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http://dx.doi.org/10.4313/TEEM.2015.16.2.53

Polyethylene-Based Dielectric Composites Containing Polyhedral Oligomeric SilSesquioxanes Obtained by Ball Milling  

Guo, Meng (Department of Mechanical Engineering, Ecole de technologie superieure (ETS))
Frehchette, Michel (Department of Materials Science, Institut de recherche d'Hydro-Quebec (IREQ))
David, Eric (Department of Mechanical Engineering, Ecole de technologie superieure (ETS))
Demarquette, Nicole Raymonde (Department of Mechanical Engineering, Ecole de technologie superieure (ETS))
Publication Information
Transactions on Electrical and Electronic Materials / v.16, no.2, 2015 , pp. 53-61 More about this Journal
Abstract
High-energy ball milling was tested as a method for producing Ultra High Molecular Weight Polyethylene (UHMWPE)- based nanodielectrics containing 1 wt% and 5 wt% OctaIsoButylPOSS (OibPOSS). Qualitative and quantitative evaluations were used to explore the compatibility between OibPOSS and PE. Several ball milling variables were optimized in a bid to achieve UHMWPE/OibPOSS nanodielectrics. The morphology, as well as the thermal and the dielectric properties of the samples, were characterized by scanning electron microscopy, thermogravimetric analysis, broadband dielectric spectroscopy, and progressive-stress breakdown tests. The results showed that (i) ball milling was an effective method for producing UHMWPE/OibPOSS dielectric composites, but appeared ineffective in dispersing OibPOSS at the nanoscale, and (ii) the resulting UHMWPE/OibPOSS dielectric composites presented thermal and dielectric properties similar to those of neat UHMWPE.
Keywords
Polyethylene; Polyhedral oligomeric silsesquioxanes; Dielectric composites; Ball milling;
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