• Title/Summary/Keyword: Mechanical testing

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Nanocrystallization of Cu-Based Bulk Glassy Alloys upon Annealing

  • Pengjun, Cao;Dong, Jiling;Haidong, Wu;Peigeng, Fan;Anruo, Zhou
    • Applied Microscopy
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    • v.46 no.1
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    • pp.32-36
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    • 2016
  • The Cu-based bulk glassy alloys in Cu-Zr-Ti-Ni systems were prepared by means of copper mold casting. The Cu-based bulk glassy alloys samples were tested by X-ray diffractomer (XRD), differential scanning calorimeter, scanning electron microscopy (SEM), Instron testing machine and Vickers hardness instruments. The result indicated that the prepared Cu-Zr-Ti-Ni alloys were bulk glassy alloys. The temperature interval of supercooled liquid region (${\Delta}T_x$) was about 45.48 to 70.98 K for the Cu-Zr-Ti-Ni alloy. The Vickers hardness was up to 565 HV for the $Cu_{50}Zr_{25}Ti_{15}Ni_{10}$ bulk glassy alloy. The $Cu_{50}Zr_{25}Ti_{15}Ni_{10}$ bulk glassy alloys were annealed in order to obtain nanocrystals. The results showed that the Vickers hardness was raise up to 630 HV from 565 HV. As shown in XRD results, the amorphous alloys changed to nanocrystals, which were $Cu_8Zr_3$, $Cu_3Ti_2$ and CuZr, improved the hardness. The SEM analysis showed that the compression fractured morphology of amorphous alloys was brittle fracture, and the fracture morphology after annealing was ductile fracture. This proved that annealing of amorphous to nanocrystals can improve the plasticity and toughness of amorphous alloys.

A Case Study on the Slope Revegetation Technology of Biological Engineering Using the Ligustrum obtusifolium (쥐똥나무를 이용한 생물공학적 비탈면 녹화공법의 사례연구)

  • Kim, Hyea-Ju;Kang, Hyo-Suk
    • Journal of the Korean Society of Environmental Restoration Technology
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    • v.2 no.3
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    • pp.47-53
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    • 1999
  • This study was carried out to suggest the slope revegetation technology of biological engineering using the Ligustrum obtusifolium, which is one of the pioneer plant species. Ahead of the experimental construction, we evaluated the L. obtusifolium's value of biological engineering for the slope stabilization by testing the growth rate after the cuttings were buried for 8 weeks('98. 7. ~ '98. 9.). In this test, it was found that the L. obtusifolium, one of the species deep rooted with developed underground parts, is very effective for the slope stabilization and that the rooting powder(Hormex Powder) gave the better effects on root germination. In April of 1999, the experimental construction of biological engineering technology using recycled L. obtusifolium live cuttings(applied growth-stimulating compound) and green bags was conducted at sandy cut-slope in GLEN ROSS G.C.(Yongin). The slope was tolerant of soil erosion despite of heavy rainfall in the rainy season and many plant species invading for five months('99. 4. ~ '99. 9.). The vegetation research was performed through examining the frequency of each block using the transect method. 21 kinds of plant speices appeared in total area($25.5m^2$) and the dominant species are Digitaria sanguinalis, Setaria viridis, Cyperus amuricus, Persicaria blumei, Artemisia princeps var. orientalis. With regard to life forms, therophytes were shown with a dominant distribution of 66.7% of total species and neophytes relatively with a low distribution of 19.0%. Furthermore, it can be estimated that there is no ecological stabilization of this slope with the result of the ruderal species' occupation of 71.4%. It is too early to argue about ecological mechanical advantages and disadvantages of this technology, but, from the result of this study, it is expected that the slope revegetation technology of biological engineering using L. obtusifolium can be effectively applied to sandy slope(not rock or weathered rock slope) and that the early rapid stabilization and favorable succession could be done with the improvement of soil condition.

