• Journal of Welding and Joining
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• 제19권5호
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• pp.534-539
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• 2001

The formation mechanism of microconstituents in brazed joints of duplex stainless steel and Cr-Cu alloy which is an essential process of rocket engine manufacturing was investigated using Cu base insert metal. $SUS329J_3L$ and C18200 were used for base metal and AMS 4764 was used for insert metal. The brazing was carried out under various conditions. There were various phases in the joints, because of reaction between liquid insert metal and base metals. Since liquid insert metal reacts with duplex stainless steel, liquid Cu from insert metal infiltrated into the $\alpha/\beta$ interface of duplex stainless steel. Through the process of Cu infiltration, isolated stainless steel pieces come into the liquid insert metal. Since liquid insert metal reacts with Cr-Cu alloy. Cr precipitates from C18200 come into the liquid insert metal. With increment of bonding temperature and holding time, amounts and sizes of phases increased. but Cr-Mn compounds decreased at 1303k for 1.2ks and Mn-rich phases disappeared Fe-Cr compounds formed.

• 한국재료학회지
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• 제17권11호
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• pp.574-579
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• 2007

Amorphous $BaTi_4O_9$ ($BT_4$) film was deposited on Pt/Si substrate by RF magnetron sputter and their dielectric properties and electrical properties are investigated. A cross sectional SEM image and AFM image of the surface of the amorphous $BT_4$ film deposited at room temperature showed the film was grown well on the substrate. The amorphous $BT_4$ film had a large dielectric constant of 32, which is similar to that of the crystalline $BT_4$ film. The leakage current density of the $BT_4$ film was low and a Poole-Frenkel emission was suggested as the leakage current mechanism. A positive quadratic voltage coefficient of capacitance (VCC) was obtained for the $BT_4$ film with a thickness of <70 nm and it could be due to the free carrier relaxation. However, a negative quadratic VCC was obtained for the films with a thickness ${\geq}96nm$, possibly due to the dipolar relaxation. The 55 nm-thick $BT_4$ film had a high capacitance density of $5.1fF/{\mu}m^2$ with a low leakage current density of $11.6nA/cm^2$ at 2 V. Its quadratic and linear VCCs were $244ppm/V^2$ and -52 ppm/V, respectively, with a low temperature coefficient of capacitance of $961ppm/^{\circ}C$ at 100 kHz. These results confirmed the potential suitability of the amorphous $BT_4$ film for use as a high performance metal-insulator-metal (MIM) capacitor.

• 한국산학기술학회논문지
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• 제16권2호
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• pp.1579-1584
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• 2015

광촉매반응에서 티타니아에 금속물질을 담지하면 광촉매표면이 변화되며 담지된 금속물질은 반응속도를 증가시킨다. 회분식 광반응기를 이용하여 $TiO_2$ 광촉매에 대한 금속물질 담지와 담지된 촉매의 소성조건 영향을 조사하였다. 광분해 효율을 증진시키기 위해 $TiO_2$ 촉매에 여러 종류의 금속물질을 담지하였다. 모든 실험에서의 수분함량은 3wt%, 반응기 온도는 $40^{\circ}C$이었다. $TiO_2$에 팔라듐을 담지한 경우가 가장 우수하였으며, Pt와 W을 첨가한 경우도 양호하였다. Pd/$TiO_2$ 촉매에 백금 또는 텅스텐을 부가적으로 담지하여도 제거효율에서의 증가는 없었다. 적절한 소성조건을 얻기위해 소성온도와 소성시간에 대하여 다양하게 실험을 수행하였으며, 실험결과 최적의 소성조건은 소성온도 $400^{\circ}C$, 소성시간 1시간이었다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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• pp.289.1-289.1
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• 2016

Germanium (Ge) with higher carrier mobility and a lower crystallization temperature has been considered as the channel material of thin-film transistors for display applications. Various methods were studied for crystallizaion of poly-Ge from amorphous Ge at low temperature. Especially Metal induced crystalliazation (MIC) process was widely studied because low process cost. In this paper, we investigate copper diffusion process of different thick (70 nm, 350 nm) poly-Ge film obtained by MIC process at various temperatures (250, 300, and $350^{\circ}C$) through atomic force microscopy (AFM), Raman spectroscopy, and secondary ion mass spectroscopy (SIMS) measurement. Crystallization completeness and grain size was similar in all the conditions. Copper diffusion profile of 370 nm poly-Ge film show simirly results regardless of process temperature. However, copper diffusion profile of 70 nm poly-Ge film show different results by process temperature.

• 소성∙가공
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• 제18권2호
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• pp.166-171
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• 2009

In this paper, a basic study on micro cutting process with SM20C at low temperature environment was performed. In macro cutting fields, the cryogenic cutting process has been applied to cut the refractory metal but, the serious problem may be generated in micro cutting fields by the cryogenic environment. However, if the proper low temperature is applied to micro cutting area, the cooling effect of cutting heat is expected. Such effect can make the reduction of tool wear and burr formation. For verifying this possibility, the micro cutting experiment at low temperature was performed and SEM images were analyzed.

