• Title/Summary/Keyword: Material property test

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Evaluation of Adhesion and Electrical Properties of CNT/PU Topcoat with Different CNT Weight Fraction for Aircraft (탄소나노튜브의 함량에 따른 항공기용 탄소나노튜브/폴리우레탄 탑코트의 접착 및 전기적 특성 평가)

  • Kim, Jong-Hyun;Shin, Pyeong-Su;Kim, So-Yeon;Park, Joung-Man
    • Composites Research
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    • v.33 no.1
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    • pp.1-6
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    • 2020
  • Dispersion and electrical resistance (ER) properties of polyurethane (PU) type topcoat were evaluated using carbon nanotube (CNT) with different CNT weight fraction. CNT was dispersed in PU type topcoat using ultra sonication dispersion method. CNT/PU topcoat was coated on carbon fiber reinforced epoxy composite (CFRC) surface using gravity feed spraying method. Static contact angles of CFRC and CNT/PU topcoat were performed using 4 types of solvents to calculate the work of adhesion between CNT/PU topcoat and CFRC surface. Surface resistance of CNT added PU topcoat was measured to determine CNT dispersion. Adhesion property between CNT/PU topcoat and CFRC was determined via cross hatch cutting test based on ASTM D3359. The optimized condition of CNT weight fraction was found.

Physical Properties of Sulfur Concrete with Modified Sulfur Binder (유황개질 바인더를 사용한 유황 콘크리트의 물리적 특성)

  • Bae, Sung Geun;Gwon, Seong Woo;Kim, Se Won;Cha, Soo Won
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.34 no.3
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    • pp.763-771
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    • 2014
  • Recently, a huge amount of sulfur has been produced as a byproduct of petroleum refining processes in Korea. Sulfur concrete is made of modified sulfur binder instead of cement paste, which has advantages of reducing $CO_2$ emission from cement industry as well as utilizing surplus sulfur. Also, sulfur concrete is a sustainable material that can be repetitively recycled. In this study, the physical properties of sulfur concrete are experimentally investigated. From the test results, sulfur concrete showed compressive strengths higher than at least 50MPa. Also, the unit weight, modulus of elasticity and splitting tensile strength of sulfur concrete was similar to that of Portland cement concrete (PCC). The coefficient of thermal expansion of sulfur concrete was a little larger than that of Portland cement concrete and sulfur concrete with mineral filler is helpful to lower the coefficient of thermal expansion. recycled aggregate sulfur concrete resulted in a slight reduction in the compressive strength, but sulfur concrete with recycled aggregate can achieve the high strength characteristics.

Measurement of Dynamic Elastic Constants of RPV Steel Weld due to Localized Microstructural Variation (원자로 용접부의 국부적 미세조직 변화에 따른 동적탄성계수 측정)

  • Cheong, Yong-Moo;Kim, Joo-Hag;Hong, Jun-Hwa;Jung, Hyun-Kyu
    • Journal of the Korean Society for Nondestructive Testing
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    • v.20 no.5
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    • pp.390-396
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    • 2000
  • The dynamic elastic constants of the simulated weld HAZ (heat-affected zone) of SA 508 Class 3 reactor pressure vessel (RPV) steel were investigated by resonant ultrasound spectroscopy (RUS). The resonance frequencies of rectangular parallelepiped samples woe calculated from the initial estimates of elastic stiffness $c_{11},\;c_{12}\;and\;c_{44}$ with an assumption of isotropic property, dimension and density. Through the comparison of calculated resonant frequencies with the measured resonant frequencies by RUS, very accurate elastic constants of SA 508 Class 3 steel were determined by iteration and convergence processes. Clear differences of Youngs modulus and shear modulus were shown from samples with different thermal cycles and microstructures. Youngs modulus and shear modulus of samples with fine-grained bainite were higher than those with coarse-grained tempered martensite. This tendency was confirmed from other results such as micro-hardness test.

