• Title/Summary/Keyword: Micro Filler

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The Leakage Reduction of Natural Inorganic Powder Compound Applying Subsurface Structural Weak Part (지하구조물 취약부에 적용한 천연 무기질계 분말형 혼화제의 누수저감효과)

  • Yoon, Sung-Hwan;Seo, Hyun-Jae;Lee, Hye-Ryung;Park, Jin-Sang;Oh, Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2011.05a
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    • pp.19-22
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    • 2011
  • For underground structures that are exposed to environmental conditions, the declination of the durability of concrete occurs easily because of leakages from high hydraulic pressure and the frequent contact of water due to environmental factors. Therefore this study is to confirm that the leakage reduction of natural inorgnic powder compound applying subsurface structural weak part and make the performance improvement of concrete as an objective. The test was done by making the rebar, flat tie, nail and film infiltration and each of its water tank and cylindrical test body then after pouring water to each of the test body, the test observe the change of the water tank surface absorbed condition and leakage of each specimen with respect to time. As a conclusion, the test was observed that this water proofing admixture has better watertightness from the beginning of the setting time(when it hardens), the ettringite and the thaumasite generates a large quantity of hydration products that controls the formation in a large opening and the CSH produced by pozzolan reaction makes a dent at this opening.

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Characterization of Mechanical Properties in the Heat Affected Zones of Alloy 82/182 Dissimilar Metal Weld Joint (Alloy 82/182 이종금속 용접부 열영향부의 계계적물성치 파악)

  • Kim, Jin-Weon;Kim, Jong-Sung;Lee, Kyoung-Soo
    • Journal of the Korean Society of Safety
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    • v.23 no.6
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    • pp.28-33
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    • 2008
  • This paper presents the characteristics of mechanical properties within the heat affected zones(HAZs) of dissimilar metal weld joint between SA508 Gr.1a and F3l6 stainless steel(SS) with Alloy 82/182 filler metal. Tensile tests were performed using small-size specimens taken from the heat affected regions close to both fusion lines of weld, and the micro-structures were examined using optical microscope(OM) and transmission microscope(TEM). The results showed that significant gradients of the yield stress(YS), ultimate tensile stress(UTS), and elongations were observed within the HAZ of SA508 Gr.1a. This was attributed to the different microstructures within the HAZ developed during the welding process. In the HAZ of F316 SS, however, the welding effect dominated the YS and elongation rather than UTS. TEM micrographs demonstrated these characteristics of the HAZ of F316 SS was associated with a dislocation-induced strain hardening.

Mechanical and microstructural study of rice husk ash geopolymer paste with ultrafine slag

  • Parveen, Parveen;Jindal, Bharat Bhushan;Junaid, M. Talha;Saloni, Saloni
    • Advances in concrete construction
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    • v.8 no.3
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    • pp.217-223
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    • 2019
  • This paper presents the mechanical and microstructural properties of the geopolymer paste which was developed by utilizing the industrial by-products, rice husk ash (RHA) and ultra-fine slag. Ultra-fine slag particles with average particle size in the range of 4 to 5 microns. RHA is partially replaced with ultra-fine slag at different levels of 0 to 50%. Sodium silicate to sodium hydroxide ratio of 1.0 and alkaline liquid to binder (AL/B) ratio of 0.60 is taken. Setting time, compressive, flexural strengths were studied up to the age of 90 days with different concentrations of NaOH. The microstructure of the hybrid geopolymer paste was studied by performing the SEM, EDS, and XRD on the broken samples. RHA based geopolymer paste blended with ultrafine slag resulted in high compressive and flexural strengths and increased setting times of the paste. Strength increased with the increase in NaOH concentration at all ages. The ultra-small particles of the slag acted as a micro-filler into the paste and enhanced the properties by improving the CASH, NASH, and CSH. The maximum compressive strength of 70MPa was achieved at 30% slag content with 16M NaOH. The results of XRD, SEM, and EDS at 30% replacement of RHA with ultra-fine slag densified the paste microstructure.

Analytical Techniques for Measurement of Crosslink Densities of Rubber Vulcanizates

