• Title/Summary/Keyword: Multiple coating

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A Study on the Thermal Oxidation and Wettability of Lead-free Solders of Sn-Ag-Cu and Sn-Ag-Cu-In

  • Lee, Hyunbok;Cho, Sang Wan
    • Applied Science and Convergence Technology
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    • v.23 no.6
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    • pp.345-350
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    • 2014
  • The surface oxidation mechanism of lead-free solder alloys has been investigated with multiple reflow using X-ray photoelectron spectroscopy. It was found that the solder surface of Sn-Ag-Cu-In solder alloy is surrounded by a thin $InO_x$ layer after reflow process; this coating protects the metallic surface from thermal oxidation. Based on this result, we have performed a wetting balance test at various temperatures. The Sn-Ag-Cu-In solder alloy shows characteristics of both thermal oxidation and wetting balance better than those of Sn-Ag-Cu solder alloy. Therefore, Sn-Ag-Cu-In solder alloy is a good candidate to solve the two problems of easy oxidation and low wettability, which are the most critical problems of Pb-free solders.

Effect of Thermal Oxidation Coating on the Hot Forging Process of High Strength Ti-6Al-4V Bolt (Ti-6Al-4V 고강도 볼트의 성형성에 미치는 표면산화효과)

  • Kim, Jeoung-Han;Lee, Chae-Hoon;Hong, Jae-Keun;Kim, Jae-Ho;Yeom, Jong-Taek
    • Transactions of Materials Processing
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    • v.18 no.3
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    • pp.251-255
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    • 2009
  • Since fastener bolt for airplane require high specific strength and corrosion resistance, Ti-6Al-4V alloy is widely used. However, the Ti-6Al-4V bolt is generally manufactured by cutting and rolling because of their poor workability. The aim of present work is to develop hot forming technology for high strength Ti-6Al-4V. Various heat-treatments were applied to specimen in order to increase hot-workability and prevent galling with die. Multiple forging were simulated with FE code to determine optimum process parameters including specimen temperature, strain rate, local strain, and thermal shrinkage. Forged samples were heat-treated again to increase their mechanical properties.

Ferroelectric Thin Film as a substitute for Non-volatile Memory (비휘발성 메모리용 대체 강유전체 박막)

  • 김창영;장승우;우동찬;남효덕;이희영
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.509-512
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    • 1999
  • Ferroelectric Sr$_2$(Nb, Ta)$_2$O$_{7}$(SNTO), La$_2$Ti$_2$O$_{7}$(LTO) thin films were prepared by sol-gel processes. SNTO, LTO thin films were spin-coated on Pt/TiO$_2$/SiO$_2$/Si(100). Pt/Ti/SiO$_2$/Si(100). PT/ZrO$_2$/SiO$_2$/Si(100) substrates. After multiple coating, dried thin films were heat-treated for decomposition of residual organics and crystallization. Dielectric and other relevant electrical properties were measured and the results showed a little possibility in ferroelectric gate random access memory devices.ces.

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Hydrogen Bonding-Driven Assembling of Thin Multiwalled Carbon Nanotubes (수소결합에 의한 얇은 다중벽 탄소나노튜브의 자기조립)

  • Han, Joong-Tark;Kim, Sun-Young;Woo, Jong-Seok;Lee, Gun-Woong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.426-427
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    • 2007
  • Here we describe the formation of a self-assembled film of thin multiwalled carbon Nanotubes(t-MWNT) modified with hydroxy groups through hydrogen peroxide treatment. Morphologies of t-MWNT films could be controlled by the various coating method, such as filtering, drop casting, spraying method, etc. The results show that on densification of the CNT suspension during drying, multiple hydroxy group-modified MWNTs can be self-assembled through strong surface hydrogen bond interaction while MWNTs usually exist an entangled state in the film. The interaction between t-MWNT was illustrated from Raman spectrum of spray coated films.

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Development of Air-powered Handpiece for Surgical Operation (외과 수술용 Air-Powered Handpiece 개발)

  • 윤길상;이영훈;허영무;서태일;최길운
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.3
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    • pp.188-193
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    • 2004
  • The purpose of this paper is concerned with a development of an air-powered handpiece for surgical operation. The handpiece is the tool of surgical instruments and it can be used to interchange multiple attachments for drilling, pinning, sawing, driving screws and reaming. Most of domestic medical instruments bring in overseas and the air-powered handpiece imported from foreign countries at 100% too. Therefore we develop new air powered handpiece. we research in 2D and 3D modeling, design of air line, analyze structure. The air-powered handpiece composes of body, power supply air-line, elements for mechanical power transmission, attachment, and surgical tools. The handpiece is developed by several processes that 3D design, machining, heat treatment and coating. The developed handpiece is experimented to confirm check the efficiency.

Magnetic withdrawal of particles for multiple purposes in nuclear power plants

  • Kam, Dong Hoon;Jeong, Yong Hoon;Choi, Sung-Min;Yun, Jong-Il
    • Nuclear Engineering and Technology
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    • v.53 no.12
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    • pp.3979-3989
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    • 2021
  • Several parametric effects on the magnetic collection have been evaluated considering dimension, strength of external magnetic field, injected velocity and particle concentration in the working fluid. Besides, accidental environments, expected in the containment of nuclear power plants, have also been addressed for the capture efficiency. The capture efficiency is especially enhanced with magnetic particle size and magnetic field strength through increased magnetic force; the non-magnetic coating thickness and fluid velocity hinder the magnetic collection. Based on the assessment, the magnetic withdrawal system can effectively capture magnetic particles even under accidental environments. Withdrawal of multifunctional magnetic particles or filtering of magnetic impurities can be effectively realized through the system.

