• Journal of the korean society of oceanography
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• v.36 no.4
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• pp.101-108
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• 2001

Polybrominated diphenylether (PBDEs) congeners, 2,4,4'-TrBDE, 2,2',4,4'-TeBDE, 2,2',4,4',5-PeBDE, 2,2',4,4',5,5'-HXBDE, and 2,2',4,4',5,6-HxBDE, were measured in sediments from 52 stations in the southeastern coastal areas of Korea. Sediment samples were analyzed using gas chromatography coupled to mass spectrometer detector (GC/MSD) with positive electron impact (PEI) mode. New analytical methodology for PBDEs by the isotope dilution method was established using a multi-layer silica gel column chromatography. Total PBDEs levels in sediments for Pohang coast ranged from 1,1 to 33.8 ng/g dry weight (mean 5.3 ng/g dry), from 1.6 to 36.4 ng/g dry weight (mean 5.7 ng/g dry) for Ulsan coast, from 0.8 to 20.3 ng/g dry weight (mean 4.9 ng/g dry) for Busan coast, and from 0.8 to 10.3 ng/g dry weight (mean 4.4 ng/g dry) for Jinhae Bay. PBDEs contamination in surface sediments from Korean southeastern coasts was relatively moderate in comparison to that of other marine environment in the world. The predominant PBDE congeners were 2,2',4,4'-TeBDE and 2,2',4,4',5-PeBDE.

• Wind and Structures
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• v.9 no.2
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• pp.125-146
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• 2006

Stonecutters Bridge of Hong Kong is a cable-stayed bridge with two single-column pylons each 298 m high and an aerodynamic twin deck. The total length of the bridge is 1596 m with a main span of 1018 m. The top 118 m of the tower will comprise structural steel and concrete composite while the bottom part will be of reinforced concrete. The bridge deck at the central span will be of steel whilst the side spans will be of concrete. Stonecutters Bridge has adopted a twin-girder deck design with a wide clear separation of 14.3 m between the two longitudinal girders. Although a number of studies have been conducted to investigate the aerodynamic performance of twin-girder deck, the actual real life application of this type of deck is extremely limited. This therefore triggered the need for conducting the present studies, the main objective of which is to investigate the performance of Stonecutters Bridge against flutter at its in-service stage as well as during construction. Based on the flutter derivatives obtained from the 1:80 scale rigid section model experiment, flutter analysis was carried out using 3-D finite element based single parameter searching method developed by the second author of this paper. A total of 6 finite element models of the bridge covering the in-service stage as well as 5 construction stages were established. The dynamic characteristics of the bridge associated with these stages were computed and applied in the analyses. Apart from the critical wind speeds for the onset of flutter, the dominant modes of vibration participating in the flutter vibration were also identified. The results indicate that the bridge will be stable against flutter at its in-service stage as well as during construction at wind speeds much higher than the verification wind speed of 95 m/s (1-minute mean).

• The Journal of Korean Institute of Communications and Information Sciences
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• v.36 no.6A
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• pp.551-557
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• 2011

We investigate lattice-reduction-aided precoding techniques using Look-Up table (LUT) for multi-user multiple-input multiple-output(MIMO) systems. Lattice-reduction-aided vector perturbation (VP) gives large sum capacity with low encoding complexity. Nevertheless lattice-reduction process based on the LLL-Algorithm still requires high computational complexity since it involves several iterations of size reduction and column vector exchange. In this paper, we apply the LUT-aided lattice reduction on VP and propose a scheme to generate the LUT efficiently. Simulation results show that a proposed scheme has similar orthogonality defect and Bit-Error-Rate(BER) even with lower memory size.

• Archives of Pharmacal Research
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• v.27 no.9
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• pp.901-905
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• 2004

A rapid, sensitive and selective hydrophilic interaction liquid chromatography-tandem mass spectrometric(HILIC-MS/MS) method for the determination of tiapride in human plasma was developed. Tiapride and internal standard, metoclopramide were extracted from human plasma with dichloromethane at basic pH and analyzed on an Atlantis HILIC silica column with the mobile phase of acetonitrile-ammonium formate (190 mM, pH 3.0) (94：6, v/v). The ana-Iytes were detected using an electrospray ionization tandem mass spectrometry in the multi-ple-reaction-monitoring mode. The standard curve was linear (r＝0.999) over the concentration range of 1.00-200 ng/mL. The coefficient of variation and relative error for intra- and inter-assay at three QC levels were 6.4∼8.8％ and -2.0∼3.6％, respectively. The recoveries of tiapride ranged from 96.3 to 97.4％, with that of metoclopramide (internal standard) being 94.2％. The lower limit of quantification for tiapride was 1.00 ng/mL using 1 00 $\mu$L of plasma sample.

• Bulletin of the Korean Chemical Society
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• v.28 no.7
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• pp.1187-1194
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• 2007

The three major active isoflavonoids (calycosin-7-O-β -glucoside, isomucronulatol 7-O-β-glucoside, formononetin) and two main saponins (astragaloside I, astragaloside IV) in an extract of Radix Astragali were determined using rapid, sensitive, reliable HPLC/UV and LC-ESI-MS/MS methods. The separation conditions employed for HPLC/UV were optimized using a phenyl-hexyl column (4.6 × 150 mm, 5 μm) with the gradient elution of acetonitrile and water as the mobile phase at a flow rate of 1.0 mL/min and a detection wavelength of 230 nm. The specificity of the peaks was determined using a triple quadrupole tandem mass spectrometer equipped with an electrospray ionization (ESI) source that was operated in multiple reaction monitoring (MRM) in the positive mode. These methods were fully validated with respect to the linearity, accuracy, precision, recovery and robustness. The HPLC/UV method was applied successfully to the quantification of three major isoflavonoids in the extract of Radix Astragali. The results indicate that the established HPLC/UV and LC-ESI-MS/MS methods are suitable for the quantitative analysis and quality control of multi-components in Radix Astragali.

