• Title/Summary/Keyword: Multi-Faculty

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Silica Gel-Supported Polyphosphoric Acid (PPA-SiO2) Catalyzed One-Pot Multi-Component Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones and -thiones: An Efficient Method for the Biginelli Reaction

  • Zeinali-Dastmalbaf, Mohsen;Davoodnia, Abolghasem;Heravi, Majid M.;Tavakoli-Hoseini, Niloofar;Khojastehnezhad, Amir;Zamani, Hassan Ali
    • Bulletin of the Korean Chemical Society
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    • v.32 no.2
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    • pp.656-658
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    • 2011
  • A green and efficient method for the synthesis of 3,4-dihydropyrimidin-2(1H)-ones and -thiones through one-pot three-component reaction of ethyl acetoacetate, an aryl aldehyde, and urea or thiourea in acetonitrile using silica gel-supported polyphosphoric acid (PPA-$SiO_2$) as catalyst is described. Compared to the classical Biginelli reaction conditions, the present methodology offers several advantages such as high yields, relatively short reaction times, mild reaction condition and a recyclable catalyst with a very easy work up.

Current Classification of the Bacillus pumilus Group Species, the Rubber-Pathogenic Bacteria Causing Trunk Bulges Disease in Malaysia as Assessed by MLSA and Multi rep-PCR Approaches

  • Husni, Ainur Ainiah Azman;Ismail, Siti Izera;Jaafar, Noraini Md.;Zulperi, Dzarifah
    • The Plant Pathology Journal
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    • v.37 no.3
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    • pp.243-257
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    • 2021
  • Bacillus pumilus is the causal agent of trunk bulges disease affecting rubber and rubberwood quality and yield production. In this study, B. pumilus and other closely related species were included in B. pumilus group, as they shared over 99.5% similarity from 16S rRNA analysis. Multilocus sequence analysis (MLSA) of five housekeeping genes and repetitive elements-based polymerase chain reaction (rep-PCR) using REP, ERIC, and BOX primers conducted to analyze the diversity and systematic relationships of 20 isolates of B. pumilus group from four rubber tree plantations in Peninsular Malaysia (Serdang, Tanah Merah, Baling, and Rawang). Multi rep-PCR results revealed the genetic profiling among the B. pumilus group isolates, while MLSA results showed 98-100% similarity across the 20 isolates of B. pumilus group species. These 20 isolates, formerly established as B. pumilus, were found not to be grouped with B. pumilus. However, being distributed within distinctive groups of the B. pumilus group comprising of two clusters, A and B. Cluster A contained of 17 isolates close to B. altitudinis, whereas Cluster B consisted of three isolates attributed to B. safensis. This is the first MLSA and rep-PCR study on B. pumilus group, which provides an in-depth understanding of the diversity of these rubber-pathogenic isolates in Malaysia.

Mechanical properties of demountable shear connectors under different confined conditions for reusable hybrid decks

  • Kavour, Florentia;Christoforidou, Angeliki;Pavlovic, Marko;Veljkovic, Milan
    • Steel and Composite Structures
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    • v.43 no.4
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    • pp.419-429
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    • 2022
  • In response to the sustainability requirements set in the EU Commission's "Green Deal" towards reduction of the greenhouse gas emissions, it is estimated that the structural design for deconstruction is going to contribute considerably to the sustainable development of the built environment. The demountability of multi-material structural systems basically depends on the shear connectors used in the structural system. This paper focuses on a type of demountable injected shear connector with an injected steel-reinforced resin (iSRR) which consists of spherical steel particles embedded in a resin. Its application to steel-to-concrete and steel-to-Fiber Reinforced Polymer (FRP) decks is presented along with its benefits. In parallel, an overview of the experimental and numerical research on the evaluation of the mechanical properties of the demountable bolted connectors with iSRR is discussed. Last, detailed finite element (FE) models and a parametric study are performed to quantify the confinement level of the SRR material influenced by the oversized hole diameter.

A STUDY ON THE AVERAGE CASE ERROR OF COMPOSITE NEWTON-COTES QUADRATURES

  • Park, Sung-Hee;Park, Jung-Ho;Park, Yoon-Young
    • Journal of applied mathematics & informatics
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    • v.12 no.1_2
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    • pp.107-117
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    • 2003
  • We study the integration problem in which one wants to compute the approximation to the definite integral in the average case setting. We choose the composite Newton- Cotes quadratures as our algorithm and the function values at equally spaced sample points on the given interval[0, 1]as information. We compute the average case error of composite Newton-Cotes quadratures and show that it is minimal (modulo a multi-plicative constant).

