• 제목/요약/키워드: NIST

검색결과 650건 처리시간 0.022초

큰 개구부가 있는 공간의 화재와 제연의 대와류모사 (Large Eddy Simulation of Fire and Smoke Control in a Compartment with Large Openings)

  • 박외철
    • 한국화재소방학회논문지
    • /
    • 제17권3호
    • /
    • pp.7-12
    • /
    • 2003
  • 지하철 역과 같이 대형 개구부가 있는 공간의 화재와 제연을 조사하기 위해, 지하철 역과 유사한 구조의 4 m ${\times}$ 1 m ${\times}$ 1.5m 크기의 공간 내 50 kW의 폴리우레탄 화재에 대한 수치모사를 수행하였다. 대와류모사를 난류모델로 사용하고, 혼합분율 연소모델과 복사 유한체적법을 사용하였다. 화재 발생 후 5초부터 급배기방식과 급기방식, 배기방식의 세가지 기계 제연방식이 각각 작동했을 때 제연방식에 따른 승강장과 출입통로의 공기온도와 연기이동을 비교하였다. 제연방식 가운데 급배기방식의 제연성능이 가장 좋고 안전한 것으로 나타났다. 그러나 지하철 역에 사용되고 있는 급기방식은 급기구를 통해 공급된 공기가 고온의 연기와 혼합됨으로써 제연성능이 오히려 자연제연방식보다 불량하므로 지하철 역과 같은 구조에서는 적합하지 않음을 확인하였다.

Inhibitory Effects of Seaweed Extracts on Growth of Malassezia furfur and Malassezia restricta

  • Choi, Jae-Suk;Lee, Bo-Bae;Joo, Chi-Un;Shin, Su-Hwa;Ha, Yu-Mi;Bae, Hee-Jung;Choi, In-Soon
    • Fisheries and Aquatic Sciences
    • /
    • 제12권1호
    • /
    • pp.29-34
    • /
    • 2009
  • Fifty seven species of common seaweed from the coast of Korea were screened for antifungal activity against Malassezia species. Seaweeds as a source of bioactive compounds are able to produce a great variety of secondary metabolites with different activities. There are numerous reports on the biological activities of seaweeds against human pathogens, fungi, and yeasts, but only few contain data regarding inhibitory effects against Malassezia sp., a major cause of dandruff and seborrheic dermatitis. To help address this paucity of information, this work was carried out to examine the antifungal effects of seaweed extracts against M. furfur and M. restricta. Of the fifty seven species of marine algae screened for their potential antifungal activity, only 17 species (29.8%) exhibited inhibitory activity. In agar disc diffusion method, the ether extracts of Corallina pilulifera, Enteromorpha linza, Laminaria japonica, Symphyocladia latiuscula and Ulva sp. showed strong antifungal activity. To identify major constituents in seaweed extracts, four selected extracts were analyzed on' a GC-MS equipped with a flame ionization detector, and compared to spectral data from databases WILEY229.LIB and NIST107.LIB. Most constituents in seaweed extracts are fatty acid-related compounds. When we evaluated any acute toxicity, the ether extracts of the selected four species were not toxic in mice. According to these results, it can be suggested that these seaweed extracts are valuable for the development of therapeutic agents in treating dandruff and seborrheic dermatitis. Further investigations to determine its bioactive compound(s) are currently in progress.

A proton induced X-ray emission (PIXE) analysis of concentration of major/trace and toxic elements in broiler gizzard and flesh of Tehsil Gujar Khan area in Pakistan

