• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 추계학술대회 논문집
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• pp.555-559
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• 2005

Spinning process is a chipless metal forming method for axis-symmetric parts, which is more economical, efficient and versatile method for producing parts than other sheet metal forming process such as stamping or deep drawing. The large-sized spindle for spinning machine is the equipment to ferm a high-pressure vessel into the demanded shape. The important problem in the spindle system fur spinning machines is to reduce and minimize the thermal effect by motor and bearings. In this study, the effect of heat generation of bearings for the large-sized spindle is considered. Temperature distribution and thermal displacement of the spindle system for spinning machine can be analyzed by using the finite element method. The numerical results are compared with the measured data. The results show that temperature distribution and thermal displacement can be reasonably estimated by using the finite element method and the three dimensional model.

• Nuclear Engineering and Technology
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• 제53권4호
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• pp.1218-1223
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• 2021

A hydrophobic ionic liquid including an amino moiety ([DiOcAPmim][NTf₂]) was synthesized. Its extraction behaviors towards Pd(II), Ru(III), Rh(III) were investigated in nitric acid aqueous solution as a function of contact time, effect of concentration of nitric acid, effect of temperature, and effect of co-existing metal ions. The extraction kinetics of Pd(II) was fairly fast and extraction equilibrium can be attained within only 5 min under the [HNO₃] = 2.05 M. When [HNO₃]< 1 M, the extraction percentage of Pd(II), Ru(III), Rh(III) were all above 80%. When [HNO₃] reached 2 M, all of the extraction percentage decreased and in an order of Pd(II)>Ru(III)>Rh(III). When [HNO₃]> 2 M, the extraction performance gradually recovered. The effect of temperature can slightly affect the extraction performance of Pd(II). Furthermore, in simulated high-level liquid waste, [DiOcAPmim][NTf₂] showed a better preference towards Pd(II) under the interference of various other co-existing metal ions.

• 한국분말재료학회지
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• 제28권4호
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• pp.342-351
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• 2021

Because of its unique properties, tungsten is a strategic and rare metal used in various industrial applications. However, the world's annual production of tungsten is only 84000 t. Ammonium paratungstate (APT), which is used as the main intermediate in industrial tungsten production, is usually obtained from tungsten concentrates of wolframite and scheelite by hydrometallurgical treatment. Intermediates such as tungsten trioxide, tungsten blue oxide, tungstic acid, and ammonium metatungstate can be derived from APT by thermal decomposition or chemical attack. Tungsten metal powder is produced through the hydrogen reduction of high-purity tungsten oxides, and tungsten carbide powder is produced by the reaction of tungsten powder and carbon black powder at 1300-1700℃ in a hydrogen atmosphere. Tungsten scrap can be divided into hard and soft scrap based on shape (bulk or powder). It can also be divided into new scrap generated during the production of tungsten-bearing goods and old scrap collected at the end of life. Recycling technologies for tungsten can be divided into four main groups: direct, chemical, and semi-direct recycling, and melting metallurgy. In this review, the current status of tungsten smelting and recycling technologies is discussed.

• 한국기계가공학회지
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• 제21권5호
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• pp.1-8
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• 2022

Fused deposition modeling (FDM), based on stacking a continuous filament of polymer or composite materials, is well matured and is thus widely used in additive manufacturing technology. To advance FDM-based 3D printing technology, the mechanical properties of additively manufactured composite materials must be improved. In this study, we proposed a novel FDM 3D printing process using metal wire-polymer composites, enabling enhanced mechanical properties. In addition, we developed a new type FDM filament of copper wire wrapped in nylon material for stable 3D printing without thermal damage during the printing process. After FDM printing of the copper wire-nylon composite filament, we conducted a tensile test to investigate the mechanical behavior of the printed composite materials. The experimental results confirmed that the tensile strength of the 3D-printed metal wire-polymer composites was higher than that of the conventional single polymer material. Thus, we expect that the FDM printing process developed in this study may be promising for high-load-bearing applications.