• Journal of the Korean housing association
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• v.24 no.6
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• pp.199-208
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• 2013

Developing a modern Han-style design and providing support for the commercialization development model in recent years has been propelled by the Han-style Support Strategies of the central government in conjunction with Han-style revitalization related projects that reflect the efforts of local governments. Han-style revitalization, the rekindling and revaluing of human behavior and interest in local governments following the social and cultural changes of the past decades, has emerged as an increasingly traditional area of concern in Han-style design. The purpose of the study was to provide a method which clarifies the design rules of the Han-style bathroom based on an evaluation of sensibilities and a rough set theory, and to give the components meaning and to systematize the method. Essentially, the Han-style bathroom design evaluation is a complex multi-criteria decision making process that seeks to improve the effectiveness and objectively of the Han-style bathroom design. Han-style bathroom design can be displayed in a graphical representation in response to input from the evaluation concerning sensibilities. Because the graphical representation is composed of 3D data, it is possible to display the Han-style bathroom design form in any desired perspective and also to perform shading and other operations. With the proposed method, it is possible to obtain a combination of several contributory components which can be referred to as Reducts, Covering Index and Column Score. Han-Style/Non Han-Style Bathroom Designs were identified by the combination of several components.

• Journal of the Institute of Electronics Engineers of Korea SD
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• v.43 no.11 s.353
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• pp.69-76
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• 2006

This paper proposes a self-repair system which is able to self-repair in cell unit by imitating the structure of living beings. Because the data of artificial cells move even diagonally, our system can self-repair faults not in column unit, but in cell unit. It leads to design an efficient self-repair system for multiple faults. Moreover, in artificial cell design, the usage of logic-based design method has smaller system size than that of the previous register-based design method. Our experimental result for 2-bit up/down counter shows 40.3% reduction in hardware overhead, compared to the previous method [6].

• Earthquakes and Structures
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• v.11 no.5
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• pp.823-840
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• 2016

The plastic hinge lengths of beams and columns are a critical demand parameter in the nonlinear analysis of structures using the finite element method. The numerical model of a plastic hinge plays an important role in evaluating the response and damage of a structure to earthquakes or other loads causing the formation of plastic hinges. Previous research demonstrates that the plastic hinge length of reinforced concrete (RC) columns is closely related to section size, reinforcement ratio, reinforcement strength, concrete strength, axial compression ratio, and so on. However, because of the limitations of testing facilities, there is a lack of experimental data on columns with large section sizes and high axial compression ratios. In this work, we conducted a series of quasi-static tests for columns with large section sizes (up to 700 mm) and high axial compression ratios (up to 0.6) to explore the propagation of plastic hinge length during the whole loading process. The experimental results show that besides these parameters mentioned in previous work, the plastic hinge of RC columns is also affected by loading amplitude and size effect. Therefore, an approach toward considering the effect of these two parameters is discussed in this work.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.17 no.2
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• pp.227-232
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• 2016

3D body scan data are used widely in various fields to make products and living spaces for superior human body fitness. Based on the 3D measurements of human bodies for teens in Size Korea 2013, this research provides a way of finding the representative body sizes and 3D body scan data. First, a multi-dimensional vector space consisting of many measurement items was projected onto a 2D vector space with circumference and length components via factor analysis. The representative body sizes and 3D scan data close to these values were obtained via the Mahalanobis distance in 2D space. Considering the adolescent growth pattern shown on this 2D space, males were divided into 4 age groups and females were divided into 3 age groups. Using the eigenbodies corresponding to the column vectors of the component score coefficient matrix, the representative body sizes of 13 measurement items (male) and 14 measurement items (female) for each age group were calculated. The representative body sizes and 3D scan data are very useful for modeling representative 3D human figures.

• YAKHAK HOEJI
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• v.57 no.4
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• pp.272-281
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• 2013

In this study, we developed and validated the HPLC method using the isolated components from Erycibae caulis. Their structures were elucidated by spectroscopic methods including UV, $^1H$-NMR, $^{13}C$-NMR, FAB-Mass and ESI-Mass as Compound 1 (crypto-chlorogenic acid), Compound 2 (scopolin), Compound 3 (neochlorogenic acid) and Compound 4 (3,4-di-O-caffeoylquinic acid). Major three compounds and scopoletin were decided as representative components of Erycibae caulis. We established HPLC analytical method by using the representative components and 20 commercial samples which were collected considering to various cultivated area. The HPLC fingerprinting was successfully achieved with an AKZO NOBEL Kromasil 100-5C18 column. The mobile phase consisted of 0.5% acetic acid in water (A) and methanol (B) using gradient method of 85(A) to 50(A) for 35min. The fingerprints of chromatograms were recorded at an optimized wavelength of 330 nm. This developed analytical method was validated with specificity, selectivity, accuracy and precision. And it is suggested that scopolin, scopoletin, neochlorogenic acid, 3,4-di-O-caffeoylquinic acid were more than 0.162%, 0.133%, 0.057%, 0.044%, respectively. In addition, principal component analysis (PCA) was performed on the analytical data of 20 different Erycibae caulis samples in order to classify samples collected from different regions. We hope that this assay can be readily utilized as quality control method for Erycibae caulis.