• Analytical Science and Technology
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• v.21 no.6
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• pp.502-509
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• 2008

An ID LC/MS (isotope dilution liquid chromatography/mass spectrometry) was used as a primary method for the quantitative analysis of cholesterol in human serum. The separation of cholesterol was carried out by Thermo ODS hypersil $C^{18}$ column. The mobile phase was 100% methanol, and flow rate was $0.3m{\ell}/min$. Cholesterol and cholesterol-$3,4-13C_2$ were monitored at m/z 369.4 and 371.3, which correspond to $[M-H_2O+H]^+$ respectively. In order to verify the measurement method, NIST SRM 909b was analyzed. The results agreed well with certified values within uncertainty. The four kinds of serum certified reference material were prepared and certified. The repeatabilities of measurement were ranged from 0.1 to 0.8% (RSD), which were relatively good. The reproducibility between independent measurement run was below 0.24% (RSD). The expanded uncertainty was about 1.43% within the 95% confidence interval.

• Journal of the Korean Society of Radiology
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• v.17 no.2
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• pp.207-213
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• 2023

Computed tomography (CT) images are used as the basis for proton Bragg peak position estimation and treatment plan simulation. During the Hounsfield Unit (HU) based proton stopping power ratio (SPR) estimation, small differences in the patient's density and elemental composition lead to uncertainty in the Bragg peak positions along the path of the proton beam. In this study, we investigated the potential of dual-energy computed tomography image-based proton SPRs prediction accuracy to reduce the uncertainty of Bragg peak position prediction. Single- and dual-energy images of an electron density phantom (CIRS Model 062M electron density phantom, CIRS Inc., Norfolk, VA, USA) were acquired using a computed tomography system (Somatom Definition AS, Siemens Health Care, Forchheim, Germany) to estimate the SPRs of the proton beam. To validate the method, it was compared to the SPRs estimated from standard data provided by the National Institute of Standards and Technology (NIST). The results show that the dual-energy image-based method has the potential to improve accuracy in predicting the SPRs of proton beams, and it is expected that further improvements in predicting the position of the proton's Bragg peak will be possible if a wider variety of substitutes with different densities and elemental compositions of the human body are used to predict the SPRs.

• Analytical Science and Technology
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• v.15 no.5
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• pp.417-426
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• 2002

Inductively Coupled Plasma Dynamic Reaction Cell Quadrupole Mass Spectrometry (ICP-DRC-QMS) was characterized for the detection of the six naturally occurring calcium isotopes. The effect of the operating conditions of the DRC system was studied to get the best signal-to-noise ratio. This experiment shows that the potentially interfering ions such as $Ar^+$, ${CO_2}^+$, ${NO_2}^+$, $CNO^+$ at the calcium masses m/z 40, 42, 43, 44 and 48 were removed by flowing $NH_3$ gas at the rate of 0.7 mL/min $NH_3$ as reactive cell gas in the DRC with a RPq value (rejection parameter) of 0.6. The limits of detection for $^{40}Ca$, $^{42}Ca$, $^{43}Ca$, $^{44}Ca$, and $^{48}Ca$ were 1, 29, 169, 34, and 15 pg/mL, respectively. This method was applied to the determination of calcium in synthetic food digest samples (CCQM-P13) provided by LGC for international comparison. The isotope dilution method was used for the determination of calcium in the samples. The uncertainty evaluation was performed according to the ISO/GUM and EURACHEM guidelines. The determined mean concentration and its expanded uncertainty of calcium was ($66.4{\pm}1.2$) mg/kg. In order to assess our method, two reference samples, Riverine Water reference sample (NRCC SLRS-3) and Trace Elements in Water reference sample (NIST SRM 1643d), were analyzed.

• Convergence Security Journal
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• v.23 no.3
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• pp.3-11
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• 2023

Zero Trust, characterized by the principle of "Never Trust, Always Verify," represents a novel security paradigm. The proliferation of remote work and the widespread use of cloud services have led to the establishment of Work From Anywhere (WFA) environments, where access to corporate systems is possible from any location. In such environments, the boundaries between internal and external networks have become increasingly ambiguous, rendering traditional perimeter security models inadequate to address the complex and diverse nature of cyber threats and attacks. This research paper introduces the implementation principles of Zero Trust and focuses on the Micro Segmentation approach, highlighting its relevance in mitigating the limitations of perimeter security. By leveraging the risk management framework provided by the National Institute of Standards and Technology (NIST), this paper proposes a comprehensive procedure for the adoption of Zero Trust. The aim is to empower organizations to enhance their security strategies.

• The KIPS Transactions:PartC
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• v.10C no.1
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• pp.51-60
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• 2003

One of the most important matters in designing network and realizing service, is to grip on the traffic characteristics. Conventional traffic prediction and analysis used the models which based on the Poisson or Markovian. Recently, experimental research on the LAN, WAN and VBR traffic properties have been pointed rut that they weren't able to display actual real traffic specificities because the models based on the Poisson assumption had been underestimated the long range dependency of network traffic and self-similar peculiarities, it has been lately presented that the new approach method using self-similarity characteristics as similar as the real traffic models. Therefore, in this paper, we generated self-similar data traffic like real traffic as background load. On the existing ABR congestion control algorithm, we analyzed by classify into ACR, buffer utilization. cell drop rate, transmission throughput with the representative EFCI, ERICA, EPRCA and NIST twitch algorithm to show the efficient reaction about the burst traffic.