  • Son, Chae Eun;Choi, Sung-Seen
    • Elastomers and Composites
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    • v.54 no.3
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    • pp.209-219
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    • 2019
  • It is important to analyze crosslink densities of rubber articles because the physical properties are dependent on the crosslink densities. In this paper, analytical techniques for the measurement of crosslink densities of rubber vulcanizates are described. The most widely used method to measure the crosslink density is a swelling method combined with the Flory-Rehner equation. Application of the interaction parameter (${\chi}$) of rubber and swelling solvent is critical because the crosslink density is absolutely dependent on the ${\chi}$ value. Methods for obtaining ${\chi}$ employ not only solubility parameters of the polymer and swelling solvent but also inverse gas chromatography (IGC). The solubilities of rubbers can be obtained using micro differential scanning calorimetry (${\mu}DSC$), intrinsic viscosity measurement, and UV-visible spectroscopy. Nuclear magnetic resonance (NMR) spectroscopy has been also used for the measurement of the crosslink density using the $T_2$ relaxation time, which is determined by spin-spin relaxation in solid-state NMR. For sulfur-cured rubber vulcanizates, crosslink densities according to the crosslink types of mono-, di-, and polysulfides are measured by treating the rubber samples with a chemical probe composed of thiol and amine compounds. Measurement methods of physical crosslinking by filler, crystallization, and ionic bonding have also been introduced.

Effect of steel fibres and nano silica on fracture properties of medium strength concrete

  • Murthy, A. Ramachandra;Ganesh, P.
    • Advances in concrete construction
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    • v.7 no.3
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    • pp.143-150
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    • 2019
  • This study presents the fracture properties of nano modified medium strength concrete (MSC). The nano particle used in this study is nano silica which replaces cement about 1 and 2% by weight, and the micro steel fibers are added about 0.4% volume of concrete. In addition to fracture properties, mechanical properties, namely, compressive strength, split tensile strength, and flexural strength of nano modified MSC are studied. To ensure the durability of the MSC, durability studies such as rapid chloride penetration test, sorptivity test, and water absorption test have been carried out for the nano modified MSC. From the study, it is observed that significant performance improvement in nano modified MSC in terms of strength and durability which could be attributed due to the addition pozzolanic reaction and the filler effect of nano silica. The incorporation of nano silica increases the fracture energy about 30% for mix without nano silica. Also, size independent fracture energy is arrived using two popular methods, namely, RILEM work of fracture method with $P-{\delta}$ tail correction and boundary effect method. Both the methods resulted in nearly the same size-independent $G_F$ irrespective of the notch to depth ratio of the same specimen. This shows evidence that either of the two procedures could be used in practice for analysis of cracked concrete structures.

Experimental and numerical study on the mechanical properties of reinforced polyester composites

  • Ibrahim Alameri;Meral Oltulu
    • Advances in materials Research
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    • v.12 no.3
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    • pp.227-242
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    • 2023
  • Polyester composites play a vital role in civil engineering applications, especially in bridge and car park structures. Therefore, the addition of waste silica-based fillers will both improve the mechanical and durability performance of composites and produce an environmentally friendly material. In this study, the mechanical performance of polyester composites was investigated experimentally and numerically by adding micro and nano-sized silica-based fillers, marble powder, silica fume and nano-silica. 24 cubes for the compression test and 18 prisms for the flexural test were produced in six different groups containing 30% marble powder, 5% silica fume and 1% nano-silica by weight. SEM/EDS testing was used to investigate the distribution of filler particles in the matrix. Experimentally collected results were used to validate tests in the Abaqus software. Additionally, the Extended Finite Element Method (XFEM) was used to estimate the fracture process for the flexural test. The results show that the added silica fume, marble powder and nano silica improves the compressive strength of polyester composites by 32-38% and the flexural tensile strength by 10-60% compared to pure polyester composite. The numerically obtained results matched well with the experimental data, demonstrating the accuracy and feasibility of the calibrated finite element model.

Effects of Polishing Methods on the Surface Characteristics of Composite Resins (연마방법에 따른 복합레진의 표면특성 평가)

  • Baik, Min-Kyung;Kim, Chong-Chul;Jang, Ki-Taeg
    • Journal of the korean academy of Pediatric Dentistry
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    • v.43 no.3
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    • pp.275-283
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    • 2016
  • The aim of this study was to evaluate the surface characteristics of composite resins polished with two different polishing methods. 30 disk-shaped specimens were prepared with microhybrid (Filtek$^{TM}$ Z250) and nanofilled (Filtek$^{TM}$ Z350) resins respectively, and classified into three groups: not polished as controls, polished by an abrasive disk (Soflex), and polished by a polishing brush (Occlubrush). Surface roughness was increased after polishing. In terms of micro-roughness, there were no significant differences between the two polishing methods. But macro-roughness values were markedly increased in the Occlubrush group (p < 0.05). In the Sof-lex group, the matrix and fillers were polished together, resulting into a smoother and homogeneous surface. However, in the Occlubrush group, the matrix layer was torn off, with more heterogeneous surfaces and large scratches. In regards to micro-hardness, no significant differences were observed between the two polishing systems (p > 0.05). And the hardness value increased about 25% after polishing. In conclusion, the method of polishing should be chosen deliberately in view of the hardness characteristics of composite resins. Sof-lex is recommended to improve the surface characteristics of polished resins.