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The Effects of Hot Corrosion on the Creep Rupture Properties of Boiler Tube Material (보일러 管材料의 크리프破斷特性에 미치는 고온부식의 影響)

  • 오세욱;박인석;강상훈
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.13 no.2
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    • pp.236-242
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    • 1989
  • In order to investigate the effects of hot corrosion on the creep rupture properties and creep life of 304 stainless steel being used as tube materials of heavy oil fired boiler, the creep rupture tests were carried out at temperature 630.deg.C, 690.deg.C and 750.deg.C in static air for the specimens with or without coating of double layer corrosives according to the new hot corrosion test method simulating the situation commonly observed on superheater tubes of the actual boiler. The double layer corrosives are 85% V$_{2}$O$_{5}$ + 10% Na$_{2}$So$_{4}$ + 5% Fe$_{2}$O$_{3}$ as the inner layer corrosive being once melted at 900.deg. C and crushed to powder, and 10% V$_{2}$O$_{5}$ + 85% Na$_{2}$SO$_{4}$ +5% Fe$_{2}$O$_{3}$ as the outer layer corrosive. As results, in the specimen coated with the double layer corrosives, the rupture strength was extremely lowered and showed a large difference each other. The rupture ductility also lowered remarkably as a result of the brittle fracture mode due to hot corrosion. These results indicate that hot corrosion could essentially alter the creep fracture mechanism. From the metallographic observation, it was clarified that the rupture life of 304 stainless steel subjected to hot corrosion was chiefly determined by the behavior of the aggressive intergranular penetration of sulfides.des.

Mechanical Properties and Flame Retardancy of Rigid Polyurethane Foam Using New Phosphorus Flame Retardant (새로운 인계 난연제 합성과 이를 이용한 경질 폴리우레탄 폼의 난연성 및 물성 분석)

  • Lee, Byoung Jun;Kim, Sang Bum
    • Applied Chemistry for Engineering
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    • v.27 no.6
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    • pp.577-582
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    • 2016
  • In this study, we compared and analyzed the flame retardancy and mechanical properties of three different rigid polyurethane foams (RPUF) containing noble non-halogen phosphorus flame retardant (BHP-RPUF) or halogen-phosphorus flame retardant (TCPP-RPUF) or no flame retardant material (Pure-RPUF). The noble phosphorus-based flame retardant, bis(3-(3-hydroxypropoxy)propyl) phenyl phosphate (BHP), was synthesized by the reaction between disodium phenyl phosphate and 3-chloro-1-propanol. Through universal testing machine (UTM) experiments, the compressive strength of BHP-RPUF was similar to that of TCPP-RPUF. From the result of foam morphology analysis, it was confirmed that BHP-RPUF has the lowest thermal conductivity of $0.023W/m{\cdot}K$. We also measured the size of air bubbles using reaction velocity and SEM, and analyzed how they affect the thermal conductivity. In addition, the heat-resisting property was investigated through TGA analysis. The limited oxygen index (LOI) test confirmed that BHP had the ability to increase the flame retardancy of RPUF.

Compressive Strength Estimation Technique of Underwater Concrete Structures using Both Rebound Hardness and Ultrasonic Pulse Velocity Values (반발경도와 초음파속도를 이용한 수중 콘크리트 구조물의 압축강도 예측 기술)

  • Shin, Eun-Seok;Lee, Ji-Sung;Park, Seung-Hee;Han, Sang-Hun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.18 no.4
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    • pp.118-125
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    • 2014
  • As the earth's current global warming has caused elevation of sea water temperature, size of storms is foreseen to increase and consequently large damages on port facilities are to be expected. In addition, due to the improved processing efficiency of port cargo volume and increasing necessity for construction of eco-friendly port, demands for various forms of port facilities are anticipated. In this study, two kinds of nondestructive evaluation (NDE) techniques (rebound hardness and ultrasonic pulse velocity methods) are investigated for the effective maintenance of smart green harbor system. A new methodology to estimate the underwater concrete strengths is proposed and its feasibility is verified throughout a series of experimental works.

A Study on High Frequency Induction Hardening of S45C Specimen by FEA and Experiment (유한요소해석 및 실험에 의한 S45C 시편의 고주파 유도경화에 관한 연구)

  • Park, Kwan-Seok;Choi, Jin-kyu;Lee, Seok-Soon
    • Journal of Aerospace System Engineering
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    • v.12 no.5
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    • pp.1-7
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    • 2018
  • In this study, we proposed a high frequency induction hardening analysis method based on electromagnetic-thermal co-simulation. In the high frequency induction heating analysis, the results of the finite element analysis (FEA) (considering the change of the material property and the cooling factor according to the temperature) and those of the high frequency induction hardening experiment (using the S45C specimen) were compared. The hardness of the S45C specimens was measured using the micro Vickers hardness test to determine the depth of hardening. The measurement results were then compared with the results of FEA. The result of high frequency induction heating analysis showed that the temperature was more than $750^{\circ}C$, which is the A2 transformation point of S45C, while the temperature during quenching was below $200^{\circ}C$. The results showed that the difference of the depth of hardening between the FEA and the experiment is 0.2mm.

