• Title/Summary/Keyword: Melt spun ribbon

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The effect on small Al addition of the melt-spun Nd-Fe-C magnent (비정질 Nd-Fe-C 자석에 미치는 Al 첨가의 영향)

  • 조대형
    • Electrical & Electronic Materials
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    • v.10 no.10
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    • pp.995-999
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    • 1997
  • For melt-spun Fe-Nd-C alloy variation of phase development and magnetic properties with the variety of small Al addition was investigated. As the amount of Al addition increased the amorphization of Fe$_{14}$/Nd$_{2}$/C or $\alpha$-Fe was retarded and the residual Fe$_{14}$/Nd$_{2}$/C or $\alpha$-Fe did not eliminated after heat treatment resulting in poor coercivities of the ribbons. The grain size of Fe$_{14}$/Nd$_{2}$/C increased with the increase of Al addition and the abnormal grain was often found out in the ribbon heat treated for more then 10 min. The enhancement of coercivity was the highest with the addition of 0.5at%Al. As the amount of Al addition increase the coercivities dropped rapidly. The highest coercivity obtained so far is 13.9kOe which about 16% higher than that(11.2kOe) obtained from the Al-free specimen.

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Microstructure and Tensile Property of Rapidly Solidified Al-Be alloy (급속응고한 Al-Be합금의 미세조직 및 인장특성)

  • Lee, In-Woo;Park, Hyun-Ho;Kim, Myung-Ho
    • Journal of Korea Foundry Society
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    • v.15 no.5
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    • pp.459-468
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    • 1995
  • For high performance aerospace structures, the properties of highest priority are low density, high strength, and high stiffness(modulus of elasticity). Addition of beryllium decrease the density of the aluminum alloy and increase the strength and the stiffness of the alloy. However it is very difficult to produce the Al-Be alloy having useful engineering properties by conventional ingot casting, because of the extremely limited solid solubility of beryllium in aluminum. So, rapid solidification processing is necessary to obtain extended solid solubility. In this study, rapidly solidified Al-6 at% Be alloy were prepared by twin roll melt spinning process and single roll melt spinning process. Twin roll melt spun ribbons were extruded at $450^{\circ}C$ with reduction in area of 25 : 1 after vacuum hot pressing at $550^{\circ}C and 375^{\circ}C$. The microstructure of melt spun ribbon exhibited a refined cellular microstructure with dispersed Be particles. As advance velocity of liquid/solid interface increase, the morphology of Be particle vary from rod-like type to spherical type and the crystal structure of Be particle from HCP to BCC. These microstructural characteristics of rapidly solidified Al-6at.%Be alloy were described on the basis of metastable phase diagram proposed by Perepezko and Boettinger. The extruded ribbon consisted of recrystallized grains dispersed with Be particles and exhibited improved tensile property compared with that of extruded ingot.

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A Comparative Study of Mechanical Property in Al-8Fe-2Mo-2V-1Zr Bulk Alloys Fabricated from an Atomized Powder and a Melt Spun Ribbon

  • Jung, T.K.;Sung, T.J.;Kim, M.S.;Kim, W.Y.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1023-1024
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    • 2006
  • Al-8Fe-2Mo-2V-1Zr alloys were prepared by the gas atomization/hot extrusion and the melt spinning/hot extrusion. For the gas atomized and extruded alloy, equiaxed grains with the average size of 400 nm and finely distributed dispersoids with their particle sizes ranging from 50nm to 200nm were observed. For the melt spun and hot extrusion processed alloy, refined microstructural feature consisting of equiaxed grains with the average size of 200nm and fine dispersoids with their particle sizes under 50nm appeared to exhibit a difference in microstructure. Strength of the latter alloy was higher than that for the former alloy up to elevated temperatures.

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Bulk Amophisation and Decomposition Behavior of Mg-Cu-Y Alloys (Mg-Cu-Y합금의 벌크 비정질화 및 상분해 거동)

  • Kim, S.H.;Kim, D.H.;Lee, J.S.;Park, C.G.
    • Applied Microscopy
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    • v.26 no.2
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    • pp.235-241
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    • 1996
  • Amophization and decomposition behaviour in $Mg_{62}Cu_{26}Y_{12}$ alloy prepared by melt spinning method and wedge type metal mold casting method have been investigated by a detailed transmission electron microscopy. Amorphous phase has formed in melt-spun ribbon. In the case of the wedge type specimen, however, the amorphous phase has formed only around the tip area within about 2 mm thickness. The remaining part of the wedge type specimen consists of crystalline phases, $Mg_{2}Cu\;and\;Cu_{2}Y$. The supercooling for crystallization behaviour of the amorphous $Mg_{62}Cu_{26}Y_{12}$ alloy, ${\Delta}T_x$ has been measured to be about 60 K. Such a large undercooling of the crystallization bahaviour enables formation of the amorphous phase in the $Mg_{62}Cu_{26}Y_{12}$ alloy under the cooling rate of $10^{2}K/s$. The amorphous $Mg_{62}Cu_{26}Y_{12}$ has decomposed into crystalline phases, $Mg_{2}Cu\;and\;Cu_{2}Y$ after heat treatment at $170^{\circ}C\;and\;250^{\circ}C$.

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A Study on the Magnetic Properties of Melt-Spun (Fe, T)-Nd-C Alloys (TAl, Ti, Co, Ni)

  • Jang, T.S.;Cho, D.H.
    • Journal of Magnetics
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    • v.3 no.4
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    • pp.116-119
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    • 1998
  • Influence of small additions ($\leq$2.0 at.%) of Al, Ti, Co, and Ni on the microstructural development and the magnetic properties of melt-spun Fe-Bd-C alloys was investigated. Addition of these elements tended to stabilize the crystallization of as-spun ribbons. Especially, Al and Ti preferred to stabilize$ Fe_{17}Nd_2C_x.$ The average grain size of Fe17Nd2Cx (0.1~0.3 ${\mu}{\textrm}{m}$), obtained by a proper annealing, in the ribbon treated with 0.5 at.% additive was much smaller than that of additive-free ribbons, which would be the major source of large increase in coercivity. Among the additives, Ni was very effective to increase the coercivity whereas Co had beneficial effect on $T_c.$ By adding 0.5 at.% Ni, intrinsic coercivities of more than 1.4 T, 40~50% higher than that (~1.0T) of additive-free ribbons, can be obtained after annealing at 750~80$0^{\circ}C$.

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