• Tribology and Lubricants
• /
• 제12권3호
• /
• pp.107-114
• /
• 1996

MoS$_{2}$ bonded film was applied to reduction gears, and its lubricating properties were experimentally evaluated in terms of the power transmission efficiency and the frictional noise with a dynamo-typed gear test rig. Tests were performed in both oil lubrication and dry condition where the rotating velocity and loading torque were varied. In dry condition, MoS$_{2}$ bonded films effected the power transmission efficiency to increase about 5%, and the frictional noise level to decrease about 6 dB under the test operating conditions. It well proved that MoS$_{2}$ bonded films were a very effective solid lubricant for reduction gears. In oil lubricating conditions, the frictional properties of the coated gears were mainly governed by the lubricating oil, and lubricating effects of MoS2 bonded films were not evident. The result suggested that lubricating effect of MoS$_{2}$ bonded films would be limited to prevent a damage of reduction gears in the initial run when they were used in oil lubrication conditions.

• Tribology and Lubricants
• /
• 제16권3호
• /
• pp.173-181
• /
• 2000

Friction, wear and corrosion characteristics of various MoS$_2$ bonded film lubricants were investigated to apply them to automotive wheel joints. MoS$_2$ bonded film lubricants were formulated by combinations of several additives and binders, and they were coated onto the pre-treated surfaces of specimens. Friction and wear characteristics were evaluated with Falex pin & vee-block test and LFW-1 block-on-ring test. For the corrosion resistant characteristics of the films, salt solution spray corrosion tests were performed. Results showed that MoS$_2$ bonded films containing both inorganic and organic corrosion-resistant additives yielded a synergy effect on anti-corrosion resistance. Also, binders having the better water-proof and thermal stability showed the lower friction and higher corrosion resistance.

• Tribology and Lubricants
• /
• 제12권1호
• /
• pp.15-21
• /
• 1996

Friction and wear properties of MoS$_2$ bonded films were studied using the Falex testing machine, and their properties were evaluated in terms of the life and the load carrying capacity of the films. MoS$_2$ bonded films were formulated from the mixtures of MoS$_2$ solid particles and epoxyphenol resin, and they were applied onto AISI 4130 steel surface by dipping method to form lubricating bonded films. The results of the life and the load carrying capacity of the films showed that films were mainly affected by the surface temperature arisen from the frictional heat at the contact surface. To obtain enhanced tribological properties of the films, various combinations of solid lubricants and additives with a basic polymer resin were attempted and evaluated. The effects of surface pretreatment, such as sand blast or Zn-phosphating, were also investigated.

• 한국윤활학회:학술대회논문집
• /
• 한국윤활학회 1997년도 제25회 춘계학술대회
• /
• pp.232-241
• /
• 1997

The tribological behavior for MoS$_2$ bonded films is evaluated according to the international standard testing methods, such as ASTM D 2625(Falex tester) and ASTM D 2714(LFW-1 tester). It has been well known that the tribological behavior for MoS$_2$ bonded films is affected by several factors. However, in this work, the wear life for MoS$_2$ bonded films is mainly experimentally measured with different contact geometry, and evaluated in terms of the frictional heating according to the contact geometry of tribotester. The test results show that the wear life of MoS$_2$ bonded films is significantly affected not only by the frictional heating, but also by the contact pressure, test running-in conditions, and the contact conformity.

• Tribology and Lubricants
• /
• 제13권3호
• /
• pp.20-27
• /
• 1997

The tribological behavior for $MoS_2$ bonded films is evaluated according to the international standard testing methods, such as ASTM D 2625 (Falex tester) and ASTM D 2714 (LFW1 tester). It has been well known that the tribological behavior for $MoS_2$ bonded films is affected by several factors. However, in this work, the wear life for $MoS_2$ bonded films is mainly experimentally measured with different contact geometry, and evaluated in terms of the frictional heating according to the contact geometry of tribotester. The test results show that the wear life of $MoS_2$ bonded films is significantly affected not only by the frictional heating, but also by the contact pressure, test running-in conditions, and the contact conformity.

• Tribology and Lubricants
• /
• 제14권4호
• /
• pp.72-78
• /
• 1998

In this work, the effects of binder materials on the tribological behavior were experimentally evaluated for air curable MoS$_2$bonded film lubricants. The binders tested were basically alkyd and acryl based resins, and also were modified by nitro-cellulose in various weight percentages. Effects on the binder ratio to solid lubricants and the molecular weight of binders were also investigated in all aspects of the tribological behavior. For the tests, LFW-1 and Falex tester were used to measure mainly the endurance life and load carrying capacity of bonded lubricants. Results showed that lubricants of methacrylic resin has the better performance than those of other resins, and also the properties of lubricants both of alkyd and acrylic resins could be improved by modification with nitro-cellulose. It was also shown that the optimum ratio of nitro-cellulose related closely to the binder material and the testing machine.

