• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.17 no.1
• /
• pp.39-45
• /
• 2004

Fine LaAlO$_3$ powders wore successfully synthesized from La$_2$O$_3$ and ${\gamma}$ $Al_2$O$_3$ powders milling for 10∼50 hours via the high energy milling technique (mechanochemical method) in room temperature and air. The particle size of LaAlO$_3$ powder were estimated from XRD patterns and SEM images to be 160∼180 nm. The LaAlO$_3$ ceramics arc derived for the synthesized powders (milling for 10, 30 and 50 hours) by sintering at 140$0^{\circ}C$ and 150$0^{\circ}C$. The micrographs of grains showed an agglomeration and the degree of agglomeration increased with the milling time. The LaAlO$_3$ made from synthesized powders milling for 50 hours can be sintered to 99.5％ of theoretical density at 150$0^{\circ}C$ for 1 hour. These ceramics exhibits a dielectric constant of 20, a dielectric loss of 0.0003 and a temperature coefficient of capacitance of 15 ppm/$^{\circ}C$ at 1 MHz.

• Journal of the Korean Society of Manufacturing Process Engineers
• /
• v.2 no.3
• /
• pp.20-25
• /
• 2003

The End-milling has been widely used in the industrial world because it is effective to cutting working with various shape. Recently the end-milling is demanded the high-precise technique with good surface roughness and rapid manufacturing time for precision machine and electronic elements. The cutting working of end-milling such as, cutting direction, revolution of spindle, feed rate and depth of cut have an effect on optimum surface roughness. This study was carried out to decide the working condition for optimum surface roughness and rapid manufacturing time by design of experiment and ANOVA. From the results of this study, the optimum working condition for end milling is upward cutting in cutting direction, 600rpm in revolution of spindle, 240mm/mm in feed rate, 2mm in axial depth of cut and 0 25mm in radial depth of cut. The design of experiment has become an useful method to select optimum working condition mend-milling.

• Transactions on Electrical and Electronic Materials
• /
• v.16 no.2
• /
• pp.53-61
• /
• 2015

High-energy ball milling was tested as a method for producing Ultra High Molecular Weight Polyethylene (UHMWPE)- based nanodielectrics containing 1 wt% and 5 wt% OctaIsoButylPOSS (OibPOSS). Qualitative and quantitative evaluations were used to explore the compatibility between OibPOSS and PE. Several ball milling variables were optimized in a bid to achieve UHMWPE/OibPOSS nanodielectrics. The morphology, as well as the thermal and the dielectric properties of the samples, were characterized by scanning electron microscopy, thermogravimetric analysis, broadband dielectric spectroscopy, and progressive-stress breakdown tests. The results showed that (i) ball milling was an effective method for producing UHMWPE/OibPOSS dielectric composites, but appeared ineffective in dispersing OibPOSS at the nanoscale, and (ii) the resulting UHMWPE/OibPOSS dielectric composites presented thermal and dielectric properties similar to those of neat UHMWPE.

• Carbon letters
• /
• v.15 no.3
• /
• pp.180-186
• /
• 2014

This study highlights a novel method and mechanism for the rapid and effective milling of carbon fibers (CFs) in silicon carbide (SiC) powder, and also the dispersion of CFs in SiC powder. The composite powders were prepared by chopping and exfoliation of CFs, and ball milling of CFs and SiC powder in isopropyl alcohol. A wide range of CFs loading, from 10 to 50 vol%, was studied. The milling of CFs and SiC powder was checked by measuring the average particle size of the composite powders. The dispersivity of CFs in SiC powder was checked through scanning electron microscope. The results show that the usage of exfoliated CF tows resulted in a rapid and effective milling of CFs and SiC powder. The results further show an excellent dispersion of CFs in SiC powder for all CFs loading without any dispersing agent.

• Journal of the Korean Society for Precision Engineering
• /
• v.18 no.5
• /
• pp.130-136
• /
• 2001

Generally, a metal slitting saw is plain milling cutter with thickness less than 3/16 inch. This is used for cutting a workpiece that high dimensional accuracy and surface finish is necessary. A small thin milling cutter like a metal slitting saw is useful for machining a narrow groove. In this case, built up edge(BUE) is severe at each tooth and affects the surface integrity of the machined surface and tool wear. It is well known that tool geometry and cutting conditions are decisive factors to remove BUE. In this paper, we optimized the geometry of the milling cutter and selected cutting conditions to remove BUE by the experimental investigation. The experiment was planned with Taguchi method based on the orthogonal array of design factors such as coating, rake angle, number of tooth, cutting speed, feed rate. Response table was obtained from the number of built-up edge generated at tooth. The optimized tool geometry and cutting conditions could be determined through response table. In addition, the relative effect of factors was identified bh the analysis of variance (ANOVA). Finally, coating and cutting speed turned out important factors for BUE.

