• Journal of electromagnetic engineering and science
• /
• v.14 no.4
• /
• pp.332-335
• /
• 2014

This paper investigates the phase singularity problem in microwave image reconstruction utilizing unwrapped phase data. The measured phases of the electric fields in most microwave measurement systems are wrapped. Thus, a certain phase unwrapping process is necessary for reconstruction of the image of a high contrast object. This unwrapping, however, is difficult in the presence of scattering nulls on/near the unwrapping path. At the null point, the phase value will be rendered, resulting in a poor image reconstruction. In this paper, we investigate the phase singularity arising from electromagnetic scattering nulls in microwave breast tomographic imaging. We then propose a transformation technique for the measured electric fields that avoids phase singularity.

• Journal of the Korean Chemical Society
• /
• v.55 no.6
• /
• pp.983-987
• /
• 2011

Surveys on the process of extracting acid from dried rinds of Garcinia oblongifolia Champ. ex Benth (G. oblongifolia) using microwave in terms of time, machine power and solid/liquid rate, have resulted in such findings as: the best time allocation for extracting is 25 minutes; machine power works best at level 2 (microwave power is 400 W); suitable rate of solid/liquid is 0.071 (approximately 150 mL solvent per 10 g of sample). The total amounts acid and (-)-hydroxycitric acid extracted from 100 g dried rinds of G. oblongifolia are 18.592 g and 10.137g respectively. This is the first finding on extraction of (-)-HCA from dried rinds of G. oblongifolia using microwave.

• Journal of Multimedia Information System
• /
• v.6 no.3
• /
• pp.155-164
• /
• 2019

We intended to confirm that microwave attenuation by tree leaves is strongly linked to water content in leaves. We sampled natural broadleaves, including Japanese cinnamon, and investigated their effects on the microwave (3 to 20 GHz) frequency characteristics using a network analyzer. Experiments determined that microwave attenuation by foliage increases as a linear function of frequency per unit weight (gram). As the frequency increases, the spatial resolution increases, but the phase difference (imaginary component) increases. So we solved the dispersion of phase difference by sweeping the frequency and taking the intermediate value. Based on these experimental results, we developed a microwave scanner on 10Ghz to describe foliage moisture as a image and to enable assessments of leaf condition. Photosynthesis is the process whereby plants synthesize oxygen and sugars from carbon dioxide and water, thereby converting light energy into chemical energy. Since water is a major parameter of photosynthesis, the quantity of water accumulated inside a leaf reflects leaf health. The equipment described here and related microwave technologies will help assess the capacity of leaves to absorb atmospheric carbon dioxide.

• Food Science and Preservation
• /
• v.12 no.4
• /
• pp.344-349
• /
• 2005

Microwave-assisted process (MAP) was applied to extract antioxidant-related components from Thymus quinquecostatus var. japonica Hara. Microwave power(2,450 MHz, $0{\sim}160$ W) and extraction time($1{\sim}5\;min$) were used as independent variables($X_i$) for central composite design to yield 10 different extraction conditions. Response surface methodology was applied to predict optimum extraction conditions for dependent variables of extracts, such as total yield, total phenolics, flavonoid, and electron donation ability depending on different powers and extraction times of MAP. Determination coefficients($R^2$) of regression equations for dependent variables were higher than 0.93 excluding that of total phenolics, and microwave power was predicted more influential than extraction time in MAP (p<0.05). The optimal extraction time for each dependent variable was ranged from 3.36 to 4.97 min, but microwave power showed wide ranges depending on variables. The superimposed contour maps for maximized dependent variables illustrated extraction conditions of 64 to 100 W in microwave power and 2.9 to 4.0 min in extraction time.

• Korean Chemical Engineering Research
• /
• v.56 no.5
• /
• pp.773-778
• /
• 2018

In-situ transesterification of microalgae lipids using microwave irradiation has potential to simplify and accelerate biodiesel production, as it minimizes production cost and reaction time by direct transesterification of microalgae into biodiesel with microwave as a heating source. This study was conducted to research the effect of microwave irradiation with in-situ transesterification of microalgae under base catalyst condition. The process variables (reaction time, solvent ratio, microwave power) were studied using 2% of catalyst concentration. The maximum yield of FAME was obtained at about 32.18% at the reaction time of 30 min with biomass-methanol ratio 1:12 (w/v) and microwave power of 450 W. The GC MS analysis obtained that the main component of FAME from microalgal oils (or lipids) was palmitic acid, stearic acid and oleic acid. The results show that microwaves can be used as a heating source to synthesize biodiesel from microalgae in terms of major components resulting.

• Journal of the Korean Vacuum Society
• /
• v.22 no.1
• /
• pp.31-36
• /
• 2013

For the simplification of doping process in amorphous carbon film, arsenic (As) ions were implanted on the nucleated silicon wafer before the growth process. Then amorphous carbon films were grown at the condition of $CH_4/H_2=5%$ by microwave plasma chemical vapour deposition. Because the implanted seeds were grown at the high temperature and the implanted ions were spread, it was possible to reduce the process steps by leaving out the annealing process. When the implanted amorphous carbon films were electrically characterized in diode configuration, field emission current of $0.1mA/cm^2$ was obtained at the applied electric field of about $2.5V/{\mu}m$. The results show that the implanted As ions were sufficiently doped by the self-annealing process by using the growth after implantation.