• 한국전기전자재료학회논문지
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• 제31권2호
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• pp.98-101
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• 2018

In this paper, we discuss the fabrication of metal alloy resistors. We connected them in parallel to estimate their resistance and temperature coefficient of resistance (TCR). The fabricated resistors have different resistances, 5 and $10{\Omega}$ and different TCRs, 50 and $200ppm/^{\circ}C$. Each resistor was confirmed to have the correct atomic composition through the use of energy dispersive X-ray (EDX). The resistors' electrical properties were confirmed by measuring resistance and TCR. The resistance and TCR of the resistors connected in parallel were estimated through the increase in resistance due to the increase in temperature, and were compared with the measured values. We are confident that this TCR estimation technique, which uses the increase in resistance due to temperature, will be very useful in designing and fabricating resistors with low and stable TCR.

• Journal of Welding and Joining
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• 제19권6호
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• pp.614-621
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• 2001

A study was carried out to determine the solidification cracking susceptibility of Ni-base superalloy as a function of Fe content in base metal. Three kinds of Ni-base superalloys with three different levels of Fe content were used. The solidification cracking susceptibility was evaluated by the Trans-Varestraint test at four different strain levels. Quantitative analysis of crack revealed that the solidification crack length and the temperature range in which hot cracking occurred in fusion zone (Brittle Temperature Range, BTR) decreased with a decrease in Fe content. Further, the thermo-calc data indicated that the solidification temperature range also decreased with decreasing Fe content. From these results, it was deduced that the improvement of the solidification cracking susceptibility with decreasing Fe content was attributed to the decrease of the solidification temperature range.

• 한국표면공학회지
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• 제51권6호
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• pp.400-404
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• 2018

A metal 3D printer has been developed on its own to electrodeposit the localized area. Nozzles were used to selectively laminate the electrolytic plating method. To analyze the factors affecting the deposition, the stack height, thickness and surface roughness were experimentally analyzed according to the current density and the temperature of the electrolyte. Electrolytic temperature and current are electrodeposited when the deposition conditions are dominant over the etching conditions, but the thickness is kept constant. On the contrary, when the etching conditions are dominant, the electrodeposited shape is rather the etched. As a result, the uniformity of surface quality and electrodeposition rate could be improved by conducting experiments under constant conditions of electrolyte temperature and current density.

• Tribology and Lubricants
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• 제34권5호
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• pp.183-190
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• 2018

Tilting pad journal bearing is widely used for steam turbines because of its excellent dynamic stability. As the turbine capacity increases, power loss in the bearings becomes a matter of concern. Power loss in tilting pad journal bearings can be reduced by increasing the bearing clearance and reducing the pad arc length. In this study, the tilting pad journal bearing is tested by changing the seal tooth clearance to verify the static characteristics of the bearing. Bearing power loss and bearing metal temperature are evaluated to compare the bearing's performance and reliability for several test cases. The test bearing is a tilting pad journal bearing with 300.62mm inner diameter and 120.00mm active length. The bearing power loss, its metal temperature, and oil film thickness are measured and evaluated based on the rotor's rotational speed, oil flow rate, and bearing load. Test results show that a tilting pad journal bearing with large seal tooth clearance has 40% lower power loss compared with a bearing with a small seal tooth clearance. As the seal tooth clearance is increased, the power loss of the tilting pad journal bearing decreases. However, with respect to the bearing metal temperatures, a detuning point is observed that makes the minimum bearing metal temperature. Moreover, as the seal tooth clearance is increased, the oil film thickness increases due to high viscosity.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 2001년도 The 6th International Symposium of East Asian Resources Recycling Technology
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• pp.106-110
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• 2001

Formation of stoichiometric lithium-, nickel-, and zinc- ferrites by calcining organo-metallic precursors a temperature below 40$0^{\circ}C$ is examined using DTA/TG, and XRD techniques. It attempts to simulate th immobilization of metal ions in industrial liquid influents (waste) through the synthesis of stoichiometric spinel ferrites (SSF). Two steps of the SSF formation during thermal treatments are noted. The transformation of magnetite to ${\gamma}$ - Fe$_2$O$_3$and subsequent first formation of SSF were observed at temperatures ranging from 200 to 45$0^{\circ}C$. Th formation of cation-containing ${\gamma}$-Fe$_2$O$_3$and subsequent second formation of the ferrite occurred at temperature ranges of < 45$0^{\circ}C$ and 500 to $650^{\circ}C$, depending on the heating rate used. Then the temperature range of 200t 45$0^{\circ}C$ is critical to the performance of the technique, because a calcination at the range would lead to a complete formation of SSF, avoiding the occurrences of ${\gamma}$-Fe$_2$O$_3$and ion-containing ${\gamma}$-Fe$_2$O$_3$. If not, so $\alpha$-Fe$_2$O$_3$would occur. And annealing at temperature above $650^{\circ}C$ must be employed by which solid-state reactio of $\alpha$-Fe$_2$O$_3$with metal ions (possibly metal oxides) to form SSF can be conducted.