• Title/Summary/Keyword: Micro-focus x-ray

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Phase identification and degree of orientation measurements far fine-grained rock forming minerals using micro-area X-ray diffractometer -$Al_{2}SiO_{5}$ Polymorphs- (미소부 X-선 회절분석기를 이용한 미립조암광물의 상동정 및 배향도 측정 -$Al_{2}SiO_{5}$ 3상다형-)

  • 박찬수;김형식
    • The Journal of the Petrological Society of Korea
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    • v.9 no.4
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    • pp.205-210
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    • 2000
  • Measurements of phase identification and degree of orientation for fine-grained (about 0.3 mm in diameter) minerals in rock samples performed by micro-area X-ray diffractometer.$Al_{2}SiO_{5}$ polymorphs (andalusite, kyanite and sillimanite) were chosen for the measurements and target minerals were existed on thin sections. Micro-area X-ray diffractometer is composed of 3(${\omega}\;{\chi}\;{\phi}$)-circle oscillating goniometer and position sensitive proportional counter (PSPC). $CuK_{\alpha}$ radiation was used as X-ray source and a pin hole ($50\;\mu\textrm{m}$$ in diameter) collimator was selected to focus radiation X-ray onto the target minerals. Phase identification and diffracted X-ray peak indexing were carried out by 3(${\omega}\;{\chi}\;{\phi}$)-circle oscillation measurement. Then, 2(${\omega}\;{\phi}$)-circle oscillation measurement was made for the purpose of searching the prevailing lattice plane of the minerals on thin section surface. Finally, for a selected peak by 2-circle oscillation measurement, X-ray pole figure measurement was executed for the purpose of check the degree of orientation of the single lattice direction and examine its pole distribution. As a result of 3-circle oscillation measurement, it was possible that phase identification among $Al_{2}SiO_{5}$ polymorphs. And from the results of 2-circle oscillation measurement and X-ray pole figure measurement, we recognized that poles of andalusite (122), kyanite (200) and sillimanite (310) lattice plances were well developed with direction normal to each mineral surface plane respectively. Therfore, the measurements used with micro-area X-ray diffractometer in this study will be a useful tool of phase identification and degree of orientation measurement for fine-grained rock forming minerals.

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Analysis of Porosity and Distribution of Pores in Rocks by Micro Focus X-Ray CT (미소 초점 X선 CT를 이용한 암석 내 공극의 분포 및 공극률 분석)

  • Jeong, Gyo-Cheol;Takahashi, Manabu
    • The Journal of Engineering Geology
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    • v.20 no.4
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    • pp.461-465
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    • 2010
  • Weathering and permeability in rocks play a very important role in underground disposal of radioactive waste and their long-term management as well as stability security of rock structures. Weathering and permeability of rocks are largely controlled by the characters of inner structures of rocks. In other words, weathering rate can be accelerated depending on the quantity of pore and microcrack in rocks. Quantitative evaluation of inner structures of rocks can serve as a tool that can assess the degree of weathering of rocks. Therefore it can be said that the understanding of three dimensional distribution of the inner structure of rocks is important for long-term management of rock structures. This study was performed to analyze three dimensional distribution of pore in rocks using Micro Focus X-ray CT on fresh granite and weathered granite from Korea. Results of the analysis clearly show distribution of pore and porosity of the inner rock.

Numerical Analysis on the compressive behavior of closed-cell Al foam (닫힌 셀 구조 Al 발포 재료의 압축 거동에 대한 수치해석)

  • Jeon, In-Su
    • Proceedings of the KSME Conference
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    • 2007.05a
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    • pp.1663-1666
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    • 2007
  • The finite element method is applied to analyze the deformation mechanisms in the closed-cell Al foam under the compression. The modeling of the real cellular structure proceeds with the concept of the reverse engineering. First of all, the small, $10{\times}\;10{\times}\;10mm^3$ sized specimens of the closed-cell Al foam are prepared. The micro focus X-ray CTsystem of SHIMADZU Corp. is used to scan the full structures of the specimens. The scanned structures are converted to the geometric surfaces and solids through the software for 3-D scan data processing, RapidFormTMof INUS Tech. Inc. Then the solid meshes are directly generated on the converted geometric solids for the finite element analysis. The large elastic-plastic deformation and 3-D contact problems for the Al cellular material are considered. The clear and successful analysis for the deformation mechanisms in the closed-cell Al foam is carried out through the comparison of the numerical results in this research with the referred experimental ones.

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Numerical analysis of fracture mechanisms for porous calcium phosphate (다공성 칼슘포스파이트에 대한 파괴분석)

  • Park, Jin-Hong;Bae, Ji-Yong;Shin, Jae-Bum;Jeon, In-Su
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1301-1302
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    • 2008
  • In this study, the fracture strength for fracture mechanism porous calcium phosphate made from sintered with ${\beta}$-tricalcium phosphate obtained by wet precipitation procedure is analyzed using finite element method and experiment measurement. First, three $3{\times}3{\times}3mm^3$ and $5{\times}5{\times}5mm^3$ specimens are prepared and tomographic images of one $5{\times}5{\times}5mm^3$ specimen are obtained by micro focus X-ray CT. The compression tests using the specimens are carried out to measure the elastic modulus and fracture strength to analyze the fracture mechanism of porous calcium phosphate specimen. The tomographic images are reconstructed by 3D reconstruction program. The finite elements are directly built up in the reconstructed specimen. The numerical simulation for the compression tests is performed using the element. The mechanism of calcium phosphate of simulation are obtained by the compression tests using there cylindric specimen of height 19.5 mm and diameter 10 mm. From the results, the applicability of porous calcium phosphate is evaluated to care fracture and vacant bone of a patient as the reinforcement material.

