• Title/Summary/Keyword: Melting point

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A Study on the Optimum Chemical Composition of Insert Metal for Liquid Phase Diffuse Bonding (액상확산접합용 인서트금속의 화학조성 최적화에 관한 연구)

  • 김대업;정승부;강정윤
    • Journal of Welding and Joining
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    • v.18 no.5
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    • pp.90-97
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    • 2000
  • Effect of alloy elements on joinability of insert metal for liquid phase diffusion bonding of heat resistant alloys was investigated in this study. Also, optimum chemical composition of insert metal was explained using interpolation method. The insert metals utilized was commercial Ni-base amorphous foils and newly developed Ni-base filler metals with B, Si and Cr in this study. Melting point and critical interlayer width(CIW) decreased with increasing additional amount of B, Si and Cr, melting point lowering element of the insert metal. Optimized chemical composition of insert metals could be estimated by interpolation method. The optimum amount of B, Si, Cr addition into the insert metal were found to be about 3%, 4% and 3%, respectively. The measured characteristic values, melting point, microhardness in the bonded interlayer and CIW of the insert metals were the almost identical to ones of the calculated results by interpolation method.

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Doctor Blade Tape Casting of In-based Low Melting Point Alloy (In 계 저융점합금의 닥터 블레이드 테이프캐스팅)

  • Youn, Ki-Byoung
    • Journal of Korea Foundry Society
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    • v.35 no.3
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    • pp.62-66
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    • 2015
  • Tape casting is an important forming operation used to prepare flat sheets in the various industries. In this study, Doctor Blade tape casting of In-based low melting point alloy was carried out. The purpose of this investigation was to determine the possibility of applying the Doctor Blade tape casting process to the manufacture of low melting point alloy sheets that can be used as thermal fusible parts of battery safety systems. In-based molten alloy that has a melting point of $95^{\circ}C$ was produced; it's viscosity was measured at various temperatures. The molten alloy was used as a slip in the caster of the Doctor Blade tape casting system. The effects of the molten alloy temperatures and carrier speeds on the produced sheet shape were observed. For the casting conditions of 1.5 cm slip height, $120^{\circ}C$ slip temperature, 0.05 mm blade gap and 60 m/min. carrier speed, an In-based alloy thin tape well shaped with 0.16 mm uniform thickness was continuously produced.

DEVELOPMENT OF TITANIUM-BASED BRAZING FILLER METALS WITH LOW-MELTING-POING

  • Onzawa, Tadao;Tiyama, Takashi
    • Proceedings of the KWS Conference
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    • 2002.10a
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    • pp.539-544
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    • 2002
  • Titanium and titanium alloy are excellent in corrosion resistance and specific intensity, and also in the biocompatibility. On the other hand, the brazing is bonding method of which productivity and reliability are high, when the complicated and precise structure of the thin plate is constructed. However, though conventional titanium-based brazing filler metal was excellent in bond strength and corrosion resistance, it was disadvantageous that metal structure and mechanical property of the base metal deteriorated, since the brazing temperature (about 1000 C) is considerably high. Authors developed new brazing filler metal which added Zr to Ti-Cu (-Ni) alloy which can be brazed at 900 C or less about 15 years ago. In this paper, the development of more low-melting-point brazing filler metal was tried by the addition of the fourth elements such as Ni, Co, Cr for the Ti-Zr-Cu alloy. As a method for finding the low-melting-point composition, eutectic composition exploration method was used in order to reduce the experiment point. As the result, several kinds of new brazing filler metal such as 37.5Ti-37.5-Zr-25Cu alloy (melting point 825 C) and 30Ti-43Zr-25Cu-2Cr alloy (melting point: 825 C) was developed. Then, the brazing joint showed the characteristics which were almost equal to the base metal from the result of obtaining metallic structure and strength of joint of brazing joint. However, the brazing filler metal composition of the melting point of 820 C or less could not be found. Consequentially, it was clarified that the brazing filler metal developed in this study could be practically sufficiently used from results such as metal structure of brazing joint and tensile test of the joint.