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The Influence of Transformational Leadership on Unethical Pro-Organizational Behavior-Mediating Effect of Organizational Identification (변혁적 리더십이 비윤리적 친조직 행동에 미치는 영향 -조직 동일시의 매개 효과)

  • Lee, Kang-Min;Choo, Shi-Gak;Jeon, Sang-Gil
    • Journal of Digital Convergence
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    • v.14 no.2
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    • pp.83-98
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    • 2016
  • This study attempted to test not only the influence of transformational leadership(TFL) on employees' unethical pro-organizational behavior(UPB), but also the mediating effect of organizational identification(OID) between TFL and employees' UPB. This study employed two research methods: literature review and empirical testing of the developed hypotheses. Data were collected through online questionnaire instruments from 229 employees working at companies in Korea. To test the hypotheses, structural equation modeling was employed. The model is shown as adequately fitting to the data. The results showed that there was not a positive and statistically significant relationship between TFL and employees' UPB, and OID played as a mediator in the relationship between TFL and employees' UPB. These findings provide a meaningful implication that the positive impact of TFL is linked to employees' UPB through OID.

Analysis of the Relationship between Unconfined Compression Strength and Shear Strength of Frozen Soils (동결토의 일축압축강도와 전단강도 상관관계 분석에 관한 연구)

  • Kang, Jae-Mo;Lee, Jang-Guen;Lee, Joonyong;Kim, YoungSeok
    • Journal of the Korean Geosynthetics Society
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    • v.12 no.3
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    • pp.23-29
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    • 2013
  • The mechanical behavior of frozen soils is different from that of unfrozen soils due to the phase change between water and ice. The strength characteristics of frozen soils are governed by the intrinsic material properties such as grain size, ice and water content, air bubbles, and by externally imposed testing conditions such as temperature, freezing time, and strain rate. Especially, the strength of the frozen soils is generally higher than that of unfrozen soils due to ice binding capacity with soil particles, and is strongly affected by a highly complex interaction between the solid soil skeleton and the pore matrix, composed of ice and unfrozen water. In this study, the direct shear test and unconfined compression test are carried out inside of a large-scaled freezing chamber, and the relationships between cohesion and unconfined compression strength under various freezing temperature conditions are discussed.

THE EFFECT OF SIZE AND SHAPE OF RETENTION ELEMENT ON COMPOSITE TO METAL BOND STRENGTH (유지요소의 크기와 형태가 간접복합레진과 금속간의 결합강도에 미치는 영향)

  • Lee, Yun-Jung;Jeon, Young-Chan;Jeong, Chang-Mo
    • The Journal of Korean Academy of Prosthodontics
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    • v.45 no.5
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    • pp.665-674
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    • 2007
  • Purpose: The purpose of this study was to investigate the effect of sire and shape of retention element on the bond strength of indirect composite resin and metal. Material and method: The metal disk specimens, each 6mm in diameter, were cast from CrCo alloy. They were divided into 8 groups by applied retention element. retention bead group $B2\;({\phi}\;0.2mm),\;B4\;({\phi}\;0.4mm),\;B6\;({\phi}\;0.6mm),\;B8\;({\phi}\;0.8mm)$, retention crystal group C2 (0.2mm), C5 (0.5mm), C8 (0.8mm) and sandblasting group SB ($110{\mu}m\;Al_2O_3$ blasting) as control. Eighty-eight metal specimens were veneered with $TESCERA^{(R)}$ Indirect resin system. One specimen of each group was sectioned and the resin-metal bonding pattern at the interface was observed under measuring microscope. Other specimens were then tested for tensile bond strength on an Instron universal testing machine at a crosshead speed of 2mm/min. Results: 1. Compared to sandblasting, beads or crystals increased the resin-metal bond strength (P<.05). 2. 0.2mm retention crystals were most effective in improving the resin-metal bond strength (P>.05). 3. 0.2mm beads showed the highest bond strength among retention bead groups, but there was no statistically significant difference (P>.05). 4. Retention crystals tend to be higher in bond strength than retention beads due to wider surface area. 5. The larger retention element, the larger the undercut for the mechanical retention, but the gap at resin-metal interface was also increased. Conclusion: Within the limitations of this study, 0.2mm retention crystals were most effective in improving the resin-metal bond strength.