The effect of adhesive thickness on microtensile bond strength to the cavity wall (와동벽에서 접착제의 두께가 미세인장 결합강도에 미치는 영향)

  • Lee, Hwa-Eon;Kim, Hyeon-Cheol;Hur, Bock;Park, Jeong-Kil
    • Restorative Dentistry and Endodontics
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    • v.32 no.1
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    • pp.9-18
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    • 2007
  • The purposes of this study were to examine the variability of adhesive thickness on the different site of the cavity wall when used total-etch system without filler and simplified self-etch system with filler and to evaluate the relationship between variable adhesive thickness and microtensile bond strength to the cavity wall. A class I cavity in six human molars was prepared to expose all dentinal walls. Three teeth were bonded with a filled adhesive, $Clearfil^{TM}$ SE bond ana the other three teeth were bonded with unfilled adhesives, $Scotchbond^{TM}$ Multi Purpose. Morphology and thickness of adhesive layer were examined using fluorescence microscope. Bonding agent thickness was measured at three points along the axial cavity wall edge of cavity margin (rim). halfway down each cavity wall (h1f), internal angle of the cavity (ang). After reproducing the adhesive thickness at rim, h1f and ang, micro-tensile bond strength were evaluated. For both bonding agents, adhesive thickness of ang was significantly thicker than that of rim and h1f (P <0.05). As reproduced the adhesive thickness, microtensile bond strength was increased as adhesive thickness was increased in two bonding agents. Adhesive thickness of internal angle of the cavity was significantly thicker than that of the cavity margin and the halfway cavity wall for both bonding agents. Microtensile bond strength of the thick adhesive layer at the internal angle of the cavity was higher than that of the thin adhesive layer at 1,he cavity margin and the halfway cavity in the two bonding systems.

The Compressive Strength and Durability Properties of Polypropylene Fiber Reinforced EVA Concrete (폴리프로필렌 섬유 보강 EVA 콘크리트의 압축강도 및 내구성)

  • Nam, Ki Sung;Sung, Chan Yong
    • Journal of The Korean Society of Agricultural Engineers
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    • v.57 no.4
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    • pp.11-19
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    • 2015
  • The important properties of EVA (ethylene vinyl acetate) redispersible polymer was waterproof, densification of internal pore space of concrete and ball bearing and micro filler. Also, the significant role of polypropylene(PP) fiber was crack control and blockade of movement for deterioration factors. The most studies for EVA were limited in the field of mortar and PP fiber reinforced concrete had been studied in the state of being restricted unit water content, rich mix and mixing much of the fiber without considering construction site. Therefore, the control mix design were applied in ready mixed concrete using 10 % fly ash of total cement weight used in batch plant. On the basis of control mix design, EVA contents ranging from 0 % to 10 % of total cement weight and PP fiber contents ranging from 0 % to 0.5 % of EVA concrete volume were used in the mix designs. The results showed the maximum compressive strength value was measured at EVA 5.0 % and PP fiber 0.1 %, the minimum water absorption ratio was at EVA 10 % and PP fiber 0 %, the durability factor for freezing and thawing resistance was at EVA 5.0 % and PP fiber 0.3 % and the minimum weight reduction ratio of resistance to sulfuric acid attack was at EVA 10 % and PP fiber 0.5 % after curing age 42days. Meanwhile, From these results, PP fiber reinforced EVA concrete would be very benefit, if each optimal mix types were used in hydraulic structures, underground utilities and agricultural structures.

Experimental Improvement of the Dropping Test for Evaluating the Appropriate Level of Water Content Ratio in Rammed Earth Method (흙다짐 건축재료의 적정함수비 현장확인을 위한 낙하시험 방법의 실험적 개선)

  • Lee, Jong-Kook
    • Journal of the Korea Institute of Building Construction
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    • v.15 no.1
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    • pp.35-42
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    • 2015
  • Although the interest for earth architecture has been expanded and settled as a part of modern architecture, precisely calculating the ratio of water content in practice is still difficult and the calculation is based on empirical analysis yet. This causes many problems in durability and maintenance of earthen architecture. Therefore, this study investigated to find the easiest way to correctly calculate the appropriate level of water content ratio (AWCR), which can be used in practice. Until now, the workers have checked the AWCR based on their own experience with popular but vague manuals. On this awareness, we studied the several testing methods and found the dropping test which uses the pattern of shape after the sample is dropped. In this point, we studied and developed the definite testing method in terms of process, and shape discrimination. Also we suggest the test recording sheet by using the cobalt chloride($CoCl_2$) whose color is instantly changed when contacts with the moisture. It is believed that this result can help improving the quality and durability of the earthen architecture using the rammed earth method and the efficiency in practice.