• Title/Summary/Keyword: Membrane Characterization

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Fabrication and Characterization of a Pressure Sensor using a Pitch-based Carbon Fiber (탄소섬유를 이용한 압력센터 제작 및 특성평가)

  • Park, Chang-Sin;Lee, Dong-Weon;Kang, Bo-Seon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.4
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    • pp.417-424
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    • 2007
  • This paper reports fabrication and characterization of a pressure sensor using a pitch-based carbon fiber. Pitch-based carbon fibers have been shown to exhibit the piezoresistive effect, in which the electric resistance of the carbon fiber changes under mechanical deformation. The main structure of pressure sensors was built by performing backside etching on a SOI wafer and creating a suspended square membrane on the front side. An AC electric field which causes dielectrophoresis was used for the alignment and deposition of a carbon fiber across the microscale gap between two electrodes on the membrane. The fabricated pressure sensors were tested by applying static pressure to the membrane and measuring the resistance change of the carbon fiber. The resistance change of carbon fibers clearly shows linear response to the applied pressure and the calculated sensitivities of pressure sensors are $0.25{\sim}0.35 and 61.8 ${\Omega}/k{\Omega}{\cdot}bar$ for thicker and thinner membrane, respectively. All these observations demonstrated the possibilities of carbon fiber-based pressure sensors.

Isolation and characterization of a noval membrane-bound cytochrome $C_{553}$ from the strictly anaerobic phototroph, heliobacillus mobilis

  • Lee, Woo-Yiel;Bla;Kim, Seung-Ho
    • Journal of Microbiology
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    • v.35 no.3
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    • pp.206-212
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    • 1997
  • Heliobacillus mobilis is a strictly anaerobic Gram-positive bacterium which contains a primitive Photosystem I-type reaction center. The membrane-bound cytochrome $C_{553}$ from the heliobacterium suggested to be the immediate electron donor to the photooxidized pigment (P798+) has been isolated and characterized. The heme protein was visualized as a major component with an apparent molecular size of 17kDa in TMBZ-staining analysis of the membrane preparation and showed characteristic $\alpha$ (552.5 nm), $\beta$ (522nm), and Soret absorption (416 nm) peaks of a typical reduced c-type cytochrome in the partially purified sample. The internal 43 amino acid sequence of the electron donor was obtained by chemical agent and protease treatments followed by N-terminal sequencing of the resulting fragments. The internal sequence carries lots of lysine residues and a Cys-X-X-Cys-His sequence motif which are the characteristics of typical c-type cytochromes. The analysis of the sequence by FAST or FASTA program, however, did not show any significant similarity to other known heme proteins.

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Preparation and Characterization of the Asymmetric Microporous Poly(vinylidene fluoride) (PVDF) Blend Membranes with Hydrophilic Surfaces

  • Hwang, Jeong-Eun;JeGal, Jong-Geon
    • Korean Membrane Journal
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    • v.9 no.1
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    • pp.1-11
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    • 2007
  • To prepare chemically stable asymmetric microporous membranes with a hydrophilic surface, which would be expected to have better antifouling properties, poly(vinylidene fluoride) (PVDF) blend membranes were prepared by the phase inversion process. PVDF mixture solutions in N-methylpyrrolidone (NMP) blended with several polar potential ionic polymers such as polyacrylonitrile (PAN), poly(methylmethacrylate) (PMMA) and poly(N-isopropylacrylamide) (NIPAM) were used for the formation of the PVDF blend membranes. They were then characterized with several analytical methods such as FESEM, FTIR, contact angle measurement, pore size distribution and permeability measurement. Regardless of different polar polymers blended, they all showed a finger-like structure with more hydrophilic surface than the pristine PVDF membrane. For all the PVDF blend membrane, due to the polar potential ionic polymers used, the flux of those was improved. Especially the PVDF blend membrane with NIPAM showed the highest flux among the membranes prepared. Also antifouling property of the PVDF membrane was improved by the use of the polar polymers.

Electrospun $SiO_2$ membrane using covalently cross-linked SPEEK/HPA by impregnation for high temperature PEMFC

  • Na, Heesoo;Hwang, Hyungkwon;Lee, Chanmin;Shul, Yonggun
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.11a
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    • pp.85.2-85.2
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    • 2010
  • There is widespread effort to develop polymer membranes in place of Nafion for high temperature polymer electrolyte membrane fuel cell(PEMFC). In our study, SiO2 membranes are arranged by electrospinning method. For impregnation solution, the modified sulfonated poly(ether ether ketone)(SPEEK) polymer is prepared from sulfonation, sulfochlorination, partial reduction and lithiation reaction. The modified polymer is cross-linked with 1,4-diiodobetane in NMP solvent and then blended with Heteropoly acid(HPA). The characterization of membranes is confimed by FT-IR, Thermogravimetry(TGA), water uptake test and single cell performance test for PEMFC, etc. The composite membrane shows satisfactory thermal and mechanical properties. Beside, The membrane exhibits good ion exchange capacity and high proton conductivity. As a result, The composite membrane is promising as an alternative membrane in high temperature PEMFC.