Comparison of bond strength between denture base resin and reline resin (의치상 레진과 이장 레진 간의 결합강도 비교)

  • Geum, Young-Hee;Kim, Busob
    • Journal of Technologic Dentistry
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    • v.39 no.3
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    • pp.161-167
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    • 2017
  • Purpose: We compare the bond strength of heat-cured PMMA of Lucitone 199 and QC-20 and Tokuyama Rebase Resin of self-cured resin, which are widely used and well accepted in clinical practice. In order to test the mechanical bonding and chemical bonding, we will compare the bond strength between EstheShot Bright, Smiletone, Repair and Rebase resins. Methods: The denture base resin used in this study was PMMA heat-cured QC-20 and Lucitone 199, polyamide resin EstheShot Bright, Smiletone. And Two types of self-curing Rapid Repair and Tokuyama Rebase were used as resection resins. To measure the bond strength, the denture specimens were fabricated in the size of $10{\times}64{\times}3.5mm$ as instructed by the manufacturer. A surface treatment agent was applied to the cut surfaces of each denture specimen, and the specimens were placed in a preformed silicone mold, and autoclaved excimer resins were prepared. The bending strength of the fabricated specimens was measured using a universal testing machine (STM-5, United Calibration Co., U.S.A.) to measure the three-point bending strength. Results: In both polycarbonate and polyacetal resin, a special resin surface treatment agent showed higher bonding strength than the resin surface treatment agent(p<0.05). Regardless of the type of surface treatment, polycarbonate showed higher bond strength than polyacetal resin(p<0.05). Conclusion: It is considered desirable to use a special surface treating agent for the thermoplastic denture base resin such as polycarbonate and polyacetal resin.

New approaches to testing and evaluating the impact capability of coal seam with hard roof and/or floor in coal mines

  • Tan, Y.L.;Liu, X.S.;Shen, B.;Ning, J.G.;Gu, Q.H.
    • Geomechanics and Engineering
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    • v.14 no.4
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    • pp.367-376
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    • 2018
  • Samples composed of coal and rock show different mechanical properties of the pure coal or rock mass. For the same coal seam with different surrounding rocks, the frequency and intensity of rock burst can be significantly different in. First, a method of measuring the strain variation of coal in the coal-rock combined sample was proposed. Second, laboratory tests have been conducted to investigate the influences of rock lithologies, combined forms and coal-rock height ratios on the deformation and failure characteristics of the coal section using this method. Third, a new bursting liability index named combined coal-rock impact energy speed index (CRIES) was proposed. This index considers not only the time effect of energy, but also the influence of surrounding rocks. At last, a new approach considering the influences of roof and/or floor was proposed to evaluate the impact capability of coal seam. Results show that the strength and elastic modulus of coal section increase significantly with the coal-rock height ratio decreasing. In addition, the values of bursting liability indexes of the same coal seam vary greatly when using the new approach. This study not only provides a new approach to measuring the strain of the coal section in coal-rock combined sample, but also improves the evaluation system for evaluating the impact capability of coal.

Synthesis and Characterization of Waterborne Polyurethanes Based on Isophorone Diisocyanate and Mixed Polyols of Poly(tetramethylene glycol)/Polydimethylsiloxane Diol (이소포론 디이소시아네이트와 폴리(테트라메틸렌 글리콜)/폴리디메틸실록산 디올 혼합 폴리올을 사용한 수분산성 폴리우레탄의 합성과 특성 분석)