  • Nadeem, Khawar;Hussain, Javaid;Haq, Noaman Ul;Haq, A. Ul;Akram, Waheed;Ahmad, Ishaq
    • Nuclear Engineering and Technology
    • /
    • 제51권8호
    • /
    • pp.2042-2049
    • /
    • 2019
  • Ten gizzard and three flesh samples of the broiler were collected from different locations in Tehsil Gujar Khan District Rawalpindi, Pakistan. The samples were dried, crushed and ground. Pellets were prepared by pressing the powder of the samples and that of the Bovine liver 1577c reference material obtained from NIST, USA. Proton induced X-ray emission (PIXE) installed at National Center for Physics, Islamabad, Pakistan has been used as a reliable and improved technique to determine concentration of various major/trace and toxic elements e.g. S, Cl, K, Ca, Cl, Fe, Cu, Mn, Co, Zn, Ti, Cd, Ga, Cr, V and Ni, in the Gizzard and Flesh samples of the broiler. The concentrations of all the detected elements in the samples are statistically significant. The certified and measured values of the elements in the reference material were in agreement with each other within a deviation of 7%. S, Cl, K and Ca are within tolerable limits and are good for human consumption. Ti, V, Cr, Mn, Fe, Co, Ni, Cu and Zn were more than the acceptable limits of World Health Organization, WHO whereas Ga, As, Sn, Sb and Pb are not detected in most of the samples.

극저온 절대복사계에 소급한 칸델라 국가표준 실현 (Realization of the national standard of candela traceable to the absolute cryogenic radiometer at KRISS)

  • 박승남;김용완;이동훈
    • 한국광학회지
    • /
    • 제15권5호
    • /
    • pp.443-448
    • /
    • 2004
  • 국제단위계 중의 하나인 칸델라 눈금을 두 개의 광도계를 사용하여 실현하였다. 광도계의 분광감응도는 광출력을 전기출력으로 치환하여 측정하는 극저온 절대복사계에 소급하여 측정하였다. 광도계 외부에 설치된 정밀 개구는 다이아몬드 회전가공기로 가공하였으며 그 면적은 불확도 0.05%(k = 1) 이내로 측정하였다. 이 광도계를 사용하여 광도 벤치 위에서 1 kW FEL 전구로 칸델라 단위를 실현할 때 불확도를 분광감응도, 감응도의 공간 균일도, 개구 면적, FEL 전구의 색온도와 위치 재현성을 고려하여 평가한 결과 0.25%(k = 1)를 얻었다. 실현한 눈금의 유효성을 확인하기 위하여 미국 NIST의 눈금과 비교한 결과 0.1% 이내에서 일치하였다.

High Speed Separation of PFCs in Human Serum by C18-Monolithic Column Liquid Chromatography-Tandem Mass Spectrometry

  • Lee, Won-Woong;Lee, Sun-Young;Yu, Se Mi;Hong, Jongki
    • Bulletin of the Korean Chemical Society
    • /
    • 제33권11호
    • /
    • pp.3727-3734
    • /
    • 2012
  • An analytical method has been developed for the rapid determination of perfluorinated compounds (PFCs) in human serum samples. The extraction and purification of PFCs from human serum were performed by the modified method of previous report. Ten PFCs were rapidly separated within 3.3 min by C18-monolithic column liquid chromatography (LC) and detected by electrospray ionization (ESI) tandem mass spectrometry (MS/MS) in negative ion mode. The runtime of PFCs on monolithic column LC was up to 4-fold faster than that on conventional column LC. The effect of triethylamine (TEA) to the mobile phase has investigated on the overall MS detection sensitivity of PFCs in ESI ionization. Quantification was performed by LC-MS/MS in multiple-ion reaction monitoring (MRM) mode, using $^{13}C$-labeled internal standards. Method validation was performed to determine recovery, linearity, precision, and limits of quantification, followed by, the analysis of a standard reference material (SRM 1957 from NIST). The overall recoveries ranged between 81.5 and 106.3% with RSDs of 3.4 to 16.2% for the entire procedure. The calibration range extended from 0.33 to 50 $ng\;mL^{-1}$, with a correlation coefficient ($R^2$) greater than 0.995 and the limits of quantification with 0.08 to 0.46 $ng\;mL^{-1}$. This approach can be used for rapid and sensitive quantitative analysis of 10 PFCs in human serum with high performance and accuracy.