• Clean Technology
• /
• v.22 no.4
• /
• pp.250-257
• /
• 2016

As an attempt to replacing petroleum-based chemicals with bio-based ones, synthesis of furfural from biomass-derived xylose attracts much attention in recent days. Conventionally, furfural from xylose has been produced via the utilization of highly corrosive, toxic, and environmentally unfriendly mineral acids such as sulfuric acid or hydrochloric acid. In this study, microwave-assisted biphasic reaction process in the presence of novel bio-based heterogeneous acid catalysts was developed for the eco-benign and effective synthesis of furfural from xylose. The microwave was irradiated for reaction acceleration and a biphasic system consisting of $H_2O$ : MIBK (1 : 2) was designed for continuous extraction of furfural into the organic phase in order to reduce the undesired side products formed by decomposition/condensation/oligomerization in the acidic aqueous phase. Moreover, sulfonated amorphous carbonaceous materials were prepared from wood powder, the most abundant lignocellulosic biomass. The prepared catalysts were characterized by FT-IR, XPS, BET, elemental analysis and they were used as bio-based heterogeneous acid catalysts for the dehydration of xylose into furfural more effectively. For further optimization, the effect of temperature, reaction time, water/organic solvent ratio, and substrate/catalyst ratio on the xylose conversion and furfural yield were investigated and 100% conversion of xylose and 74% yield of furfural was achieved within 5 h at $180^{\circ}C$. The bio-based heterogeneous acid catalysts could be used three times without any significant loss of activity. This greener protocol provides highly selective conversion of xylose to furfural as well as facile isolation of product and bio-based heterogeneous acid catalysts can alternate the environmentally-burdened mineral acids.

• Journal of Korean Society of Environmental Engineers
• /
• v.29 no.3
• /
• pp.304-310
• /
• 2007

The purpose of this research was to investigate the effects of the co-treatment of municipal wastewater with microwave-irradiated excess sludge on the treatment efficiency and excess sludge production of the activated sludge process. When 250 mL of excess sludge with a MLSS concentration of approximately 2,000 mg/L was microwave-irradiated at $20^{\circ}C$ for $40\sim300$ sec by a microwave oven (2,450 MHz, 700 W), the temperature of the sludge increased at a rate of approximately $20^{\circ}C/min$ and the SCOD, TKN and T-P concentrations of the sludge showed the highest increase in the irradiation time of $40\sim130$ sec. And, the oxygen uptake rate measurement of the sludge microorganism suggested most of the microorganisms in the sludge were destroyed at an irradiation time above 130 sec(above $65^{\circ}C$). When the municipal wastewater and microwave-irradiated excess sludge was co-treated by the activated sludge process, almost no effect was observed in the pH and alkalinity of both the influent and effluent, but the influent concentrations of SS, COD, T-N and T-P increased. Even though the effluent SS, BOD and T-P concentrations showed almost no effect, the COD and TKN concentrations increased. The microbial yield coefficient decreased at a rate of 0.91 g SS/g COD removed as the irradiation ratio increased at a rate of 1 g SS/g SS-day.

• Clean Technology
• /
• v.21 no.3
• /
• pp.178-183
• /
• 2015

Lead molybdate (PbMoO₄) oxides were successfully synthesized using a conventional hydrothermal method and a microwave-assisted hydrothermal method. They were characterized by XRD, DRS, BET, Raman, SEM and PL. We also investigated the photocatalytic activity of these materials for the decomposition of Rhodamine B under UV-light irradiation. From XRD and Raman results, well-crystallized PbMoO₄ crystals have been successfully synthesized regardless of preparation method and had 42~59 nm particle size. The PbMoO₄ catalysts prepared using microwave-assisted process had the similar particle size and enhanced the photocatalytic activity when compared to that prepared by hydrothermal method. The PbMoO₄ catalysts prepared under the irradiation of microwave for 75 min showed the highest photocatalytic activity. The PL peaks appears at about 530 nm at all catalysts and it was also shown that the excitonic PL signal is proportional to the photocatalytic activity for the decomposition of Rhodamine B.

• Korean Journal of Materials Research
• /
• v.20 no.8
• /
• pp.418-422
• /
• 2010

As a starting material, BCP (biphasic calcium phosphate) nano powder was synthesized by a hydrothermal microwave-assisted process. A highly porous BCP scaffold was fabricated by the sponge replica method using 60 ppi (pore per inch) of polyurethane sponge. The BCP scaffold had interconnected pores ranging from $100\;{\mu}m$ to $1000\;{\mu}m$, which were similar to natural cancellous bone. To realize the antibacterial property, a microwave-assisted nano Ag spot coating process was used. The morphology and distribution of nano Ag particles were different depending on the coating conditions, such as concentration of the $AgNO_3$ solution, microwave irradiation times, etc. With an increased microwave irradiation time, the amount of coated nano Ag particles increased. The surface of the BCP scaffold was totally covered with nano Ag particles homogeneously at 20 seconds of microwave irradiation time when 0.6 g of $AgNO_3$ was used. With an increased amount of $AgNO_3$ and irradiation time, the size of the coated particles increased. Antibacterial activities of the solution extracted from the Ag-coated BCP scaffold were examined against gram-negative (Escherichia coli) and gram-positive bacteria (Staphylococcus aureus). When 0.6 g of $AgNO_3$ was used for coating the Ag-coated scaffold, it showed higher antibacterial activities than that of the Ag-coated scaffold using 0.8 g of $AgNO_3$.