• 한국자기학회지
• /
• 제11권4호
• /
• pp.168-172
• /
• 2001

Sol-gel법을 이용하여 Co$_{0.9}$Zn$_{0.1}$Fe$_2$O$_4$ 박막을 제조하였다. 성장한 박막의 구조 및 자기적 성질에 관하여 x선 회절분석기 (XRD), atomic force microscopy(AFM) 및 Auger electron spectroscopy(AES), 진동시료자화측정기 (VSM)을 이용하였다. Co-Zn 페라이트 박막의 경우, 400 $^{\circ}C$ 이상의 열처리 온도에서 단일상의 spinel 구조만을 가지고 있으며, 아무런 방향성이 없이 성장함을 나타내고 있다. 열처리 온도가 600 $^{\circ}C$ 이하에서 성장된 박막 표면의 거칠기는 3 nm 이하였으며, 형성된 입자의 크기는 약 40nm이하임을 알 수 있었다. 또한, 40$0^{\circ}C$에서 열처리한 경우 기판에서 Si이 Co-Zn 페라이트 박막내로 확산이 거의 나타나지 않았으나, 870 $^{\circ}C$에서 열처리한 경우 계면에서 기판과 박막의 상호 확산을 확인할 수 있었다. 제작한 박막은 외부 자기장의 방향과는 무관한 등방성의 자기적 특성을 보이며, 최대 보자력은 600 $^{\circ}C$에선 열처리한 자성박막이 약 1,900 Oe을 가짐을 알 수 있었다.있었다.

• The Journal of Advanced Prosthodontics
• /
• 제9권5호
• /
• pp.335-340
• /
• 2017

PURPOSE. Bacterial adhesion on provisional crown materials retained for a long time can influence the duration for which permanent prosthetic restorations can be healthily worn in the oral cavity. The aim of this study was to compare seven different commonly used provisional crown materials with regard to Streptococcus mutans and Candida albicans surface adhesion. MATERIALS AND METHODS. For each group, twenty specimens of the provisional fixed prosthodontic materials TemDent ($Sch{\ddot{u}}tz$), Imident (Imicryl), Tab 2000 (Kerr), Structur Premium (Voco), Systemp (Ivoclar Vivadent), Acrytemp (Zhermack), and Takilon-BBF (Takilon) were prepared (diameter, 10.0 mm; height, 2.0 mm). Surface roughness was assessed by atomic force microscopy. Each group was then divided into 2 subgroups (n=10) according to the microbial suspensions used: S. mutans and C. albicans. The specimens were incubated at $37^{\circ}C$ with S. mutans or C. albicans for seven days. Bacterial adherence on surfaces was assessed using the 2,3-bis[2-methyloxy-4-nitro-5-sulfophenyl]-2H-tetrazolium-5-carboxanilide (XTT) assay. RESULTS. S. mutans showed maximum adhesion to Structur, followed by Systemp, Acrytemp, Takilon, Tab 2000, Imident, and TemDent (P<.05). The highest vital C. albicans adhesion was noted on Takilon, followed by Imident and Tab 2000; the lowest adhesion was noted on Systemp (P<.05). CONCLUSION. The materials showed significant differences in the degree of bacterial adhesion. C. albicans showed higher surface adhesion than S. mutans on provisional crown and fixed partial denture denture materials.

• Korean Chemical Engineering Research
• /
• 제56권3호
• /
• pp.327-334
• /
• 2018

출발물질로서 테트라에톡시실란(TEOS)과 메틸트리메톡시실란(MTMS)을 사용하여 졸-겔법에 의해 발수성 코팅용액을 제조하였다. 이 용액을 냉연강판 위에 스핀 코팅하고 열처리하여 비불소계 발수 코팅 도막을 제조 하였다. 이 과정 중 MTMS/TEOS의 몰 비, 물 농도 및 암모니아 농도가 코팅 도막의 발수성에 미치는 영향을 연구하였다. MTMS/TEOS의 몰 비를 1~20으로 변화시켜 제조 한 코팅 도막의 접촉각은 MTMS/TEOS 몰 비가 10 일 때 최대 수치인 $108^{\circ}$를 나타내었다. 반면에 물의 첨가량을 증가시킴에 따라 코팅 도막의 접촉각이 증가하여 발수성이 향상되었다. 또한 암모니아의 첨가량이 커질수록실리카입자의 크기가커져 실리카입자의표면 거칠기가증가하므로 발수성이 증가하였다.