콘크리트의 수축으로 인한 미세균열 발생 평가를 위한 해석적 기법 (An Analytical Method for the Evaluation of Micro-cracking in Concrete Shrinkage Induced)

  • 송영철;김도겸;문재흠
    • 콘크리트학회논문집
    • /
    • 제22권1호
    • /
    • pp.69-76
    • /
    • 2010
  • 콘크리트의 수축으로 인한 균열가능성 평가에 있어서 대부분의 경우 콘크리트를 균질한 물질로 가정하는 방식으로 접근하고 있다. 그러나 이러한 방식으로 접근할 경우 불구속조건 하의 콘크리트에서 자기수축으로 인한 미세균열(micro-cracking) 현상을 평가하는 것이 불가능함과 동시에 콘크리트 내부의 균열 발생 현상을 이해하는데 한계가 있다. 이에 이 연구에서는 시멘트 모르타르 시험체를 가지고 실험적으로는 음향방출(acoustic emission) 장비를 사용하여 내부 균열 발생량을 측정 및 평가하였으며, 이론적인 접근방식의 일환으로 실제 모르타르 시험체로부터 구하여진 이차원 이미지를 사용하여 NIST에서 개발한 OOF code로 유한요소해석을 수행하였다. 실험 및 해석 결과, 모르타르의 내부에서 시멘트 페이스트상의 수축 및 골재의 내부구속으로 인하여 발생하는 미세균열 발생 현상을 보다 현실적으로 이해할 수 있었다.

모형 가스터빈 연소기의 입구 형상변화에 따른 연소 불안정성에 관한 LES 연구 (LES Studies on the Combustion Instability with Inlet Configurations in a Model Gas Turbine Combustor)

  • 황철홍;이창언
    • 대한기계학회논문집B
    • /
    • 제32권5호
    • /
    • pp.342-350
    • /
    • 2008
  • The effects of combustion instability on flow structure and flame dynamics with the inlet configurations in a model gas turbine combustor were investigated using large eddy simulation (LES). A G-equation flamelet model was employed to simulate the unsteady flame behaviors. As a result of mean flow field, the change of divergent half angle($\alpha$) at combustor inlet results in variations in the size and shape of the central toroidal recirculation (CTRZ) as well as the flame length by changing corner recirculation zone (CRZ). The case of ${\alpha}=45^{\circ}$ show smaller size and upstream location of CTRZ than those of $90^{\circ}$ and $30^{\circ}$ by the development of higher swirl velocity. The flame length in the case of ${\alpha}=45^{\circ}$ is shorter than other cases, while the case of ${\alpha}=30^{\circ}$ yields the longest flame length due to the decrease of effective reactive area with the absence of CRZ. Through the analysis of pressure fluctuation, it was identified that the case of ${\alpha}=45^{\circ}$ shows the largest damping effect of pressure oscillation in all configurations and brings in the noise reduction of 2.97dB, compared to that of ${\alpha}=30^{\circ}$ having the largest pressure oscillation. These reasons were discussed in detail through the analysis of unsteady phenomena related to recirculation zone and flame surface. Finally the effects of flame-acoustic interaction were evaluated using local Rayleigh parameter.

GC-MS 기반 대사체학 기술을 응용한 참당귀의 산지비교분석 (Comparative Analysis of Cultivation Region of Angelica gigas Using a GC-MS-Based Metabolomics Approach)

  • 강귀보;임재윤
    • 한국약용작물학회지
    • /
    • 제24권2호
    • /
    • pp.93-100
    • /
    • 2016
  • Background: A set of logical criteria that can accurately identify and verify the cultivation region of raw materials is a critical tool for the scientific management of traditional herbal medicine. Methods and Results: Volatile compounds were obtained from 19 and 32 samples of Angelica gigas Nakai cultivated in Korea and China, respectively, by using steam distillation extraction. The metabolites were identified using GC/MS by querying against the NIST reference library. Data binning was performed to normalize the number of variables used in statistical analysis. Multivariate statistical analyses, such as Principal Component Analysis (PCA), Partial Least Squares-Discriminant Analysis (PLS-DA), and Orthogonal Partial Least Squares-Discriminant Analysis (OPLS-DA) were performed using the SIMCA-P software. Significant variables with a Variable Importance in the Projection (VIP) score higher than 1.0 as obtained through OPLS-DA and those that resulted in p-values less than 0.05 through one-way ANOVA were selected to verify the marker compounds. Among the 19 variables extracted, styrene, ${\alpha}$-pinene, and ${\beta}$-terpinene were selected as markers to indicate the origin of A. gigas. Conclusions: The statistical model developed was suitable for determination of the geographical origin of A. gigas. The cultivation regions of six Korean and eight Chinese A. gigas. samples were predicted using the established OPLS-DA model and it was confirmed that 13 of the 14 samples were accurately classified.

