• Title/Summary/Keyword: Medium chemical analysis

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The Characteristic of Pt-RTD Fabricated on Si Substrate (실리콘 기판상에 제작된 박막형 Pt-RTD의 특성)

  • Hong, Seok-Woo;Moon, Kyung-Min;Noh, Sang-Soo;Chung, Gwiy-Sang
    • Proceedings of the KIEE Conference
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    • 1999.07d
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    • pp.1806-1808
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    • 1999
  • The electrical and physical characteristics of MgO and Pt thin-films on Si substrate, deposited by r.f magnetron sputtering. It were analyzed with annealing condition($1000^{\circ}C$ for 120 min) by four point probe, a-step, SEM and XRD. Until $1000^{\circ}C$ of annealing temperature, MgO medium layer had the properties of improving Pt adhesion to $SiO_2$ and insulation without chemical reaction to Pt thin-films and the resistivity of Pt thin-films was improved. In the analysis of properties of Pt-RTD, TCR value had $3927ppm/^{\circ}C$ and liner in the temperature range of room temperature ${\sim}400^{\circ}C$.

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The Effect of Annealing Treament with Aluminum Oxide as Medium Layer and Platinum Heater (매개층 알루미늄산화막과 백금 발열체의 열처리 효과)

  • 노상수;정귀상
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1997.04a
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    • pp.314-317
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    • 1997
  • The electrical and physical characteristics of aluminum oxide and Pt thin films on it, deposited by reactive sputtering and DC magnetron sputtering respectively, were analyzed with increasing annealing temperature(400~80$0^{\circ}C$) by four point probe, SEM and XRD. Under $600^{\circ}C$ of annealing temperature, aluminum oxide had the properties of improving Pt adhesion to SiO$_2$and insulation without chemical reaction to Pt thin films and the resistivity of Pt thin films was improved. But these properties of aluminum oxide and Pt thin films on it were degraded over $700^{\circ}C$ of annealing temperature because aluminum oxide was changed into metal aluminum and then reacted to Pt thin films deposited on it. In the analysis of the thermal charateristics of Pt micro-heater fabricated on Si07/si substrate, the temperature of Pt micro-heater is up to 41$0^{\circ}C$ with the power dissipation 1.8 watts.

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Accumulation and Depuration of Fluoranthene, a Polycyclic Aromatic Hydrocarbon, in Rockfish Sebastes schlegeli (조피볼락 (Sebastes schiegeii)에서 다환성방향족탄화수소 fluoranthene의 축적과 배설)

  • Park Kwan Ha
    • Environmental Analysis Health and Toxicology
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    • v.20 no.3 s.50
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    • pp.223-228
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    • 2005
  • Rockfish Sebastes schlegeli was exposed to fluoranthene, a ubiquitous polycyclic aromatic hydrocarbon, at 1 and 10 $\mu$g/L for 4 weeks followed by depuration period of 8 weeks. Although the fluoranthene in the p]asma reached only 1.8$\~$1.9 times seawater concentration, it was 6.5 $\~$ 15.7 times higher in the liver, spleen and bile indicating efficient accumulation in the lipid -containing body tissues. When the exposed fish were then maintained in clean water, rapid fluoranthene decline occurred in the initial 2 weeks followed by a rather slow phase. This result suggests that fluoranthene accumulates efficiently provided the existence in the culture medium, but the contaminant disappears rapidly once the chemical source is removed. The fluoranthne residue in fish tissues my be a good indifator for relent PAHs exposure.

The Fabrication of Micro-Heater MgO Medium Layer and It`s Characteristics (산화마그네슘을 매개층으로 이용한 백금박막 미세발열체의 제작과 그 특성)

  • 홍석우;노상수;장영석;정쉬상
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.150-153
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    • 1999
  • The electrical and physical characteristics of MgO and Pt thin-films on Si wafers deposited by r.f magnetron sputtering, were analyzed with annealing condition(100$0^{\circ}C$, 120 min) by four point probe, SEM and XRD. Until annealing temperature of 100$0^{\circ}C$, MgO had the properties of improving Pt adhesion to SiO$_2$ and insulation without chemical reaction to Pt thin-films and the resistivity of Pt thin-films was improved. The thermal characteristics of Pt micro-heater were analyed with Pt-RTD integrated on the same substrate, In the analysis of properties of Pt-RTD, TCR value had 3927 ppm/$^{\circ}C$ and liner in the temperature range of 25~40$0^{\circ}C$ temperature of Pt micro-heater had up to 40$0^{\circ}C$ with 1.5 watts of the heating power.