• 대한치과보철학회지
• /
• 제39권6호
• /
• pp.682-697
• /
• 2001

This investigation evaluated the fracture toughness($K_{IC}$) of eight currently available core materials, and relate the fracture toughness value to fractography analysis and surface characteristics using a atomic force microscope (AFM). Single-edge notched (SEN) test specimens (n=10) and compact tension (CT) test specimens (n=10) were prepared conforming to the ASTM Standard E-399 for a high copper amalgam, three composite core materials (Core-Max II, Core Paste, Bisfil Core), two reinforced composite core materials (Ti-Core, Ti-Core Natural), a resin-modified glass ionomer core material (Vitremer), and a conventional glass ionomer core material (Ketac-Molar). The specimens were tested with an Instron Universal Testing Machine. The maximum loads were measured to calculate the fracture toughness ($K_{IC}$). Thereafter, fracture surfaces of SEN specimens of each material were investigated for fractography analysis using scanning electron microscope. And, disc-shaped specimens with 1mm thickness were fabricated for each material and were investigated under AFM for surface morphology analysis. The results were as follows: 1. Bisfil Core showed the highest mean fracture toughness regardless of test methods. 2. For the tooth-colored materials, Ti-Core Natural exhibited the highest fracture toughness. 3. Ketac Molar showed a significantly low fracture toughness when compared with the amalgam and the composite resin core materials(p<0.05). 4. The fracture toughness values obtained with the single-edge notched test, except Ketac Molar, were higher than those obtained in the compact tension test. 5. SEM revealed that the fracture surface of high fracture toughness material was rougher than that of low fracture toughness material. 6. AFM revealed that the surface particles of the composite resins were smaller in size, with a lower surface roughness than the glass ionomer core materials.

• 한국기계가공학회지
• /
• 제14권3호
• /
• pp.50-56
• /
• 2015

In this study, AISI M2 powder was selected primarily through various pieces of literature in order to improve the hardness and wear resistance. Among the laser metal deposition parameters, laser power was studied to improve the deposition efficiency in the laser metal deposition using a diode-pumped disk laser. An SKD61 hot work steel plate and AISI M2 powder were used as a substrate and powder for laser metal deposition, respectively. Experiments for the laser metal deposition were carried out by changing the laser power and track layer. The quality of the track surface and cross-section after applying the single-layer method was better than that obtained from applying the multi-layer method. As the laser power increased, the track thickness was increased, and the surface roughness deviation was decreased. In laser power condition of 1.6kW, the maximum hardness of the deposition track was 790Hv. This value was 40% better than the hardness of the SKD61 after heat treatment.

• 한국의류산업학회지
• /
• 제17권6호
• /
• pp.1020-1029
• /
• 2015

This paper investigated the wearing performance of knitted fabrics made of air vortex yarns using PTT/tencel/cotton fibres in comparison with ring and compact yarns for emotional garment. Wicking property of knitted fabric made of MVS yarns was worse than those by ring and compact yarns, however, drying property of knitted fabric made of MVS yarns was better than those by ring and compact yarns, which was explained as more water vapor transport due to larger openness between fibres in the MVS yarns than those in the ring and compact yarns. Thermal conductivity of knitted fabric made of MVS was lower than those of ring and compact yarns and maximum heat flow(Q_max) at the transient state of MVS knitted fabric was lower than those of ring and compact yarns, which may be attributed to MVS yarn structure that has parallel fibres in the core part of the yarn and fasciated fibre bundles on the sheath part with roughness on the yarn surface. However, pilling of MVS knitted fabric was better than those by ring and compact yarns, which was caused by less and shorter hairy fibres protruded from MVS yarn surface than those of ring and compact yarns. It was observed that tactile hand of MVS yarn knitted fabrics was stiffer than those of ring and compact yarns knitted fabrics. It was explained by low extensibility and compressibility and high bending and shear rigidities of the MVS yarn knitted fabrics, which resulted in bad wearing performance of MVS knitted fabric.