주요기반시설 서비스의 안정적 운영을 위한 보안 프레임워크 설계에 관한 연구 (A Study on the Security Framework Design for Stable Operation of Critical Infrastructure Service)

  • 이수연;유지연;임종인
    • 한국IT서비스학회지
    • /
    • 제15권4호
    • /
    • pp.63-72
    • /
    • 2016
  • Critical infrastructure has been operating in a closed environment with a completely separate information system and in the private area. However, with the current ICT environment changes due to convergence and open platforms it has increased the threats and risks to critical infrastructure. The importance of cyber security is increasing in the infrastructure control system, such as the outbreak of Ukraine blackout in 2015 by a malicious code called 'black energy'. This thesis aims to recognize the importance and necessity of protecting the critical infrastructure service, designing a security framework reflecting environmental and characteristic changes, and analyzing the management system suitable for a security framework. We also propose a theoretical basis for constructing a new security framework by comparing and analyzing seven international security management system standards, such as NIST 800-82 and IEC 62443-2-1, which are used in the control system. As a result, the environment surrounding critical infrastructure changes with the characteristics of connectivity, openness, and finality was studied, and as a response to this, many scholars and institutions present critical infrastructure security frameworks as cycle enhancement type structures, risk management structures, and management domain expansion structures. In response, the security framework encompassing these structures, CISF (Critical Infrastructure Security Framework), was designed. Additionally, through the security related international standard and criterion analysis, as a newly designed security standard suitable for CISF, IEC 62443-2-1 is reviewed and suggestions are made.

특징점과 필터뱅크에 기반한 적응적 혼합형 지문정합 방법 (Adaptive Hybrid Fingerprint Matching Method Based on Minutiae and Filterbank)

  • 정석재;박상현;문성림;김동윤
    • 한국정보과학회논문지:소프트웨어및응용
    • /
    • 제31권7호
    • /
    • pp.959-967
    • /
    • 2004
  • Jain 등은 한 지문 영상에 특징점 기반 지문 정합 방법과 필터뱅크 기반 지문 정합 방법을 적용해 두 정합 방법의 성능을 혼합하는 혼합형 지문정합 방법을 제안하고, 이 방법이 두 가지 각 정합 방법에 비해 높은 성능을 보인다는 것을 실험을 통해 입증하였다[l]. 그러나 이 방법은 혼합을 수행할 때 두 정합 방법을 별도로 수행한 후, 각 방법의 정합도(matching score)에 가중치를 부여해 최종 정합도를 결정하므로 두 정합 방법의 특성을 상쇄 시키는 결과를 얻게 된다. 본 논문에서는 두 가지 정합 방법을 특징값 추출 과정에서 혼합하는 방법을 제안하였다. 이 방법은 필터뱅크 기반 방법보다는 낮은 ERR(Equal eRror Rate)을 보이나 특징점 기반 방법보다 높은 ERR을 보였다. 이에 본 논문에서는 적응적인 정합도 혼합방법을 제안하여, 두 가지 방법의 특성을 살리도록 적응적으로 정합도를 선택하는 방법을 취했다. 이 방법을 이용해 Jain 등의 혼합형 방법보다 더 낮은 ERR을 얻을 수 있었다. 제안한 방법에 따라 NIST Special Database 14 지문 데이타로 실험한 결과 ERR에서 약 1%의 성능 향상을 보였다.