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http://dx.doi.org/10.3740/MRSK.2021.31.9.488

Single Crystal Growth Behavior in High-Density Nano-Sized Aerosol Deposited Films  

Lim, Ji-Ho (Dept. of Materials Science and Engineering, Inha University)
Kim, Seung-Wook (Dept. of Materials Science and Engineering, Inha University)
Kim, Samjung (Dept. of Materials Science and Engineering, Inha University)
Kang, Eun-Young (Dept. of Materials Science and Engineering, Inha University)
Lee, Min Lyul (Program in Metal.Materials Process Engineering, Inha University)
Samal, Sneha (Institute of Physics of the Czech Academy of Sciences)
Jeong, Dae-Yong (Dept. of Materials Science and Engineering, Inha University)
Publication Information
Korean Journal of Materials Research / v.31, no.9, 2021 , pp. 488-495 More about this Journal
Abstract
Solid state grain growth (SSCG) is a method of growing large single crystals from seed single crystals by abnormal grain growth in a small-grained matrix. During grain growth, pores are often trapped in the matrix and remain in single crystals. Aerosol deposition (AD) is a method of manufacturing films with almost full density from nano grains by causing high energy collision between substrates and ceramic powders. AD and SSCG are used to grow single crystals with few pores. BaTiO3 films are coated on (100) SrTiO3 seeds by AD. To generate grain growth, BaTiO3 films are heated to 1,300 ℃ and held for 10 h, and entire films are grown as single crystals. The condition of grain growth driving force is ∆Gmax < ∆Gc ≤ ∆Gseed. On the other hand, the condition of grain growth driving force in BaTiO3 AD films heat-treated at 1,100 and 1,200 ℃ is ∆Gc < ∆Gmax, and single crystals are not grown.
Keywords
aerosol deposition; single crystal growth; solid state grain growth;
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