• Title/Summary/Keyword: Mixture experiments

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Stability of Matrine and Oxymatrine from the Biopesticide from Sophora flavescens under Aquatic and Soil Environment (고삼 추출물을 주성분으로 하는 유기농자재의 alkaloid계 살충성분 2종의 토양 및 수계 노출 안정성)

  • Kim, Jin Hyo;Choi, Geun-Hyoung;Lim, Sung-Jin;Park, Byung-Jun
    • Korean Journal of Environmental Agriculture
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    • v.34 no.1
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    • pp.1-5
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    • 2015
  • BACKGROUND: The stabilities of the two alkaloidal insecticides of S. flavescens including matrine and oxymatrine are important factor to establish expiry date and usage manual for crop protection. However, the environmental stability of the compounds had not been studied with the extract and its commercial biopesticide. METHODS AND RESULTS: The environmental stabilities of the two alkaloids were performed with extract of S. flavescens, and its two commercial biopesticides both in controlled aquatic and soil conditions. The half-lives of the total matrines for the extract and its two commercial biopesticides were estimated over 200 days both under aerobic and anaerobic water condition. Under dry soil condition, the initial decay rates of the matrines were calculated 0.0804-0.1275 ($t_{1/2}$ 5.4-8.6 days), and the half-lives under wet soil condition were calculated 33.0-231 days. Total soil bacteria on the wet soil ranged 6.0-8.0 log CFU/g-soil during the experiments period. CONCLUSION: The aquatic mixture of the extract showed excellent stability both with the extract and its biopesticides, however, the stability of soil mixture were shorter than the aquatic mixture, suggesting that soil metal consider as a catalyst for the degradation of the two alkaloids.

Solvent Extraction of Zirconium and Hafnium from Hydrochloric Acid solution by LIX 63 and Cyanex 301 (염산용액(鹽酸溶液)에서 LIX 63 및 Cyanex 301에 의한 지르코늄과 하프늄의 용매추출(溶媒抽出))

  • Min, Soo-Hwan;Lee, Man-Seung
    • Resources Recycling
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    • v.22 no.6
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    • pp.19-25
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    • 2013
  • Solvent extraction experiments have been conducted to separate Zr(IV) and Hf(IV) from chloride solutions by using LIX63 and Cyanex301. Zr and Hf were extracted by cation exchange reaction in the pH range from 1 to 4 by the extratants. Since the extraction percentage of the two metals was similar to each other, it was difficult to separate the two metals by using LIX63 or Cyanex301. Use of a mixture of LIX63/TBP or Cyanex301/TBP resulted in antagonism in our experimental ranges. Our data showed that there is some possibility of separating the two metals by the mixture of Cyanex301 and TBP because the extraction percentage of Hf decreased more rapidly than that of Zr as HCl concentration was decreased. The mixture of LIX63 and Cyanex301 had little effect on the separation of the two metals.

Implementation of An Unmanned Visual Surveillance System with Embedded Control (임베디드 제어에 의한 무인 영상 감시시스템 구현)

  • Kim, Dong-Jin;Jung, Yong-Bae;Park, Young-Seak;Kim, Tae-Hyo
    • Journal of the Institute of Convergence Signal Processing
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    • v.12 no.1
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    • pp.13-19
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    • 2011
  • In this paper, a visual surveillance system using SOPC based NIOS II embedded processor and C2H compiler was implemented. In this system, the IP is constructed by C2H compiler for the output of the camera images, image processing, serial communication and network communication, then, it is implemented to effectively control each IP based on the SOPC and the NIOS II embedded processor. And, an algorithm which updates the background images for high speed and robust detection of the moving objects is proposed using the Adaptive Gaussian Mixture Model(AGMM). In results, it can detecte the moving objects(pedestrians and vehicles) under day-time and night-time. It is confirmed that the proposed AGMM algorithm has better performance than the Adaptive Threshold Method(ATM) and the Gaussian Mixture Model(GMM) from our experiments.

Utilization of Canola Full-Fat Seeds and the Restored Mixture of Meal and Oil by Broiler (브로일러에 대한 Canola 전지종실 및 Canola 박과 기름 혼합물의 사료이용)

  • 이규호;심정석
    • Korean Journal of Poultry Science
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    • v.17 no.2
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    • pp.93-100
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    • 1990
  • Two experiments were conducted to assess the use of full-fat canola seed and restored oil meal plus oil of canola in the ration for broiler chicks. In the first experiment, broilers received diets containing 10% heated or non-heated full-fat canola seed and conola oil meal mixed with corresponding oil or animal fat. In the second experiment, broiler diets contained 10 or 20% of canola seed and canoia meal mixed with canola oil. Heat treatment of full-fat canola seed and the types of fat mixed with meals had no significant effect on all of broiler performance and nutrient retention parameters investigated. Bioilers consuming 10 to 20% dietary canola seed or mixture of canola meal plus oil performed as well as the control birds. It is concluded that the canola seed or the mixture of restored canola meal plus oil or fat can be well utilized by broiler at dietary levels of 10 to 20%.

