• 한국표면공학회지
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• 제53권2호
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• pp.59-66
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• 2020

Effects of Na₂SiO₃ concentration added into 0.1 M NaOH + 0.05 M NaF solution on the formation behavior and properties of PEO films on AZ91 Mg alloy were investigated under 1200 Hz of alternating current (AC) by voltage-time curves, in-situ observation of arc generation behavior and measurements of film thickness, surface roughness and micro vickers hardness. In the absence of Na₂SiO₃ in the 0.1 M NaOH + 0.05 M NaF solution, about 4 ㎛ thick PEO film was formed within 1 min and then PEO film did not grow but white spots were formed by local burning. Addition of Na₂SiO₃ up to 0.2 M caused more increased formation voltage and growth of PEO film with uniform generation of arcs. Addition of Na₂SiO₃ from 0.2 M to 0.4 M showed nearly the same voltage-time behavior and uniform arc generation. Addition of Na₂SiO₃ more than 0.5 M resulted in a decrease of formation voltage and non-uniform arc generation due to local burning. PEO film growth rate increased with increasing added Na₂SiO₃ concentration but maximum PEO film thickness was limited by local burning if added Na₂SiO₃ concentration is higher than 0.5 M. Surface roughness of PEO film increased with increasing added Na₂SiO₃ concentration and appeared to be proportional to the PEO film thickness. PEO film hardness increased with increasing added Na₂SiO₃ concentration and reached a steady-state value of about 930 H_V at more than 0.5 M of added Na₂SiO₃ concentration.

• 한국결정성장학회지
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• 제15권6호
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• pp.234-238
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• 2005

[ $Cl_2/Ar$ ] 유도결합 플라즈마(ICP)내의 플라즈마 조성, 이온 flux 및 이온 에너지가 $La_3Ga_5SiO_{14}$ 단결정 wafer의 식각속도, 표면 양상 및 화학량론적 조성에 미치는 영향을 조사하였다. 비교적 높은 ICP source power$({\sim}1000W)$ 또는 높은 $Cl_2$ gas 유량 비율 조건으로부터 최고 약 $1600{\AA}/min$의 실용적이고 조절이 용이한 식각속도를 확보하였다. 식각된 $La_3Ga_5SiO_{14}$ 표면은 식각 이전과 비슷하거나 더 낮은 표면 조도 특성을 나타내었으며 식각 공정 전, 후 표면의 화학량론적 조성에 있어서의 변화는 없는 것으로 조사되었다.

• 대한기계학회논문집A
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• 제34권5호
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• pp.651-657
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• 2010

180 bar 이상의 최대 폭발압과 높은 열부하를 가진 박용 디젤엔진의 분리형 피스톤은 크라운과 스커트를 각각 고강도 합금강과 연성주철을 사용한다. 피스톤의 피로설계를 위해서는 작용 하중, 표면조도 뿐만 아니라 온도영향에 의한 강도 저하를 고려해야 하며, 실린더 내부의 폭발력이 크라운을 거쳐 스커트에 전달되는 하중의 분율도 고려되어야 한다. 본 연구에서는 노치부의 피로강도 증분을 응력구배방법을 사용하여 고려하였으며, 열전달해석과 그에 따른 온도영향을 고려하였다. 하중 분율과 접촉압력은 공차해석을 통해 최적화하였으며, 프로타입 엔진에 대한 실차 시험을 통해 냉각 및 내구설계를 검증하였다.

• 한국정밀공학회지
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• 제30권6호
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• pp.589-595
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• 2013

Solution processed conjugated molecules enable to manufacture various electronic devices by unconventional and cost effective patterning methods as screen or gravure printing. Spin-coating is the most popularly used method to form conjugated polymeric film for various electronic devices. The coating method has certain disadvantages such as a large amount of unwanted wastes, difficulty forming a film with a large area, and impossible to apply roll-to-roll manufacturing. We present here a promising alternative coating method, bar-coating for conjugated polymer film and OLED with the bar coated light emitting layer. In this papers, we show atomic force microscope images of spin- and bar-coated Poly[(9,9-di-n-octylfluorenyl-2,7-diyl)-alt-(benzo[2,1,3]thiadiazol-4,8-diyl)] (F8BT) films on substrate. The bar-coated film showed a slight lower RMS roughness (1.058 [nm]) than spin-coated film (1.767 [nm]). It means the bar-coating is suitable method to form light emitting layers in OLEDs. By using bar-coating process, an OLED obtained with 4.7 [cd/A] in maximum current efficiency.