• Journal of the Korean Society of Radiology
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• v.9 no.6
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• pp.375-379
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• 2015

The purpose of this study is to determine the effective energy of a polyenegetic X-ray beam. The half value layer(HVL) of aluminum for 80 kVp X-ray beam was measured by using optically stimulated luminescent nanoDot dosimeters(OSLnDs). The linear attenuation coefficient(${\mu}$) was calculated using the measured HVL. And the mass attenuation coefficient(${\mu}/{\rho}$) was obtained by dividing the linear attenuation coefficient by the density(${\rho}$) of aluminum. The effective energy($E_{eff}$) of the obtained mass attenuation coefficient was determined using data of the X-ray mass attenuation coefficients for photon energies of aluminum given by National Institute of Standards and Technology(NIST). As a result, the HVL value is 2.262 mmAl. The ${\mu}$ value is $3.06cm^{-1}$. The ${\mu}/{\rho}$ value is $1.114cm^2/g$. And the $E_{eff}$ value was determined at 29.79 keV.

• Journal of Korean Society of Environmental Engineers
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• v.39 no.11
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• pp.634-640
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• 2017

Toxicity and fate assessment is necessary in the evaluation of the environmental, health and safety risks of engineered nanomaaterials (ENMs). Therefore, in order to ensure the reproducibility, reliability and relevance of ENMs toxicity results, stable and monomodal dispersion protocols in toxicity test media are needed. Zinc oxide nanoparticles (nZnO) are widely used in various products such as cosmetic products, paper, paints etc. In this study, nZnO dispersions in ecotoxicity test media were produced by following a series of steps of modified National Institute of Standards and Technology (NIST) Special publication 1200-5. In addition, natural organic matter (humic acid (HA)) was used as a stabilizing agent to disperse nZnO in the test media. The hydrodynamic diameters (HDD) of the nZnO in dispersion ranged between 150 and 200 nm according to the dynamic light scattering (DLS) measurement. Based on these dispersions in ecotoxicity test using ecological species (Oryzias latipes, Daphnia magna, Pseudokirchneriella subcapitata and Chironomusus riparius), dispersion protocol was found to have a considerable potential in ecotoxicity test of ENMs.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.19 no.6
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• pp.457-463
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• 2007

Various correlations of saturated vapor density in a truncated power series form are tested and compared in this study. Saturated vapor density correlation can be expressed relating logarithmic reduced density to the reduced temperature. Five types of correlation has been investigated using saturated vapor density data for 22 pure substance refrigerants from ASHRAE (American Society of Heating, Reftigerating and Air-Conditioning Engineers, Inc.) property tables and NIST (National Institute of Standards and Technology) Chemistry Webbook. Correlations are fitted to the data points by least squares method. Data points are equally weighted. The best type of correlation among the five types is suggested. The results obtained indicate that the best correlations with 3, 4, and 5 terms yield average AAD's (Average Absolute Deviation) of 0.27%, 0.04%, and 0.02%, respectively, while widely used conventional correlations with 3, 4, and 5 terms yield those of 1.19%, 0.61%, and 0.17%. The suggested type of correlation could reduce the number of terms while improving performance.

• Proceedings of the KSR Conference
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• 2007.05a
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• pp.1319-1324
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• 2007

Many researches have been performed to analyze the smoke movement in tunnel fires by using field model. Recently, FDS(Fire Dynamics Simulator) v.4, which is one of the field model and developed from NIST(National Institute of Standards and Technology), is widely used. In tunnel fires, FDS can show detail results in local point, but it has difficulties in boundary condition and taking long computing time as the number of grid increases. So, there is a need to use alternative method for tunnel fire simulation. A zone model is different kind of CFD method and solves ordinary differential equation based on conservation and auxiliary equations. It shows good macroscopic view in less computing time compared to field model. In this study, therefore, to confirm the applicability of CFAST in tunnel fire analysis, numerical simulations using CFAST are conducted to analyze smoke movement in longitudinal ventilation reduced-scale tunnel fires. Then the results are compared with experimental results. The differences of temperature and critical velocity between numerical results and experimental data are over $30^{\circ}C$ and 0.9m/s, respectively. These values are out of error range. It shows that CFAST 6.0 is hard to be used for tunnel fire simulation.

• Analytical Science and Technology
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• v.20 no.1
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• pp.33-40
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• 2007

This study centered on the quantitative analysis of about 27 trace elements including toxic ones using instrumental neutron activation analysis of fine ambient particulate matter in the third and fourth industrial complex area of Daejeon city, Korea. For analytical quality control, the certified reference material (NIST, the National Institute of Standards and Technology, U.S.A., SRM 2783, air particulate on filter media) was used. The errors relative to SRM values of Sb, Mn, V, Mg, Na, K, Ti, Co, Zn, and Sm fell below 5%, while those of Cr, Fe, Ba, Th, Ce, Al, and Cu were less than 10%. From the results of the quantitative analysis, the concentration of toxic metals such as As, Mn, Se, V, and Zn were $3.26{\pm}2.72$, $9.86{\pm}4.71$, $2.18{\pm}1.25$, $4.91{\pm}2.41$, $158{\pm}78ng/m^3$, respectively. And the results of factor analysis indicated that there are no more than six factors of sources of fine ambient particulate with statistical significance in the study area.