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Design Optimization of Hydrated Liquid Crystalline Vesicles Containing a High Content of Ceramide Using DOE (실험 계획법을 적용한 세라마이드 고함량의 수화 액정형 베시클의 최적설계)

  • Shin, Juyeong;Jin, Byung-Suk
    • Journal of the Korean Applied Science and Technology
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    • v.39 no.5
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    • pp.623-631
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    • 2022
  • Using the design of experiment (DOE), factors affecting the particle size of hydrated liquid crystalline vesicles containing a high content of ceramide were analyzed and the mixture composition was optimized. Manufacturing temperature, amount of ethanol, and ultrasonic time were selected as the main variables affecting the droplet size of the vesicles, and the effect of these variables on the droplet size was examined through the signal to noise (S/N) ratios of Taguchi method and ANOVA analysis. In addition, mixture composition experiments of three lipid components constituting the vesicle membrane, hydrogenated phosphatidyl choline (HPC), cholesterol (Chol), and ceramide (Cer), were performed according to the simplex central design matrix of the mixture. Regression analysis was conducted with the experimental data to obtain a model equation, and the optimal mixing composition of the three lipid components to minimize the vesicle droplet size was determined as HPC (0.6), Chol (0.1), and Cer (0.3).

Evaluation on the Effect of Coal-ash as Landfill Cover Material of Mono-Layer Cover System through the Field Scale Test (현장 실험을 통한 단층형 매립복토시스템의 복토재로서 석탄회의 효과 검토)

  • Yun, Sung-Wook;Kang, Sin-Il;Jin, Hae-Geun;Kim, Pil-Joo;Kim, Soon-Oh;Yu, Chan
    • Journal of the Korean Geotechnical Society
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    • v.26 no.7
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    • pp.81-91
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    • 2010
  • In order to investigate the applicability and suitability of the coal ash (bottom ash) to landfill final cover, field pilot-scale lysimeter experiments were carried out. The mixture of loamy soil, bottom ash, and construction waste was placed as a cover material in lysimeter ($2m{\times}6m{\times}1.2m$) which were constructed with cement brick, and then volumetric water contents, pF value, and the quantity of runoff and seepage of treatment boxes filled with the mixture of loamy soil and the industrial by-products were monitored from July, 2007 to february, 2008. Among the cases tested, consequently, the case containing the mixture of bottom ash and loamy soil was most effective in plant growth and water retention ability.

Mechanical Properties and Field Implementation of Floor Mortar Incorporated with VAE Polymer (VAE 폴리머를 이용한 모르타르 바닥재의 역학적 특성과 현작 적용성)

  • Bang, Jin-Wook;Lee, Sun-Mok;Kim, Yun-Yong
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.3
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    • pp.27-34
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    • 2017
  • Recently, the importance of the industrial warehouse floor has been increasing due to the development of the distribution and logistics industry. In this present study, an early-hardening polymer floor mortar which can compensate for the limitation of conventional cement based floor mortar regarding fluidity and long curing time was developed. In order to achieve the early-hardening of mortar characteristic ultra rapid hardening cement was used as binder. Four types of mixture proportions in accordance with the vinyl acetate ethylene(VAE) polymer contents with range from 10% to 20% and the other proto proportion without VAE polymer were designed. Mechanical experiments including the fluidity test, compressive strength test, bending test, bond test, and abrasion test were conducted for all mixture proportions. From the flow test result, it was possible to achieve the high flow with 250 mm by controlling the amount of superplasticizer. The incorporation of VAE polymer was found to affect the compressive strength reduction, however, the flexural strength was higher than that of the proto mixture, and it was evaluated to increase the compressive strength / flexural strength ratio. Moreover, at least 2.6 times higher bond strength and more than 4 times higher abrasion resistance were secured. From the mechanical experiments results, the optimum mixing ratio of the VAE polymer was determined to be 10%. As a result of application and monitoring, it shows that it has excellent resistance to cracking, discoloration, impact, and scratch as well as bond performance compared to the cement based floor mortar.