• International Journal of Industrial Entomology and Biomaterials
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• 제26권2호
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• pp.81-88
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• 2013

Wet-spun silk fibers have attracted the attention of many researchers because of 1) the unique properties of silk as a biomaterial, including good biocompatibility and cyto-compatability and 2) the various methods available to control the structure and properties of the fiber. Cellulose nanofibrils (CNFs) have typically been used as a reinforcing material for natural and synthetic polymers. In this study, CNF-embedded silk fibroin (SF) nanocomposite fibers were prepared for the first time. The effects of CNF content on the rheology of the dope solution and the characteristics of wet-spun CNF/SF composite fibers were also examined. A 5% SF formic acid solution that contained no CNFs showed nearly Newtonian fluid behavior, with slight shear thinning. However, after the addition of 1% CNFs, the viscosity of the dope solution increased significantly, and apparent shear thinning was observed. The maximum draw ratio of the CNF/SF composite fibers decreased as the CNF content increased. Interestingly, the crystallinity index for the silk in the CNF/SF fibers was sequentially reduced as the CNF content was increased. This phenomenon may be due to the fact that the CNFs prevent ${\beta}$-sheet crystallization of the SF by elimination of formic acid from the dope solution during the coagulation process. The CNF/SF composite fibers displayed a relatively smooth surface with stripes, at low magnification (${\times}500$). However, a rugged nanoscale surface was observed at high magnification (${\times}10,000$), and the surface roughness increased with the CNF content.

• 한국환경복원기술학회지
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• 제7권6호
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• pp.61-74
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• 2004

Hydraulic engineers and scientists working on river restoration recognize the need for a deeper understanding of natural streams as a complex and dynamic system, which involves not only abiotic elements(flow, sediments) but also biotic components. From this point of view, the role played by riverine vegetation dynamics and flow conditions becomes essential. Hydro-mechanic interaction between flow and flexible plants covering a river bed is studied in this paper and some previous works are discussed. Measurements of turbulence and flow resistance in vegetated open channel were performed using rigid and flexible tube. Measuring detailed turbulent velocity profiles within and above submerged and flexible stems allowed to distinguish different turbulent regimes. Some interesting relationships were obtained between the velocity field and the deflected height of the plants, such as a reduced drag coefficient in the flexible stems. Turbulent intensities and Reynolds stresses were measured showing two different regions : above and inside the vegetation domain. In flexible vegetated open channel, the maximum values of turbulent intensities and Reynolds stresses appear above the top of canopy. Method to predict a flow resistance in flexible vegetated open channel is developed by modifying an analytical model proposed by Klopstra et al. (1997). Calculated velocity profiles and roughness values correspond well with flume experiments. These confirm the applicability of the presented model for open channel with flexible vegetation. The new method will be verified in the real vegetated conditions in the near future. After these verifications, the new method should be applied for nature rehabilitation projects such as river restorations.

• 한국전기전자재료학회논문지
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• 제15권6호
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• pp.479-485
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• 2002

We have investigated the effects of various wafers cleaning on glass/Si bonding using 4 inch Pyrex glass wafers and 4 inch silicon wafers. The various wafer cleaning methods were examined; SPM(sulfuric-peroxide mixture, $H_2SO_4:H_2O_2$ = 4 : 1, $120^{\circ}C$), RCA(company name, $NH_4OH:H_2O_2:H_2O$ = 1 : 1 : 5, $80^{\circ}C$), and combinations of those. The best room temperature bonding result was achieved when wafers were cleaned by SPM followed by RCA cleaning. The minimum increase in surface roughness measured by AFM(atomic force microscope) confirmed such results. During successive heat treatments, the bonding strength was improved with increased annealing temperatures up to $400^{\circ}C$, but debonding was observed at $450^{\circ}C$. The difference in thermal expansion coefficients between glass and Si wafer led debonding. When annealed at fixed temperatures(300 and $400^{\circ}C$), bonding strength was enhanced until 28 hours, but then decreased for further anneal. To find the cause of decrease in bonding strength in excessively long annealing time, the ion distribution at Si surface was investigated using SIMS(secondary ion mass spectrometry). tons such as sodium, which had been existed only in glass before annealing, were found at Si surface for long annealed samples. Decrease in bonding strength can be caused by the diffused sodium ions to pass the glass/si interface. Therefore, maximum bonding strength can be achieved when the cleaning procedure and the ion concentrations at interface are optimized in glass/Si wafer direct bonding.