• Acta Via Serica
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• 제9권1호
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• pp.91-138
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• 2024

This survey explores artifacts like steles, metal or stone statues, metal foils, and coins, bearing inscriptions in the Sanskrit language and Siddhamātṛkā (or "Siddham"), Nāgarī, and Proto-Bengali/Gauḍī scripts produced in Java between the 8th and 13th century CE, contextualizing them against the background of the pan-Asian networks of Tantric Buddhism or Mahāyāna Buddhist Tantra and especially its circulation along the maritime "Silk Routes." Discussing the interrelationship between languages, scripts, religions, and politics in Java and relevant regions of the wider Buddhist world, it tries to answer questions concerning foreign or local agency and audience as well as transregional connectivity. In particular, it argues that the quick spread of varieties of Mahāyāna/Mantrayāna Buddhism from the Subcontinent to Java and East Asia during a "first wave" from the 8th to the 9th century appears to have occurred in parallel with the diffusion of Siddhamātṛkā script in those locales, whereas a "second wave" of Tantric Buddhism linking the Indo-Tibetan and East Asian Buddhist world is associated with Nāgarī and Proto-Bengali/Gauḍī script in East Java.

• 한국토양환경학회지
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• 제3권2호
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• pp.41-51
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• 1998

충남 금산의 대성폐탄광 주변 토양 및 식생에 대한 중금속의 오염도를 파악하기 위해, 탄질물을 함유하는 오염지역과 그렇지 않은 비오염지지역으로 구분하여 양 지역에서 토양과 식물체(참억새와 리기 다소나무에 대해 Co, Cr, Fe, Ni, Mo, Sc및 Zn등 7개 중금속의 농도를 조사하였다. 토양내 중금속 농도는 Cr, Mo, Ni, Fe의 경우 탄질물을 많이 함유하는 오염지역에서 높았으며, Co, Sc, Zn은 비오염지역의 토양에 더 많이 함유되어 있었다 오염지에서 생육하는 참억새 및 리기다소나무의 Co, Cr, Sc, Fe농도는 지상부 보다 뿌리내의 농도가 더 높았으며, 비오염지에서 Ni및 Mo은 반대의 경향을 나타내었다. 참억새의 경우 지상부는 Cr을 제외한 Co, Mo, Ni, Sc, Zn, Fe원소 모두 비오염지에서 농도가 높았고, 뿌리는 Zn을 제외한 모든 원소가 오염지에서 높게 나타났다. 리기다소나무의 경우에 지상부는 Cr과 Fe만 비오염지에서 높았고, 뿌리는 모든 원소가 오염지에서 높았다. 오염지 및 비오염지의 식생내 중금속 농도는 Zn을 제외하고 전원소가 토양의 농도 보다 낮았다. 토양과 식물체내 중금속 농도의 원소별 변화는 리기다소나무 보다 참억새가 토양의 함량치에 가까웠으며, 탄질물을 많이 함유한지역일수록 참억새 보다 리기다소나무의 중금속 흡수가 더 높았다.

• 한국지반환경공학회 논문집
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• 제11권12호
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• pp.47-56
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• 2010

국가 차원 사회 간접자본 투자증가로 도로 개설 및 확장 등으로 인해 도로 절개비탈면의 증가가 필연적 현상으로 나타나고 있다. 도로 절개 비탈면이 증가됨에 따라 매년 많은 인명피해와 재산 피해가 발생되고 있으며 국내에서는 이러한 낙석 및 산사태로 인한 피해를 저감하고자 하는 취지에서 많은 연구가 수행되고 있다. 일반적으로 국내 도로사면의 대부분은 국토해양부에서 발간한 "도로안전시설 설치 및 관리지침"에 근거한 표준낙석방지시설을 사용하고 있으나 이러한 낙석방지시설이 실제 낙석 발생 시 큰 파손 없이 낙석을 방어할 수 있는 지에 대해서 많은 의문점들이 제기되고 있다. 또한 기술수준이 미약하여 전체적으로 해외 기술력에 의존하고 있으며, 낙석방지망의 경우 부분적 취약점(일체화가 되지 못함)으로 인해 충분한 지지능력을 발휘하지 못하고 망이 터지는 문제점 등이 발생됨에 따라 국내에서도 보다 높은 낙석 에너지를 지지할 수 있는 낙석방지망에 대한 연구가 필요할 것으로 판단된다. 이에 본 연구에서는 낙석방지망으로써의 적용가능한 Expanded Metal(3.2T)을 대상으로 낙석방지망 인발시험을 실시하여 망 크기에 따른 하중-변위 특성 및 파괴형태를 분석하여 Expanded Metal 낙석방지망의 경제적이고 합리적인 규격을 판단하는데 기초자료로 제공하고자 하였다.