  • Lee, Ji Hye;Hong, Seongdon;Kim, Young Ho
    • Polymer(Korea)
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    • v.37 no.2
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    • pp.167-176
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    • 2013
  • Linear and cross-linked waterborne polyurethanes (WPUs) based on isophorone diisocyanate and mixed diols of poly(tetramethylene glycol)/hydroxyethyl-terminated polydimethylsiloxane (PDMS-OH) were synthesized with dimethylol propionic acid as an anionic component, trimethylolpropane as a cross-linking agent, and butanediol as a chain extender and characterized. The hydrophobicity, $T_g$, stress-strain behaviors of the linear or cross-linked siloxane-containing WPU (WPU-Si) films with different PDMS content were analyzed by using water contact shape analyzer, energy dispersive spectrometer, dynamic mechanical analyzer, and universal testing machine. The results reveal that as the PDMS content increased, the hydrophobicity of WPU-Si films increased, $T_g$ moved to higher temperature, the breaking stress increased, and the breaking strain decreased.

ANALYSIS OF THE OPTIMIZED H TYPE GRID SPRING BY A CHARACTERIZATION TEST AND THE FINITE ELEMENT METHOD UNDER THE IN-GRID BOUNDARY CONDITION

  • Yoon Kyung-Ho;Lee Kang-Hee;Kang Heung-Seok;Song Kee-Nam
    • Nuclear Engineering and Technology
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    • v.38 no.4
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    • pp.375-382
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    • 2006
  • Characterization tests (load vs. displacement curve) are conducted for the springs of Zirconium alloy spacer grids for an advanced LWR fuel assembly. Twofold testing is employed: strap-based and assembly-based tests. The assembly-based test satisfies the in situ boundary conditions of the spring within the grid assembly. The aim of the characterization test via the aforementioned two methods is to establish an appropriate assembly-based test method that fulfills the actual boundary conditions. A characterization test under the spacer grid assembly boundary condition is also conducted to investigate the actual behavior of the spring in the core. The stiffness of the characteristic curve is smaller than that of the strap-wised boundary condition. This phenomenon may cause the strap slit condition. A spacer grid consists of horizontal and vertical straps. The strap slit positions are differentiated from each other. They affords examination of the variation of the external load distribution in the grid spring. Localized legions of high stress and their values are analyzed, as they may be affected by the spring shape. Through a comparison of the results of the test and FE analysis, it is concluded that the present assembly-based analysis model and procedure are reasonably well conducted and can be used for spring characterization in the core. Guidelines for improving the mechanical integrity of the spring are also discussed.

Studies on the Oxygen Permeability and It's Proofness of the Various Commercial Polymer Films (상업용 고분자 필름의 산소투과도 및 산소투과 방지도에 관한 연구)

  • Suh, Hwan-Kyu;Kim, Joon-Soo;Lee, Jung-Keun
    • Elastomers and Composites
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    • v.15 no.1
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    • pp.3-9
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    • 1980
  • The oxygen permeability and it's proofness of te various commercial polymer films have been investigated at the constant pressure and temperature. Oxygen proofness, the reciprocals of the oxygen permeability for the various samples, were determined by means of a coulometric oxygen permeability tester. The testing of sample films was performed at constant temperature $(23{\pm}1^{\circ}C)$ under 1 atm. for 24 hours. The order of the relative proofness observed are as follows; oriented Nylon (O. Nylon)> oriented Polyester (O. PET)>nonoriented Nylon (N. Nylon)>nonoriented Polyester (N.PET)> rigid Polyvinyl chloride (Rigid PVC)>semirigid Polyvinyl chloride (Semirigid PVC)> oriented Polypropylene (O. PP)>plasticized Polyvinyl chloride (P. PVC)> casted Polypropylene (C. PP)> low density Polyethylene (LDPE)>high density Polyethylene (HDPE, Inflation)> high density-polyethylene (HDPE, T-die) The oxygen proofness of the films was increased with the polarity cf polymer, the film thickness and mechanical orientation and decreased with the addition of plasticizer in PVC. For the use of wrapping materials, one film with the polar property in the main chain of the polymer molecule and the others with nonpolar property in it are laminated for the protection from oxygen and moisture.

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