Time Resolved Measurement of Electric Field Distribution in a Liquid Dielectric

  • Arii, Kiyomitsu;Ihori, Haruo;Fujii, Masaharu
    • KIEE International Transactions on Electrophysics and Applications
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    • v.2C no.6
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    • pp.287-291
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    • 2002
  • Measurement technique of three dimensional electric field distribution in liquid dielectrics have been studied. Kerr effect and computed tomography(CT) method have been used. Measuring time has been shortened by the use of multi-optical systems to less than several milliseconds. Near future, electric field distribution in front of a streamer tip of breakdown would be measured.

Fault Evaluation Based on Fuzzy Logic for Analog Electronic Circuits

  • Hashizume, Masaki;Iwata, Yoshihiro;Tamesada, Takeomi
    • Proceedings of the Korean Institute of Intelligent Systems Conference
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    • 1993.06a
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    • pp.1402-1405
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    • 1993
  • In this paper, a fault evaluation method is proposed, which is to determine whether analog electronic circuits are faulty or not. In our method, evaluation characteristics of an expert test engineer are defined by means of directed graphs. By performing a multi-stage fuzzy inference based on the graphs, novice test engineers can derive a fault evaluation result satisfied by the expert. The effectiveness of our method is checked by some experiments for an amplifier circuit.

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A state-space realization form of multi-input multi-output two-dimensional systems

  • Kawakami, Atsushi
    • 제어로봇시스템학회:학술대회논문집
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    • 1992.10b
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    • pp.214-218
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    • 1992
  • In this paper, we propose a method for obtaining state-space realization form of two-dimensional transfer function matrices (2DTFM). It contains free parameters. And, we perform various consideration about it. Moreover, we present the conditions so that the state-space realization form exists.

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Effect of an Al underlayer on the Growth of mm-long Thin Multi-walled Carbon Nanotubes in Water-Assisted Thermal CVD

  • Choi, In-Sung;Jeon, Hong-Jun;Lee, Han-Sung;Lee, Nae-Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.11a
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    • pp.26-26
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    • 2009
  • Vertically aligned arrays of mm-long multi-walled carbon nanotubes (MWCNTs) on Si substrates have been synthesized by water-assisted thermal chemical vapor deposition (CVD). The growth of CNTs was investigated by changing the experimental parameters such as growth temperature, growth time, gas composition, annealing time, catalyst thickness, and Al underlayer thickness. The 0.5-nm-thick Fe served as catalyst, underneath which Al was coated as a catalyst support as well as a diffusion barrier on the Si substrate. We grew CNTs by adding a little amount of water vapor to enhance the activity and the lifetime of the catalyst. Al was very good at producing the nm-size catalyst particles by preventing "Ostwald ripening". The Al underlayer was varied over the range of 15~40 nm in thickness. The optimum conditions for the synthesis parameters were as follows: pressure of 95 torr, growth temperature of $815^{\circ}C$, growth for 30 min, 60 sccm Ar + 60 sccm $H_2$ + 20 sccm $C_2H_2$. The water vapor also had a great effect on the growth of CNTs. CNTs grew 5.03 mm long for 30 min with the water vapor added while CNTs were 1.73 mm long without water vapor at the same condition. As-grown CNTs were characterized by using scanning electron microscopy (SEM), high resolution transmission electron microscopy (HRTEM), and Raman spectroscopy. High-resolution transmission electron microscopy showed that the as-grown CNTs were of ~3 graphitic walls and ~6.6 nm in diameter.

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Elastic solutions due to a time-harmonic point load in isotropic multi-layered media

  • Lin, Gao;Zhang, Pengchong;Liu, Jun;Wang, Wenyuan
    • Structural Engineering and Mechanics
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    • v.57 no.2
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    • pp.327-355
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    • 2016
  • A new analytical derivation of the elastodynamic point load solutions for an isotropic multi-layered half-space is presented by means of the precise integration method (PIM) and the approach of dual vector. The time-harmonic external load is prescribed either on the external boundary or in the interior of the solid medium. Starting with the axisymmetric governing motion equations in a cylindrical coordinate system, a second order ordinary differential matrix equation can be gained by making use of the Hankel integral transform. Employing the technique of dual vector, the second order ordinary differential matrix equation can be simplified into a first-order one. The approach of PIM is implemented to obtain the solutions of the ordinary differential matrix equation in the Hankel integral transform domain. The PIM is a highly accurate algorithm to solve sets of first-order ordinary differential equations and any desired accuracy of the dynamic point load solutions can be achieved. The numerical simulation is based on algebraic matrix operation. As a result, the computational effort is reduced to a great extent and the computation is unconditionally stable. Selected numerical trials are given to validate the accuracy and applicability of the proposed approach. More examples are discussed to portray the dependence of the load-displacement response on the isotropic parameters of the multi-layered media, the depth of external load and the frequency of excitation.