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Cloning and Characterization of Ribosome-associated Membrane Protein 4 (RAMP4) gene in silkworm Bombyx mori

  • Yao Qin;Hu Zhigang;Xu Jiaping;Chen Keping
    • International Journal of Industrial Entomology and Biomaterials
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    • v.10 no.2
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    • pp.125-129
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    • 2005
  • Ribosome-associated membrane protein 4 (RAMP4) is a membrane protein that exposes its N-terminal hydrophilic portion on the cytoplasmic side and spans the membrane close to the C-terminal end. RAMP4 has previously been reported to belong to the set of proteins that remains associated with membrane-bound ribosomes, and controls the glycosylation of major histocompatbility complex class II-associated invariant chain. RAMP4 also may be relative to the stabilization of membrane proteins in response to stress, with other components of translocon, and molecular chaperons in ER. Application of 5'-RACE technique with specially designed primer, we cloned a 715 bp cDNA fragment which contains a 195 bp ORF, termed RAMP4. The deduced protein has 64 amino acid residues and contains a putative transmembrane-spanning domain at the COOH terminus.

Characterization of Organic Solvent Resistant Membranes

  • 전종영;김윤조;탁태문
    • Proceedings of the Membrane Society of Korea Conference
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    • 1994.10a
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    • pp.62-63
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    • 1994
  • The membrane technology is more convenient and economical way in the separation field than conventional technology such as distillation, extration, crystallization, and so on. Therefore, membrane are used as efficient tools for the separation and concentration of molecular mixture in many industrial area. Although the polymeric membrane have various advantage, they have disadvantages as well. One of them is a poor resistance to organic solvent. Therefore, organic solvent resistant membranes were prepared by soluble polyimide. prepared by phase inversion method. The membranes were The homogeneous polymer solutions were obtained by the two different method ; the one is that the polymer sythesized was completely dissolved in a solvent to prepare a membrane casting solution, the other is that a membrane casting solution was prepared by the unit process from the viscose solution of polymerization.

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Recent Progress in Surface Science and Its Application in Advanced Water Treatment by Membrane Processes

  • Matsuura, Takeshi
    • Proceedings of the Membrane Society of Korea Conference
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    • 1997.06a
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    • pp.21-35
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    • 1997
  • As environmental regulations become more stringent, water, used either as drinking water or as industrial process water, becomes increasingly better in its quality. As a result, an increasingly more advanced water treatment technology is required. It is believed that membrane technology will be able to satisfy such a requirement. The heart of the membrane technology is membrane. The advancement in water treatment technology using membranes, therefore, depends on the development of novel membranes which are superior in performance to the currently available membranes. In this paper, a brief review will be made how the recent progress in surface science, such as surface modification and surface characterization, has aided to improve the performance of the membranes used for water treatment. Some suggestions will also be made regarding the future direction of the research in this area.

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Characterization of Phase Inversion Membrane of Sulfonated Polyetherimide (Sulfonated Polyetherimide Membrane의 특성)

  • 김완주;최남석;최중구;김인철;김종호;탁태문
    • Membrane Journal
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    • v.9 no.1
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    • pp.1-9
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    • 1999
  • Sulfonated polyetherimide having anionic charge and better hydrophilicity than polyetherimide was prepared by reacting polyetherimide with chlorosulfonic acid. To prepare casting solution, from which the membrane having good performance can produce. Polyvinylpyrrolidone as a pore forming agent and volatile weak solvent such as dichloromethane to foml the dense skin layer were added to the sulfonated polyetherimide / N -methyl-2-pyrrolidone solution. Membrane fabricated sulfonated PEl showed better fouling resistance to the protein than those fabricated PEL because of its hydrophilicity. Solute having negative charge was removed effectively with membrane fabricated from the sulfonated PEl because of its the same electron charge.

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Study of Thermally Induced Phase Separation of Polyvinylidene Fluoride-Silica Mixture for the Preparation of Porous Polymeric Membrane (다공성 분리막 제조를 위한 폴리플루오르화비닐리덴-실리카 혼합물의 열유도상분리 연구)

  • Kim, Se Jong;Lee, Jeong Woo;Nam, Sang Yong
    • Membrane Journal
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    • v.27 no.2
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    • pp.189-198
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    • 2017
  • In this study, we used thermally induced phase separation (TIPS) to produce water treatment membrane and poly(vinylidene fluoride) (PVDF), silica with excellent mechanical properties and chemical resistance to evaluate characterization of the membrane. The diluents used for the characterization were dioctyl phthalate (DOP) and dibutyl phthalate (DBP). We observed the crystallization temperature, cloud point and SEM images to see the manufacture conditions according to the ratio of PVDF and silica. The crystallization temperature and cloud point increased with the contents of silica. Through the phase diagram drawn from these results, the conditions for the preparation of the membrane confirmed.