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A Study on the Non-destructive Inspection for End Closure Welding of Nuclear Fuel Elements for the Irradiation Test (조사시험용 핵연료봉 용접부 비파괴검사에 관한 연구)

  • 김웅기;김수성;이철용;이도연;이정원
    • Proceedings of the KWS Conference
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    • 2004.05a
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    • pp.302-304
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    • 2004
  • Nuclear fuel elements containing dry recycling nuclear fuel pellets for the irradiation test in a reactor were remotely fabricated from spent PWR fuel materials in a hot cell. End closure welding as well as seal tube welding for thermal sensor of the elements was performed by Nd:YAG laser. The soundness of the end closure welds and seal tube welds for the elements were evaluated by a precise X-ray inspection system composed of a micro-focus X-ray generator with an image intensifier and a real time camera system. Then, helium leak test was performed for the elements. The soundness of the welds of the fuel elements was confirmed by the X-ray inspection and helium leak test. The irradiation test for the fuel elements were successfully completed at the HANARO research reactor.

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Quantitative Evaluation of Concrete Damage by X-ray CT Methods (마이크로 포커스 X-ray CT를 이용한 콘크리트 손상균열의 정량적 평가)

  • Jung, Jahe
    • The Journal of Engineering Geology
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    • v.28 no.3
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    • pp.455-463
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    • 2018
  • This study developed a method to quantitatively measure the size of cracks in concrete using X-ray CT images. We prepared samples with a diameter of 50 mm and a length of 100 mm by coring cracked concrete block that was obtained by chipping. We used a micro-focus X-ray CT, then applied the 3DMA method (3 Dimensional Medial axis Analysis) to the 3D CT images to find effective parameters for damage assessment. Finally, we quantitatively assessed the damage based on sample locations, using the damage assessment parameter. Results clearly show that the area near the chipping surface was damaged to a depth of 3 cm. Furthermore, X-ray methods can be used to evaluate the porosity index, burn number, and medial axis, which are used to estimate the damage to the area near the chipping surface.

Laser Welding of Seal Tube for Instrumented Irradiation Fuel Test (계장핵연료 조사시험용 실튜브 레이저용접기술)

  • Kim Soo-Sung;Lee Chul-Yong;Kim Woong-Ki;Park Geun-Il;Koh Jinh-Yun;Seo Jun-Seok
    • Journal of Welding and Joining
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    • v.23 no.6
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    • pp.43-48
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    • 2005
  • This work was carried out to obtain sound welds and to select a most suitable binary metal joint among three different dissimilar binary metal combinations such as Zr-4/Ta, Mo/Ta and Ti/Ta(seal tube/sensor sheath) joints fur the instrumented nuclear fuel irradiation test. To do this, Taguchi experimental method was employed to optimize the experimental data. In addition, metallography, micro-focus x-ray radiography and hardness test were conducted to examine the welds. From the weld bead appearance, penetration depth and bead width as well as weld defects standpoint, Zr-4/Ta joint is suggested for the circumferential joining between a seal tube and a sensor sheath. The optimized welding parameters based on Zr-4/Ta joint are suggested as well.

Experimental Study on Deformation and Failure Behavior of Limestones under Dynamic Loadings (동적하중 하에서 석회암의 변형 및 파괴거동에 관한 실험적 연구)

  • Kang, Myoung-Soo;Kang, Hyeong-Min;Kim, Seung-Kon;Cheon, Dae-Sung;Kaneko, Katsuhiko;Cho, Sang-Ho
    • Tunnel and Underground Space
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    • v.22 no.5
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    • pp.339-345
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    • 2012
  • Information on the deformation behavior and fracture strength of rocks subjected to dynamic loadings is important to stability analyses of underground openings underground vibration due to rock blasts, earthquakes and rock bursts. In this study, Split Hopkinson Pressure Bar (SHPB) system was applied to estimate dynamic compressive and tensile fracture strengths of limestone and also examine deformation behavior of limestones under dynamic loadings. A micro-focus X-ray CT scanner was used to observe non-destructively inside the impacted limestone specimens. From the dynamic tests, it was revealed that the limestone have over 140MPa dynamic compressive strength and the strain-rate dependency of the strength. Dynamic Brazilian tensile strength of the limestone exceeds 21MPa and shows over 3 times static Brazilian tensile strength.

A X-ray Tube Using Field Emitter Made by Multi-walled Carbon Nanotube Yarns

  • Kim, Hyun-Suk;Castro, Edward Joseph D.;Kwak, Seung-Im;Ju, Jin-Young;Hwang, Yong-Gyoo;Lee, Choong-Hun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.392-392
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    • 2011
  • Carbon nanotubes (CNT) emitter has widely become an attractive mechanism that draws growing interests for cold cathode field emission.$^{1,2}$ CNT yarns have demonstrated its potential as excellent field emitters.$^3$ Extensive simulations were carried out in designing a CNT yarn-based cathode assembly. The focal spot size dependence on the anode surface of the geometric parameters such as axial distance of the electrostatic focus lens from the cathode and the applied bias voltages at the cathode, grid mesh and electrostatic focus lens were studied. The detailed computer simulations using Opera 3D electromagnetic software$^4$ had revealed that a remarkable size of focal spot under a focusing lens triode type set-up design was achieved. The result of this optimization simulation would then be applied for the construction of the CNT yarn based micro-focus x-ray tube with its field emission characteristics evaluated.

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