung-Won Yoo;Young-Cheol Choi
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.11 no.2
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    • pp.153-160
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    • 2023
  • In this study, nano-sized C-S-H crystals were synthesized using the liquid phase reaction method and their properties were investigated. The synthesized C-S-H crystals were added to the cement composite in suspension form to determine their effect on the hydration properties of the cement. The amount of chemical admixture was varied to obtain nano-sized C-S-H crystals with optimal agglomerated morphology, and SEM photographs were analyzed. A cleaning process was added to remove harmful substances other than the synthesiz ed C-S-H crystals. It was found that the concentration of harmful substances was reduced in the case of C-S-H crystals subjected to the cleaning process. The synthesized C-S-H suspensions were prepared with and without the cleaning process, and cement composites were prepared with the cement weight content as the main variable. The effect of C-S-H crystals on the initial hydration properties of the cement was confirmed by microhydration heat analysis. In addition, mortar specimens were prepared to measure the compressive strength over time. The test results showed that the nano-sized C-S-H crystals act as nucleation sites in the cement paste to promote the early hydration of the cement and increase the early compressive strength.

Nano stamp fabrication for photonic crystal waveguides (나노 광소자용 나노스탬프 제조공정 연구)

  • Jeong, Myung-Yung;Jung, Une-Teak;Kim, Chang-Seok
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.12 s.177
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    • pp.16-21
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    • 2005
  • Photonic crystals, periodic structure with a high refractive index contrast modulation, have recently become very interesting platform for the manipulation of light. The existence of a photonic bandgap, a frequency range in which the propagation of light is prevented in all directions, makes photonic crystal very useful in application where the spatial localization of light is required, for example waveguide, beam splitter, and cavity. However, the fabrication of 3 dimensional photonic crystals is still difficult process. A concept that has recently attracted a lot of attention is a planar photonic crystal based on a dielectric membrane, suspended in the air and perforated with two dimensional lattice of hole. The fabrication of Si master with pillar structure using hot embossing process is investigated for two dimensional, low-index-contrast photonic crystal waveguide. From our research we show that the multiple stamp copy process proved to be feasible and useful.

Aluminum Oxide Photonic Crystals Fabricated on Compound Semiconductor (화합물 반도체 기판 위에 제작된 산화 알루미늄 광결정 특성)

  • Choi, Jae-Ho;Kim, Keun-Joo;Jung, Mi;Woo, Duk-Ha
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.77-78
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    • 2006
  • We fabricated photonic crystals on GaAs and GaN substrates. After anodizing the aluminium thin film in electrochemical embient, the porous alumina was implemented to the mask for reactive ion beam etching process of GaAs wafer. And photonic crystals in GaN wafer were also fabricated using electron beam nano-lithography process. The coated PMMA thin film with 200 nm-thickness on GaN surface was patterned with triangular lattice and etched out the GaN surface by the inductively coupled plasma source. The fabricated GaAs and GaN photonic crystals provide the enhanced intensities of light emission for the wavelengths of 858 and 450 nm, respectively. We will present the detailed dimensions of photonic crystals from SEM and AFM measurements.

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