• 자원환경지질
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• 제23권2호
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• pp.183-199
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• 1990

Ore deposits of Dongwon mine are composed of numerous gold and silver veins emplaced in sedimentary rocks of Cambrian Choseon Supergroup and granitoids of Cretaceous age. Ore veins of the mine can be divided into gold and silver veins on the base of vein structure, mineral assemblage and vein trends. Mutual relationships between gold and silver veins are uncertain. Gold veins are simple veins which are composed of base-metal sulfides, and electrum with quartz and ankerite. On the other hand, silver veins are complex veins which reveal three distinct stages of mineral deposition based on vein structure; stage I, deposition of small amounts of oxides and pyrite with quartz; stage II, deposition of base-metal sulfides, small amounts of Ag-bearing minerals, calcite and quartz; stage III, deposition of base metal sulfides, electrum, Ag-sulfosalts, native silver, carbonates and quartz. Homogenization temperature and salinity of fluid inclusion from quartz of gold vein are as follows; $229^{\circ}$ to $283^{\circ}C$, 4.7 to 6.4 wt.% equivalent NaCI. The ore mineralogy suggests that temperature(T) and sulfur fugacity($fs_2$) of the formation of the gold vein and stage III of silver vein are estimated as T ; $294^{\circ}$ to $318^{\circ}C$, $fs_2\;10^{-9.4}$ to $10^{-10.1}$ atm. and T; $240^{\circ}$ to $279^{\circ}C$, $fs_2;10^{-11.1}$ to $10^{-17.3}$ atm. respectively. Pressure condition during gold vein formation estimated from data of ore mineralogy and fluid inclusion range 500 to 750 bar.

• 한국재료학회지
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• 제12권2호
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• pp.140-145
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• 2002

This study was conducted to investigate the brazing characteristics between Zircaloy-4 nuclear fuel cladding tubes and bearing pads with filler metals of amorphous $Zr_{1-x}Be_x$(0.3$\leq$x$\leq$0.5) binary alloy, in which they were produced in the ribbon form by the melt-spinning metod. The crystallization behavior, stability, hardness and micro-structure of brazed zone were examined by X-ray diffraction, differential scanning calorimetry, micro-Vickers hardness test, optical microscopy, and transmission electron microscopy. $Zr_{1-x}Be_x$(0.3$\leq$x$\leq$0.4) amorphous alloys were crystallized to $\alpha$-Zr with increasing the temperature, and the rest were transformed to ZrBe$_2$at higher temperatures. On the other hand, $Zr_{1-x}Be_x$(0.4$\leq$x$\leq$0.5) amorphous alloys were crystallized to $\alpha$-Zr and ZrBe$_2$, simultaneously. The thickness of the layer brazed with amorphous alloy was increased with increasing the beryllium content due to the higher diffusion of Be. The morphology of brazed layer with PVD Be filler metal showed dendrite while that brazed with amorphous alloys appeared globular. Micro-Vickers hardness of brazed zone increased as the beryllium content of filler metal was decreased.

• Bulletin of the Korean Chemical Society
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• 제24권3호
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• pp.269-273
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• 2003

The synthesis and properties of 2,13-bis(3'-pyridylmethyl) $(L^3)$, 2,13-bis(4'-pyridylmethyl) $(L^4)$, and 2,13-bis(phenylmethyl) $(L^5)$ derivatives of 5,16-dimethyl-2,6,13,17-tetraazatrcyclo$[16.4.0.^{1.18}0^{7.12}]$docosane are reported. The 3- or 4-pyridylmethyl groups of $[ML^3](ClO_4)_2\;or\;[ML^4](ClO_4)_2$ (M = Ni(Ⅱ) or Cu(Ⅱ)) are not involved in coordination, and the coordination geometry (square-planar) and ligand field strength of the complexes are quite similar to those of $[ML^5](ClO_4)_2$, bearing two phenylmethyl pendant arms. However, the complex formation reactions of $L^3\;and\;L^4$ are strongly influenced by the pyridyl groups, which can interact with a proton or metal ion outside the macrocyclic ring. The macrocycle $L^5$ exhibits a high copper(Ⅱ) ion selectivity against nickel(Ⅱ) ion; the ligand readily reacts with copper(Ⅱ) ion to form $[CuL^5]^{2+}$ but does not react with hydrated nickel(Ⅱ) ion in methanol solutions. On the other hand, $L^3\;and\;L^4$ form their copper(Ⅱ) and nickel(Ⅱ) complexes under a similar condition, without showing any considerable metal ion selectivity. The ligands $L^3\;and\;L^4$ react with copper(Ⅱ) ion more rapidly than does $L^5$ at pH 6.4. At pH 5.0, however, the reaction rate of the former macrocycles is slower than that of the latter. The effects of the 3- or 4-pyridylmethyl pendant arms on the complex formation reaction of $L^3\;and\;L^4$ are discussed.