• 한국의류산업학회지
• /
• 제14권3호
• /
• pp.486-491
• /
• 2012

This study examined the sound characteristics of Taekwondo uniform fabrics to investigate the relationship between the sound parameters and the mechanical properties of the fabric as well as to provide the conditions to maximize the frictional sound of the uniform. Frictional sounds of 6 fabrics for Taekwondo uniforms were generated by the Simulator for Frictional Sound of Fabrics. The frictional speeds were controlled at low(0.62 m/s), at mid(1.21 m/s) and at high(2.25 m/s) speed, respectively. The frictional sounds were recorded using a Data Recorder and Sound Quality System subsequently, the physical sound properties such as SPL(Sound Pressure Level) and Zwicker's psychoacoustic parameters were calculated. Mechanical properties of specimens were measured by KES-FB. The SPL, Loudness(Z) values increased while Sharpness(Z) value decreased. In the physical sound parameter, specimen E had the highest SPL value at low speed and specimen B at high speed. In case of Zwicker's psychoacoustic parameters, the commercially available Taekwondo uniform fabrics(E, F) showed higher values of Loudness(Z), Sharpness(Z), and Roughness(Z), that indicates they can produce louder, shaper and rougher sounds than other fabrics for Taekwondo uniforms. The decisive factors that affected frictional sounds for Taekwondo uniforms were W(weight) as well as EM(elongation at maximum load) at low speed and WC(compressional energy) at high speed.

• Membrane and Water Treatment
• /
• 제6권5호
• /
• pp.423-437
• /
• 2015

Polyvinylidene fluoride/fullerene nanoparticle (PVDF/$C_{60}$) composite microfiltration (MF) membranes were fabricated by a non-solvent induced phase separation (NIPS) using N, N-dimethylacetamide (DMAc) as solvent and deionized water (DI) as coagulation solution. Polyvinylpyrrolidone (PVP) was added to the casting solution to form membrane pores. $C_{60}$ was added in increments of 0.2% from 0.0% to 1.0% to produce six different membrane types: one pristine PVDF membrane type with no $C_{60}$ added as control, and five composite membrane types with varying $C_{60}$ concentrations of 0.2, 0.4, 0.6, 0.8 and 1.0%, respectively. The mechanical strength, morphology, pore size and distribution, hydrophilicity, surface property, permeation performance, and fouling resistance of the six membranes types were characterized using respective analytical methods. The results indicate that membranes containing $C_{60}$ have higher surface porosity and pore density than the pristine membrane. The presence of numerous pores on the membrane caused weaker mechanical strength, but the water flux of the composite membranes increased in spite of their smaller size. Initial flux and surface roughness reached the maximum point among the composite membranes when the $C_{60}$ concentration was 0.6 wt.%.

• 마이크로전자및패키징학회지
• /
• 제23권4호
• /
• pp.101-105
• /
• 2016

최근 자연모방을 이용한 소수성 표면 가공이 많은 관심을 끌고 있다. 대표적인 가공 방법으로 기계적 가공, 포토리소그래피 가공, 레이저를 이용한 공정이 있다. 본 논문에서는 구리필름에 UV 펄스 레이저를 직접 조사해 마이크로 그루브를 형성하고 상온에서의 산화를 통해 표면의 거칠기를 증가시켜 소수성 표면을 제작하였다. 패턴 생성 뒤 일정 시간 산화를 시킨 후에 측정된 접촉각은 산화를 시키기 전보다 약 $30{\sim}70^{\circ}$까지 증가함을 보인다. 본 연구 결과를 통해서 화학적인 처리과정 없이 보다 안정한 소수성 표면을 제조할 수 있음을 확인하였다.

• 한국방재안전학회논문집
• /
• 제6권2호
• /
• pp.1-8
• /
• 2013

우리나라 전체 재해 60%이상인 태풍과 같은 바람재난으로부터 구조물이나 외장재가 안전과 사용성 측면에서 설계되려면 내풍설계과정에서 기본풍속, 설계속도압, 풍하중 등 많은 파라미터들이 요구된다. 본 논문에서는 최근 2003년부터 2012년까지의 10년 동안 년최대풍속이 발생한 날의 풍속으로부터 확률과정과 확률분포, 통계적 성질 등을 알아보기 위하여 8개의 대표지점을 여수, 인천, 서울, 청주, 원주, 대구, 속초, 울릉도로 선정했다. 선정된 각 지점에 대한 최근 10년 동안의 풍속자료는 기상청으로부터 획득했다. 각 지점의 획득한 풍속자료는 우리나라를 직접 통과하면서 영향을 미친 태풍과 통과는 안했지만 간접 영향을 미친 태풍, 년최대순간풍속과 년최대평균퐁속이 같은 날 등을 고려 90개의 앙상블 중 선별된 33개의 모집단에 대한 풍속자료의 확률과정 및 확률분포의 특성을 비교 검토하였다.