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Analysis of Erythropoietin Glycoform Produced by Recombinant CHO Cells Using the Lectin-Blotting Technique

  • Chang, Kern-Hee;Kim, Kyung-Soo;Kim, Jung-Hoe
    • Biotechnology and Bioprocess Engineering:BBE
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    • v.3 no.1
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    • pp.40-43
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    • 1998
  • The glycosylation pattern of Erythropoietin (EPO), produced by recombinant CHO cells, was studied using the simple and rapid technique of 'Lectin-blotting'. In this experiment we used three different kinds of lectins, MAA(Maackia amurensis agglutinine), RCA(Ricinus communis agglutinine), and DSA(Datura stramonium agglutinine), which bind to the terminal sialic acid, galactose, and the N-acetyllactosamine chain respectively. The lectin-blotting technique was used to analyze the carbohydrate structure of EPO produced in the presence of two physiologically active chemical compounds, ammonium and chloroquine. The effect of the ammonium ion on the glycosylation of EPO was studied because it accumulated in the medium mainly as a by-product of glutamine matabolism. Ammonium chloride significantly inhibited the sialylation of the terminal galactose residue at concentrations of 8mM or more. Chloroquine, a potent inhibitor of glycosylation, inhibited terminal sialylation at concentrations of 100 and 200 $\mu$M, and at a concentration of 300 $\mu$M, also inhibited Nacetyllactosamine chain synthesis.

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Determination of Mercury in Korean Mussels (Mytilus coruscus) for Marine Environmental Monitoring (연안환경 모니터링을 위한 홍합(Mytilus coruscus)의 체내 수은 함량 분석)

  • Lee, Soo Yong;Lee, Jangho
    • Journal of Environmental Science International
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    • v.27 no.12
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    • pp.1291-1298
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    • 2018
  • Marine ecosystems are frequently exposed to a variety of chronic and acute pollutants derived from anthropogenic production and consumption activities. Mussels are sessile (can provide location-specific information), medium-sized (have enough tissue matrix for chemical analysis) filter-feeders (show accumulation of pollutant chemicals from seawater). These biological and ecological characteristics make mussels virtually ideal for pollution monitoring. In this study, Korean mussels (Mytilus coruscus) were collected from nine different sites situated along the coasts of the western sea to the eastern sea of Korea in 2017. Total mercury concentration was highest (mean ${\pm}$ standard error, $92.7{\pm}3.5ng/g\;dry$) on Baengnyeongdo Island in the western sea, and the sites in the southern sea showed the lowest mean concentrations (42.3 - 44.5 ng/g dry). These results were discussed in terms of possible pollution sources.

Paraffin-Based Phase Change Materials for Solar Reflective Paints Applications (파라핀 기반 상변화 물질을 이용한 태양광 반사 페인트 개발에 관한 연구)

  • Adnin Raihana Jannat;Soumen Mandal;Lee, Han Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2023.11a
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    • pp.67-68
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    • 2023
  • This paper reports on the synthesis of paraffin-based phase change materials (PCMs) designed for use in solar reflective paint (SRP) as a thermal energy storage (TES) medium. These PCMs are prepared using the sol-gel process and are encapsulated in silica. The focus of this research is to evaluate the suitability of these synthesized PCMs for efficient thermal energy storage within SRP applications. The obtained PCMs have nanometric dimensions, which make them well-suited for integration into paint formulations. The study also includes a thorough analysis of the chemical, thermal, and structural stabilities of these materials, confirming their applicability in solar reflective paint.