• 한국윤활학회:학술대회논문집
• /
• 한국윤활학회 1996년도 제24회 춘계학술대회
• /
• pp.35-40
• /
• 1996

Friction and wear behavior of MoS$_{2}$ bonded films were evaluated at a Block-on-Ring typed tribo-tester, and their properties were compared with those of Falex tester in terms of the wear life of the films. Test results showed that friction and wear properties were significantly affected by the test methods of different contact configuration, and the wear life at a Block-on-Ring type tribo-tester was mostly governed by the resin binder. To obtain long wear life of the films, various combinations of solid-resin-content ratio and chemical resin modification were attempted and evaluated. Adhesion properties of resin binders were also measured and compared by using a scratch tester.

• 한국윤활학회:학술대회논문집
• /
• 한국윤활학회 1996년도 제23회 춘계학술대회
• /
• pp.122-127
• /
• 1996

In this paper, the effects of the film tinckness, pre-treatment and testing load on. the tribological characteristics have been studied. During the "Ring on-Disk" testing period silica-gel was used to remove the effect of humidity. As a result, increasing the film thickness revealed prolonged wear life, in the case or reasl the testing loads the dynamic friction coefficient was decreased gradually but in regarding the wear life, an intermideate contact pressure (4kgf/mm${2}$) revealed the maximum value. In regarding the surface protuberance friction an intermediate value of area fraction (60%) revealed maximum wear life. In this paper, the qualitative model in regarding the variation of the friction coefficient andworn depth was presented.presented.

• 한국윤활학회:학술대회논문집
• /
• 한국윤활학회 1995년도 제22회 학술대회
• /
• pp.38-46
• /
• 1995

Bonded film을 형성시키기 위한 대표적인 고체윤활제들로는 이황화-몰리브데늄, 이황화-텅스텐(WS$_{2}$), 보론-나이트라이드(BN), 흑연(Graphite) 등을 들 수 있으며, 이들 고체윤활제를 표면에 효과적으로 부착시키기 위하여 사용되는 수지류는 페놀 및 에폭시계수지 등이 사용되고 있아. Bonded film의 마찰마모특성은 이와 간이 피막 내에 첨가된 고체윤활제 및 수지의 종류, 고체윤활 입자들의 크기 및 순도,그리고 이들 상호간의 배합비율 등에 의하여 크게 좌우되며, 아울러 피막 내에 소량으로 첨가될 수 있는 여러 가지 보조첨가제들에 의해서도 크게 영향을 받는 것으로 알려져 있다. 고체윤활제 성분들의 조성과 더불어, 재료표면의 물리화학적인 전처리 조건도 매우 중요한 요인이 될 수 있다. 따라서 본 논문에서는 이와 같은 윤활피막내 고체윤활제들의 배합, 고체윤활피막의 표면전처리 방법들을 변화하고 이들에 따른 상기 고체윤활피막들의 마찰 및 마모 특성에 관하여 시험을 행하였다.

• Tribology and Lubricants
• /
• 제19권4호
• /
• pp.203-210
• /
• 2003

In order to enhance the thermal stability of binder materials of bonded type solid lubricants, several metal-alkoxide based sol-gel materials such as methyltrimethoxysilane(MTMOS), titaniumisopropoxide (Ti(Opr$\^$i/)$_4$), zirconiumisopropoxide (Zr(Opr$\^$i/)$_4$) and aluminumbutoxide (Al(Obu$\^$t/)$_4$) were modified chemically by both epoxy and acrylic silane compounds. Friction and wear characteristics of the bonded solid lubricants, whose binders were of several hybrid ceramic materials, were tested with a reciprocating tribo-tester. Wear life was evaluated with respect to the heat-curing temperature, friction temperature, type of supplement lubricants, and ratio of binder materials. Test results showed that the Si-Zr hybrid ceramic materials modified by epoxy-silane compounds had a higher wear life compared to others. Sb$_2$O$_3$ was the most effective supplement lubricants in the high temperature, and BUS analyses revealed that it was caused mainly by a strong anti-oxidation effect to MoS$_2$ particles. The higher heat-curing temperature resulted in the higher wear life, and the higher friction temperature resulted in the lower wear life.