• Applied Microscopy
• /
• v.50
• /
• pp.22.1-22.6
• /
• 2020

In-situ transmission electron microscopy (TEM) holders that employ a chip-type specimen stage have been widely utilized in recent years. The specimen on the microelectromechanical system (MEMS)-based chip is commonly prepared by focused ion beam (FIB) milling and ex-situ lift-out (EXLO). However, the FIB-milled thin-foil specimens are inevitably contaminated with Ga⁺ ions. When these specimens are heated for real time observation, the Ga⁺ ions influence the reaction or aggregate in the protection layer. An effective method of removing the Ga residue by Ar⁺ ion milling within FIB system was explored in this study. However, the Ga residue remained in the thin-foil specimen that was extracted by EXLO from the trench after the conduct of Ar⁺ ion milling. To address this drawback, the thin-foil specimen was attached to an FIB lift-out grid, subjected to Ar⁺ ion milling, and subsequently transferred to an MEMS-based chip by EXLO. The removal of the Ga residue was confirmed by energy dispersive spectroscopy.

• Journal of the Korean Magnetics Society
• /
• v.9 no.4
• /
• pp.217-222
• /
• 1999

The pick up impurity was studied for preparing the NiCuZn ferrite powder by a ball milling method that usually uses in the industrial ceramic process. The raw materials of NiO, CuO, ZnO, and $Fe_2O_3$ powder were weighted according to various spinel composition and mixed for 18 hrs by a wet ball milling method after that the slurry was followed by spray dried and calcined at $700^{\circ}C$ 3 hrs. The calcined NCZF powder was finally ball milled during 65 hrs as same method. The stainless steel ball and jar are used as mixing and milling equipment and the solid concentration of the slurry was 25 vol%. The impurities, stainless steel pickup, were effected by the composition of raw materials especially iron oxide, nickel oxide in the mixing process and by the rate of calcine of NiCuZn ferrite in final milling process. The empirical equation of stainless steel pickup was driven in the wet ball milling system. Finally, the composition of NiCuZn ferrite could be controlled by the empirical equation.

• The Journal of the Convergence on Culture Technology
• /
• v.9 no.6
• /
• pp.67-71
• /
• 2023

Recently, the method of making a dental prothesis is changed in the ICT based digital way. In particular, with the emergence of the CAD/CAM or 3D printing for dental purpose, a computer based digital type is selected gradually more than an analog type. To make an implant abutment, it is possible to apply the conventional technique of making round bars, or the technique using a CNC milling machine. This study tested these two types of the techniques to find which one had more precision and a smaller error when the margin and occlusal surface was made. According to the test, the technique using a CNC milling machine to make an implant abutment had a small error and supported precise processing in terms of the margin fit and the occlusal surface. Therefore, it was found to be useful in making a custom-made prothesis.

• Design & Manufacturing
• /
• v.14 no.2
• /
• pp.56-61
• /
• 2020

Recently, research for machining next-generation micro semiconductor processes and micro patterns has been actively conducted. In particular, it is applied to various industrial fields depending on the machining method in the case of FIB (Focused ion beam) milling. In this study, intends to deal with FIB milling machining technology for ultra-precision diamond tool fabrication technology. Ultra-precision diamond tools require nano-scale precision, and FIB milling is a useful method for nano-scale precision machining. However, FIB milling has a problem of Gaussian characteristics that are differently formed according to the beam current due to the input of an ion beam source, and there are process conditions to be considered, such as a side clearance angle problem of a diamond tool that is differently formed according to the tilting angle. A series of process steps for fabrication a ultra-precision diamond tool were studied and analyzed for each process. It was confirmed that the effect on the fabrication process was large depending on the spot size of the beam and the current of the beam as a result of the experimental analysis.

• 제어로봇시스템학회:학술대회논문집
• /
• 1997.10a
• /
• pp.1407-1410
• /
• 1997

Advanced sensor design and filtering technology have been studied to obtain information for condition monitoring and diagnostics inmachining processes. To develope and economic monitoring system in end milling processes, indirect and reliable type of cutting force estimators were required. In this paper, an estimation method of cutting forces during end milling processes was studied through the measurement of current signals obtained from spindle and feeddrive motors. Cutting force and torque models were derived from the cutting geometry in down milling processes. Relationships between motor currents and cutting forces were also developed in the form of AC and DC components from the developed force models. The validity of the cutting force estimator was confirmed by the experiments under various cutting conditions.