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Sensory Characteristics of Different Types of Commercial Soy Sauce (제조방법이 다양한 시판 재래 및 양조 간장의 관능적 특성)

  • Lee, Da-Yeon;Chung, Seo-Jin;Kim, Kwang-Ok
    • Journal of the Korean Society of Food Culture
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    • v.28 no.6
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    • pp.640-650
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    • 2013
  • Soy sauce, a basic ingredient in Asian cuisine, is made of fermented soybeans, salt, water, and barley or wheat flour. The sensory characteristics of soy sauce are not only determined through its main ingredients but also by various flavor compounds produced during the fermentation process. This study was conducted to identify the sensory attributes of five different commercial soy sauce samples that differ in Meju types (traditional Meju or modified Meju) and usage types. Thirty three sensory attributes, including appearance (1), odor (16), flavor (14), and mouthfeel (2) attributes, were generated and evaluated by eight trained panelists. The collected data were analyzed by analysis of variance and principal component analysis. There were significant differences in the intensities of all sensory attributes among the soy sauce samples. Soy sauce made with traditional Meju had high intensity of fermented fish, beany, musty odors and salt, Cheonggukjang, fermented fish flavors. Whereas two soy sauces made with modified Meju were strong in alcohol, sweet, Doenjang, roasted soybean flavors. Two soy sauces for soup made with modified Meju had medium levels of briny, sulfury, fermented odors and bitter, chemical flavors and biting mouthfeel characteristic.

Molecular Analysis of the Microorganisms in a Thermophilic CSTR used for Continuous Biohydrogen Production (연속수소생성에 사용되는 고온 CSTR 내의 미생물의 분자적 분석)

  • Oh, You-Kwan;Park, Sung-Hoon;Ahn, Yeong-Hee
    • KSBB Journal
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    • v.20 no.6
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    • pp.431-437
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    • 2005
  • Molecular methods were employed to investigate microorganisms in a thermophilic continuous stirred tank reactor(CSTR) used for continuous $H_2$ production. The reactor was inoculated with heat-treated anaerobic sludge and fed with a glucose-based medium. Denaturing gradient gel electrophoresis showed dynamic changes of bacterial populations in the reactor during 43 days of operation. Gas composition was constant from approximately 14 days but population shift still occurred. Populations affiliated with Fervidobactrium gondwanens and Thermoanaerobacterium thermosaccharolyticum were dominant on 21 and 41 days, respectively. Keeping pH of the medium at 5.0 could suppress methanogenic activity that was detected during initial operation period. $CH_4$ and mcrA detected in the samples obtained from the reactor or inoculum suggested the heat treatment condition employed in this study is not enough to remove methanogens in the inoculum. PCR using primer sets specific to 4 main orders of methanogens suggested that major $H_2$-consuming methanogens in the CSTR belong to the order Methanobacteriales.

Comparable Electron Capture Efficiencies for Various Protonated Sites on the 3rd Generation Poly(Propylene Imine) Dendrimer Ions: Applications by SORI-CAD and Electron Capture Dissociation Mass Spectrometry (ECD MS)

  • Han, Sang-Yun;Lee, Sun-Young;Oh, Han-Bin
    • Bulletin of the Korean Chemical Society
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    • v.26 no.5
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    • pp.740-746
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    • 2005
  • In this article, we report the tandem mass spectrometry investigations for the electron capture efficiencies of the protons belonging to the different locations (generations) in a poly(propylene imine) dendrimer with three layers of a repeat unit (named as the third generation dendrimer). The employed tandem mass spectrometry methods include SORI-CAD (sustained off-resonance irradiation collisional activation dissociation) and ECD(electron capture dissociation) mass spectrometry. We obtained SORI-CAD spectra for the dendrimer ions in the different charge states, ranging from 2+ to 4+. The analysis of fragmentation sites provides the information as to where the protons are distributed among various generations of the dendrimer. Based upon this, a new strategy to study the electron capture efficiencies of the protons is utilized to examine a new type of triplycharged ions by SORI-CAD, i.e., the 3+ ions generated from the charge reduction of the native 4+ ions by ECD: (M+4H)$^{4+}\;+\;e^-\;{\rightarrow}$ (M+4H)$^{3+\bullet}$ ${\rightarrow}\;({H^{\bullet}}_{ejected}$) + (M+3H)$^{3+}\;\rightarrow$ CAD. Interestingly, comparison of these four SORICAD spectra indicates that the proton distribution in the charge-reduced 3+ ions is very close to that in the native 4+ ions. It further suggests that in this synthetic polymer ($\sim$1.7 kDa) with an artificial architecture, the electron capture efficiencies of the protons are actually insensitive to where they are located in the molecule. This is somewhat contradictory to common expectations that the protons in the inner generations may not be well exposed to the incoming electron irradiation as much as the outer ones are, thus may be less efficient for electron capture. This finding may carry some implications for the case of medium sized peptide ions with similar masses, which are known to show no obvious site-specific fragmentations in ECD MS.