Bearing Capacity Characteristics of Stone Column by Numerical Analysis (수치해석에 의한 쇄석기둥의 지지력 특성)

  • Chun, Byung-Sik;Kim, Baek-Young
    • Journal of the Korean GEO-environmental Society
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    • v.5 no.1
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    • pp.75-84
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    • 2004
  • Stone column is one of the soft ground improvement method, which can enhance ground conditions such as the settlement reduction and the increasement of bearing capacity with applying the crushed stone instead of sand. In recent, general construction material, sand is in short of supply. Therefore, the bearing capacity improvement by the stone column is considered as the alternative method needed in many cases so the bearing capacity estimation is considered as important point. Nevertheless, adequate estimation methods to predict bearing capacity of stone column considering stone column and improvement effect of ground is not yet prepared. For the analysis of above mentioned points, the behavior of stone column were simulated as numerically on various property cases of crushed stone and surrounded ground. Through the numerical analysis of simulation results, the formula for the bearing capacity estimation of stone column was suggested. This formula was verified by comparing the prediction result of in situ test.

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Mixing and Strength Properties of 150MPa Ultra High Strength Concrete (150MPa 초고강도 콘크리트 배합 및 강도발현 특성)

  • Ahn, Jong-Mun;Kang, Hoon;Kim, Jong-Keun;Shin, Sung-Woo
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.373-376
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    • 2008
  • Ultra High Strength Concrete(UHSC) is necessary a clear presentation about mechanical property that is different from normal strength concrete and an evaluation of serviceability of high rise building which is used ultra high strength concrete. To mixing ultra high strength concrete with $f_{ck}$=150MPa pre-mix cement were manufactured and experimental study were conducted to evaluated on the mixing properties and compressive strength with major variables as unit cement contents, water-binder ratio and type of pre-mix cement. As a test result, it is shown that the concrete mixing time is required about 5$^{\sim}$6 minute untill the each materials(ordinary portland cement, silica fume, blast-furnace slag powder and anhydrite) are revitalized enough. A slump flow of fresh concrete are shown about 700$^{\sim}$750mm with proper viscosity. And average value of concrete compressive strength are shown about 77% in 7days, 87% in 14days and 102% in 56days for 28days of concrete material age. From this experimental study, a proper mixture proportion of pre-mix cement are recommended about 54$^{\sim}$59% OPC, 25$^{\sim}$30% blast-furnace slag powder and 10$^{\sim}$15% silica fume for mix the ultra high strength concrete with $f_{ck}$=150MPa.

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THE EFFECTS OF SPURE AND INVENTS ON THE CASTING ACCURACY AND POROSITY OF TI-NI CASTINGS

  • Cho Lee-Ra;Yi Yang-Jin;Park Chan-Jin
    • The Journal of Korean Academy of Prosthodontics
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    • v.41 no.3
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    • pp.342-350
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    • 2003
  • Statement of problem. Titanium-Nickel alloy might be used in various prosthetic restorations since it has a unique property such as super-elasticity and high fatigue resistance. However, little is known about the casting ability of this alloy. Purpose. This in vitro study compared the casting accuracy and the porosity made with different investments and various sprue designs to ascertain what casting condition would be better for the fabrication of Ti-Ni cast restorations. Material and methods. A total of 70 Ti-Ni alloy crowns were made and divided into 7 groups of 10 copings on a metal master die. For measuring the effect of the sprue numbers, two groups with one and two 8-gauge sprues were compared. Moreover, the results of the conventional sprue and the double thickness sprues were compared. Three investments were used; carbon free phosphate bonded investment, titanium investment and gypsum bonded investment. The cast restorations were evaluated at 48 points on the entire circumferential margin with a stereomicroscope measuring in micrometers. Each crown was radiographically examined for casting defects and porosity. Data on casting accuracy were analyzed using two-way and Post hoc Scheffe's comparison to determine whether significant differences existed at the 95% confidence level. Student-Newman-Keuls test were performed to identify significant differences in the number of voids. Results. The double sprueing group and double thickness group had significantly less marginal discrepancy than the single sprueing group (P<.05 and P<.01, respectively). The castings with phosphate bonded investment showed the least marginal discrepancy and the smoothest surface. The castings invested in the gypsum bonded investment had the greatest gaps in margin and the largest failure rate. The double sprueing group and phosphate bonded investment group had significantly smaller void numbers and smaller void size than the other groups. Conclusion. Within the limitations of this in vitro study, the casting accuracy of the groups using thicker, double sprue design and the phosphate bonded investment was significantly superior. Moreover, void number and size were less than other groups.