• 한국환경과학회지
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• 제17권2호
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• pp.195-201
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• 2008

Damage from typhoon disaster can be mitigated by grasping and dealing with the damage promptly for the regions in typhoon track. What is this work, a technique to analyzed dangerousness of typhoon should be presupposed. This study estimated 10 m level wind speed using 700 hPa wind by typhoon, referring to GPS dropwindsonde study of Franklin(2003). For 700 hPa wind, 30 km resolution data of Regional Data Assimilation Prediction System(RDAPS) were used. For roughness length in estimating wind of 10 m level, landuse data of USGS are employed. For 10 m level wind speed of Typhoon Rusa in 2002, we sampled AWS site of $7.4{\sim}30km$ distant from typhoon center and compare them with observational data. The results show that the 10 m level wind speed is the estimation of maximum wind speed which can appear in surface by typhoon and it cannot be compared with general hourly observational data. Wind load on domestic buildings relies on probability distributions of extreme wind speed. Hence, calculated 10 m level wind speed is useful for estimating the damage structure from typhoon.

• 한국정밀공학회지
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• 제19권6호
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• pp.176-183
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• 2002

Plasma Display Panel(PDP) is a type of flat panel display utilizing the light emission produced by gas discharge. Barrier Ribs of PDP separating each sub-pixel prevents optical and electrical crosstalks from adjacent sub-pixels. The mold for forming the barrier ribs has been newly researched to overcome the disadvantages of conventional manufacturing processes such as screen printing, sand-blasting and photosensitive glass methods. The mold for PDP barrier ribs have stripes of micro grooves transferring glass-material wall. In this paper , Stripes of grooves of which width 48$\mu$m, depth 124$\mu$m , pitch 274$\mu$m was acquired by machining of single crystal silicon with dicing saw blade. Maximum roughness of the bottom of the grooves was 59.6 nm Ra in grooving Si. Barrier ribs were farmed with silicone rubber mold, which is transferred from grooved Si forming hard mold. Silicone rubber mold has the elasticity, which enable to accommodate the waviness of lower glass plate of PDP. The methods assisted by the microwave and UV was adopted for reducing the forming time of glass paste.

• 한국재료학회지
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• 제26권4호
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• pp.207-211
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• 2016

Ti films were deposited on glass substrates under various preparation conditions in a chamber of two-facing-target type dc sputtering; after deposition, the electric resistivity values were measured using a conventional four-probe method. Crystallographic orientations and microstructures, including the texture and columnar structure, were also investigated for the Ti films. The morphological features, including the columnar structures and surface roughness, are well explained on the basis of Thornton's zone model. The electric resistivity and the thermal coefficient of the resistivity vary with the sputtering gas pressure. The minimum value of resistivity was around 0.4 Pa for both the $0.5{\mu}m$ and $3.0{\mu}m$ thick films; the apparent tendencies are almost the same for the two films, with a small difference in resistivity because of the different film thicknesses. The films deposited at high gas pressures show higher resistivities. The maximum of TCR is also around 0.4 Pa, which is the same as that obtained from the relationship between the resistivity and the gas pressure. The lattice spacing also decreases with increasing sputtering gas pressure for both the $0.5{\mu}m$ and $3.0{\mu}m$ thick films. Because they are strongly related to the sputtering gas pressures for Ti films that have a crystallographic anisotropy that is different from cubic symmetry, these changes are well explained on the basis of the film microstructures. It is shown that resistivity measurement can serve as a promising monitor for microstructures in sputtered Ti films.