Nanoparticles Modified With Cationic Thiol Surfactant as Efficient Inhibitors for the Corrosion of Carbon Steel

  • Azzam, Eid M.S.;Sami, Radwa M.;Alenezi, Khalaf M.;El Moll, Hani;Haque, A.
    • Journal of Electrochemical Science and Technology
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    • v.12 no.3
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    • pp.308-316
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    • 2021
  • In this work, we report synthesis, characterization and corrosion inhibition properties of cationic thiol surfactant-capped silver (SC-Ag-NPs) and gold (SC-Au-NPs) nanoparticles. SC-Ag-NPs and SC-Au-NPs were characterized using regular techniques include TEM. Corrosion study was carried out using carbon steel (CS) in 3.5% NaCl aqueous solution and characterized using multiple electrochemical techniques. Our results suggest that the paint containing SC-Ag-NPs and SC-Au-NPs endow efficient corrosion protection to the CS. Especially, SC-Au-NPs based paint form a stronger barrier between the metal and the corrosive ions, leading to better inhibition properties.

Evaluation Method for Improvement Efficiency of Indoor Air Quality in Residence (주택의 실내공기질 개선 평가 방법)

  • Yang, Won-Ho;Son, Bu-Soon;Yim, Sung-Kuk
    • Journal of Environmental Health Sciences
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    • v.33 no.4
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    • pp.255-263
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    • 2007
  • Indoor air quality is the dominant contributor to total personal exposure because most people spend a majority of their time indoors. The purposes of this study were to evaluate the alternative method for improvement of indoor air quality in house after coating titanium dioxide ($TiO_2$) photocatalyst for interior part of the house using nitrogen dioxide ($NO_2$) multiple measurements. To evaluate the alternative method in indoor environment, daily indoor and outdoor $NO_2$ concentrations of an apartment and a detached house were daily measured for consecutive 21 days in winter and summer, respectively, Another daily 21 measurements were carried out after $TiO_2$ coating on wall paper of interior part in houses. All $NO_2$ concentrations were measured by passive filter badges. Indoor air quality models using mass balance are useful tool to quantify the relationship between indoor air pollution levels, ambient concentrations, and explanatory variables. Using a mass balance model and linear regression analysis, penetration factor (ventilation rate divided by sum of ventilation rate and decay rate) and source strength factor (emission rate divided by sum of ventilation rate and decay rate) were calculated. Subsequently, the decay constants were estimated. In this study. magnitude of improvement of indoor air quality could be evaluated by decay constant.

Drying Shrinkage of Concretes according to Different Volume-Surface Ratios and Aggregate Types (형상비 및 골재의 종류에 따른 콘크리트 시편의 건조수축특성 연구)

  • Yang, Sung-Chul;Ahn, Nam-Shik;Choi, Dong-Uk;Kang, Seoung-Min
    • International Journal of Highway Engineering
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    • v.6 no.4 s.22
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    • pp.109-121
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    • 2004
  • This study was performed to investigate the characteristics of drying shrinkage for concrete slabs as a project for Korean pavement design procedure. According to the volume-surface ratios and aggregate types, the experiments have been executed for 252 days. In order to simulate the volume-surface ratio of a real concrete pavement slab, three-layer epoxy coating and wrapping were used to prevent the evaporation at the part of specimen surfaces. As a result of preliminary test, coating and wrapping method was identified as reliable for three months. According to the volume-surface ratio, the drying shrinkage of the concrete specimen using sandstone was measured 1.32 to 1.8 times higher than that of the limestone specimen. Comparing to the measured drying shrinkage strains and established ACI and CEB-FIP model equations, it turned out that those model equations were underestimated. Finally, considering the age and volume-surface ratios, the prediction equations of the drying shrinkage of concrete specimen were proposed through a multiple nonlinear regression analysis.

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Fabrication of Alloy Target for Formation of Ti-Al-Si-N Composite Thin Film and Their Mechanical Properties (Ti-Al-Si-N 박막 제작을 위한 합금 타겟 제조 및 박막의 기계적 특성)

  • Lee, Han-Chan
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.10
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    • pp.665-670
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    • 2016
  • Prevailing dissemination of machine tools and cutting technology have caused drastic developments of high speed dry machining with work materials of high hardness, and demands on the high-hardness-materials with high efficiency have become increasingly important in terms of productivity, cost reduction, as well as environment-friendly issue. Addition of Si to TiAlN has been known to form nano-composite coating with higher hardness of over 30 GPa and oxidation temperature over $1,000^{\circ}C$. However, it is not easy to add Si to TiAlN by using conventional PVD technologies. Therefore, Ti-Al-Si-N have been prepared by hybrid process of PVD with multiple target sources or PVD combined with PECVD of Si source gas. In this study, a single composite target of Ti-Al-Si was prepared by powder metallurgy of MA (mechanical alloying) and SPS (spark plasma sintering). Properties of he resulting alloying targets were examined. They revealed a microstructure with micro-sized grain of about $1{\sim}5{\mu}m$, and all the elements were distributed homogeneously in the alloying target. Hardness of the Ti-Al-Si-N target was about 1,127 Hv. Thin films of Ti-Al-Si-N were prepared by unbalanced magnetron sputtering method by using the home-made Ti-Al-Si alloying target. Composition of the resulting thin film of Ti-Al-Si-N was almost the same with that of the target. The thin film of Ti-Al-Si-N showed a hardness of 35 GPa and friction coefficient of 0.66.