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Prediction of Melting Point for Drug-like Compounds Using Principal Component-Genetic Algorithm-Artificial Neural Network

  • Habibi-Yangjeh, Aziz;Pourbasheer, Eslam;Danandeh-Jenagharad, Mohammad
    • Bulletin of the Korean Chemical Society
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    • v.29 no.4
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    • pp.833-841
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    • 2008
  • Principal component-genetic algorithm-multiparameter linear regression (PC-GA-MLR) and principal component-genetic algorithm-artificial neural network (PC-GA-ANN) models were applied for prediction of melting point for 323 drug-like compounds. A large number of theoretical descriptors were calculated for each compound. The first 234 principal components (PC’s) were found to explain more than 99.9% of variances in the original data matrix. From the pool of these PC’s, the genetic algorithm was employed for selection of the best set of extracted PC’s for PC-MLR and PC-ANN models. The models were generated using fifteen PC’s as variables. For evaluation of the predictive power of the models, melting points of 64 compounds in the prediction set were calculated. Root-mean square errors (RMSE) for PC-GA-MLR and PC-GA-ANN models are 48.18 and $12.77{^{\circ}C}$, respectively. Comparison of the results obtained by the models reveals superiority of the PC-GA-ANN relative to the PC-GA-MLR and the recently proposed models (RMSE = $40.7{^{\circ}C}$). The improvements are due to the fact that the melting point of the compounds demonstrates non-linear correlations with the principal components.

Study of Manufacturing Jewelry Master Pattern by Using the DuraForm Rapid Prototyping Mold and the Low Melting Alloy (쾌속조형 듀라폼몰도와 저융점합금을 이용한 주얼리용 마스터패턴 제작에 관한 연구)

  • Joo, Young-Cheol;Song, Oh-Sung
    • Journal of Korea Foundry Society
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    • v.22 no.5
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    • pp.265-270
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    • 2002
  • A novel jewelry master pattern manufacturing process which reduce manufacturing steps by employing a Duraform rapid prototyping mold and a low melting alloy has been suggested. The novel process follows the steps of 'jewelry 3D CAD design ${\rightarrow}$ Durafrom RP mold ${\rightarrow}$ low melting alloy master pattern' while the previous process follows more complicated steps of 'jewelry idea sketch ${\rightarrow}$ detailed drawing ${\rightarrow}$ wax carving ${\rightarrow}$ flask ${\rightarrow}$ silver master pattern.' An upper and a lower part of molds have been manufactured of Duraform powder, of which melting point is $190^{\circ}C$. A maser pattern was manufactured by pouring a low melting alloy of Pb-Sn-Bi-Cd, so called Woods Metal, of which melting point is $70^{\circ}C$, into the mold. The master pattern is a shape of a disk of 20mm diameter that contains various design factors. The variations of dimensions, surface roughness, surface pore ratio were measured by an optical microscope, a surface roughness profilometer, and a Rockwell hardness tester. The pattern made of were maeasured by an optical microscope, a surface roughness profilometer, and a Rockwell hardness tester. The pattern made of low melting alloy has sufficient surface hardness, and surface pore ratio to be used as the jewelry master pattern.

Phase transition features of binary Co-C eutectic temperature fixed-point (이원계 Co-C 공정계 온도 고정점의 특성)

  • Kim, Yong-Gyoo;Yang, In-Seok;Gam, Kee-Sool
    • Journal of Sensor Science and Technology
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    • v.14 no.6
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    • pp.381-386
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    • 2005
  • A Co-C eutectic cell for thermocouple calibration was manufactured and tested to investigate its phase transition characteristics using Type B thermocouples. It was observed that the freezing plateaus were flatter than those of melting, but the melting points were closer to the true transition temperature than the freezing points. The expanded uncertainty of melting temperature was calculated not to exceed $0.2^{\circ}C$ (k = 2). Based on the observed results, the melting process is recommended for the calibration of thermocouples.