Improved Compressive·Flexural Performance of Hybrid Fiber-Reinforced Mortar Using Steel and Carbon Fibers (강 및 탄소 섬유를 사용한 하이브리드 섬유보강 모르타르의 압축·휨성능 향상)

  • Heo, Gwang-Hee;Park, Jong-Gun;Seo, Dong-Ju;Koh, Sung-Gon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.25 no.5
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    • pp.48-59
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    • 2021
  • In this study, experiments were conducted to investigate the compressive·flexural performances of single fiber-reinforced mortar (FRM) using only steel fiber or carbon fiber which has different material properties as well as hybrid FRM using a mixture of steel and carbon fibers. The mortar specimens incorporated steel and carbon fibers in the mix proportions of 1+0%, 0.75+0.25%, 0.5+0.5%, 0.25+0.75% and 0+1% by volume at a total volume fraction of 1.0%. Their mechanical performance was compared and examined with a plain mortar without fiber at 28 days of age. The experiments of mortar showed that the hybrid FRM using a mixture of 0.75% steel fibers + 0.25% carbon fibers had the highest compressive and flexural strength, confirming by thus the synergistic reinforcing effect of the hybrid FRM. On the contrast, in the case of hybrid FRM using a mixture of 0.5% steel fibers + 0.5% carbon fibers witnessed the highest flexural toughness, suggesting as a result the optimal fiber mixing ratio of hybrid FRM to improve the strength and flexural toughness at the same time. Moreover, the fracture surface was observed through a scanning electron microscope (SEM) for image analysis of the FRM specimen. These results were of great help for images analysis of hybrid reinforcing fibers in cement matrix.

Changes of Biomass of Green Manure and Rice Growth and Yield using Leguminous Crops and Barley Mixtures by Cutting Heights at Paddy (두과 녹비작물과 보리 혼파 이용 시 예취 높이에 따른 Biomass와 벼 생육 및 수량 변화)

  • Jeon, Weon-Tai;Seong, Ki-Yeong;Oh, Gye-Jeong;Kim, Min-Tae;Lee, Yong-Hwan;Kang, Ui-Gum;Lee, Hyun-Bok;Kang, Hang-Won
    • Korean Journal of Soil Science and Fertilizer
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    • v.45 no.2
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    • pp.192-197
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    • 2012
  • The competition between green manure and forage crops frequently occurred at agricultural field because of soil fertility and livestock feeding selection. These experiments were carried out to evaluate the effects shoot and residue for green manure and forage production by leguminous crops and barley mixtures at paddy. Field experiments were conducted at paddy soil from 2008 to 2009. Treatments consisted of mixture and inter-seeding of barley and leguminous crops (hairy vetch and crimson clover). These treatments were divided into cutting height of 8 and 25 cm for using of green manure and forage at once. The residue biomass of 25 cm cutting height was higher than 8 cm and were no significantly between mixture and inter-seeding. However, residues of legume crop were significantly higher at inter-seeding than mixture. The shoot biomass of 8 cm cutting height was higher than 25 cm for forage using. The production of legume crop was high at the barley and hairy vetch seeding plot. The mixture of hairy vetch and barley showed the best biomass of shoot and residue for green manure and forage using at 25 cm of cutting height. Also this treatment could be possible to rice cultivation by no fertilization. Therefore, we suggested that 25 cm cutting of hairy vetch and barley mixture could be used for green manure and forage at the same time under rice-based cropping system.

A Study of the Optimization of the MOF-5 Synthesis Process using Design of Experiments (실험계획법을 이용한 MOF-5 합성공정 최적화 연구)

  • Lee, Min Hyung;Lee, Sangmin;Yoo, Kye Sang
    • Applied Chemistry for Engineering
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    • v.33 no.4
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    • pp.402-407
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    • 2022
  • Statistical design of experiments was used to optimize the MOF-5 synthesis process. A mixture design was employed to optimize precursor concentration. The optimal composition of three chemical materials, terephthalic acid, zinc acetate dihydrate, and N,N-dimethylformamide for MOF-5 synthesis was determined by extreme vertices design methods as follows; 1 mol : 2.7 mol : 40 mol. A multilevel factorial design was selected to screen the significance of synthesis reaction conditions such as temperature, time, and stirring speed. Statistical analysis results suggested excluding stirring speed from further investigation. Using a central composition design, the synthesis time and temperature were optimized. The quadratic model equation was derived from 13 synthesis experiments. The model predicted that MOF-5 synthesized at 119 ℃ for 10.4 h had the highest crystallinity.