Effect of Si content on Nugget Diameter of Electric Resistance Spot Welded Dual Phase Steel (DP강의 전기저항점용접부 너깃직경에 미치는 Si 함량의 영향)

  • Kong, Jong-Pan;Kang, Gil-Mo;Han, Tae-Kyo;Chin, Kwang-Geun;Kang, Chung-Yun
    • Journal of Welding and Joining
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    • v.29 no.5
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    • pp.99-105
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    • 2011
  • In this study, effect of Si content on nugget diameter in electric resistance spot welded dual-phase(DP) steel was investigated. The cold rolled DP steels with different Si content (0.5, 1.0, 1.5, 2.0 wt.%) were used and thickness of those sheet was 1.2mm. With increasing Si content, nugget diameter was increased at the same welding current. This is attributed to increase of heat input result from high resistivity. Also, nugget diameter was increased with an increase in Si content for the same heat input. For this reason, the melting point of DP steel is lowered with an increase in the Si content. And solid DP steel can easily be transformed to a liquid phase because the low melting point. Finally, a prediction formula for the nugget diameter(N.D.) could be obtained in terms of heat input(Q) and melting point(M.P) as follows: N.D.(mm) = 0.11Q(J) - 0.0031 M.P.($^{\circ}C$) + 0.32.

A Study on the Preheating Effect of Multi-Heat Sources using Laser Plasma in the Thermally Assisted Machining of a High-Melting-Point Material (고융점 소재의 열 보조 가공에서 레이저 -플라즈마 다중열원의 예열 효과에 대한 연구)

  • Lee, Choon-Man;Kim, Seong-Gyu
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.18 no.10
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    • pp.93-98
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    • 2019
  • Recently, with the development of the aerospace and automotive industries, the demand for high-melting-point materials has increased. However, high-melting-point materials are difficult to cut through conventional machining methods. Thermally assisted machining (TAM) is a method for improving the machinability by preheating the materials. A laser, the most commonly used device for TAM, has high efficiency through local preheating but is not sufficient for maintaining a high preheating temperature due to rapid cooling. However, the use of multi-heat sources can supplement the disadvantage of a single heat source. The high preheating temperature can be maintained with a wide and deep heat-affected zone (HAZ) by multi-heat sources. The purpose of this study is to analyze the preheating effects of multi-heat sources using laser plasma. Thermal analysis and preheating experiments were carried out. As a result, the high preheating effect of multi-heat sources compared with a single heat source was verified.

Inter-comparison of temperature measurement capability using standard platinum resistance thermometers (표준백금저항온도계를 이용한 온도측정능력 상호비교)

  • Gam, K.S.;Kang, C.S.;Lee, Y.J.;Lee, K.B.;Kim, Y.G.;Park, S.N.
    • Journal of Sensor Science and Technology
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    • v.18 no.1
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    • pp.86-94
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    • 2009
  • Temperature measurement capability was inter-compared using the transfer standard platinum resistance thermometers(SPRT) among four laboratories of KRISS. The transfer SPRTs were primarily calibrated at the triple point of water and Ga melting point, then used at inter-comparison experiment. Temperature difference of calibration value between temperature laboratory and length laboratory at $20^{\circ}C$ was -0.7 mK and +2.4 mK at density laboratory. Temperature measured near $20^{\circ}C$, $25^{\circ}C$ and $30^{\circ}C$ at fluid flow laboratory was deviated by $34.2{\sim}80.4\;mK$ from the calibration values of the transfer SPRT. Ga melting points was inter-compared among three laboratories, and the difference of Ga melting points against the standard Ga melting point of temperature laboratory were $0.03{\sim}0.54\;mK$ at length laboratory and 0.02 mK at density laboratory.

Dyeing and Heat Setting Properties of Low Melting PET Fiber (저온융착사를 이용한 섬유의 염색성 및 열처리 특성)

  • Hwang, Se-Jeong;Choi, Hyun-Seuk;Kim, Dong-Kwon;Chong, In-Sik;Kim, Sung-Gun
    • Textile Coloration and Finishing
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    • v.21 no.3
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    • pp.37-42
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    • 2009
  • The low melting PET yarn has sheath/core structure: sheath portion consists of low melting point PET and core portion is regular PET. Dyeing properties of fabric made from low melting PET yarn were investigated at different dyeing temperatures. It was found that the exhaustion yield on the low melting PET fabric was higher than on regular PET fabric. The total K/S value of the dyed low melting PET fabric increased as heat setting temperature increased above $150^{\circ}C$ because the sheath portion of the low melting yarn melted. Although fastness to light of the low melting PET fabric was similar to regular PET fabric, fastness to washing was inferior to regular PET fabric by 1 grade.